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Jurnal Teknik Kimia dan Lingkungan

jtkl
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Published by Politeknik Negeri Malang

ISSN : 25798537 EISSN : 25799746 DOI : http://dx.doi.org/10.33795/jtkl

Core Subject : Science, Engineering,

Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Engineering Materials Science & Nanotechnology

JTKL editors welcome manuscripts in the form of research articles, literature review, or case reports that have not been accepted for publication or even published in other scientific journals. Articles published in cover key areas in the development of chemical and environmental engineering sciences, such as: Energy Waste treatment Unit operation Thermodynamic Process simulation Development and application of new material Chemical engineering reaction Biochemical Biomass Corrosion technology The "JURNAL TEKNIK KIMIA DAN LINGKUNGAN" journal is a peer-reviewed Open Access scientiﬁc journal published by Politeknik Negeri Malang. This journal ﬁrst appeared in October 2017. The main purpose of the journal was to support publication of the results of scientiﬁc and research activities in the field of Chemical and Environmental Engineering. It is published twice a year in April and October.

Arjuna Subject : Teknik Kimia (semua kategori) - Kimia Proses dan Teknologi

Articles 133 Documents

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Valorization of Waste Cooking Oil into Liquid Organic Fertilizer by Anaerobic Fermentation Method Budi Santoso; Arista Putri Permatasari; Sisilia Pratama; Prahady Susmanto; R.R. Yunita Bayu Ningsih
Jurnal Teknik Kimia dan Lingkungan Vol. 7 No. 1 (2023): April 2023
Publisher : Politeknik Negeri Malang

Liquid organic fertilizer is a type of fertilizer that has a liquid form with a brownish color and is commonly used in agriculture as a supporting material for the main fertilizer. Liquid organic fertilizer can be produced through the fermentation process of organic matter, such as plant residues, animal or human waste, and organic waste so that it will not damage the environment. The manufacture of liquid organic fertilizer in this study uses waste cooking oil as raw material which will be fermented anaerobically for 21 days with the use of EM4 activator volume of 10 mL and 50 mL. This study was conducted to determine how much potential used cooking oil waste can be converted into liquid organic fertilizer. The results showed that the best concentration of nitrogen, phosphorus, potassium, and carbon organic in liquid organic fertilizer was obtained at 10 mL volume of EM4 activator. The best nitrogen concentration is 0.520 ppm, the best phosphorus concentration is 12.213 ppm, the best potassium concentration is 12013.825 ppm, and the best organic carbon concentration is 2.10%.

Effect of Immersion Concentration in Salt Solution, Drying Time and Air Velocity on Drying Wet Noodles Using a Tray Dryer and Solar Assistance Maktum Muharja; Siska Nuri Fadilah; Achri Isnan Khamil; Rizki Fitria Darmayanti; Ditta Kharisma Yolanda Putri; Meta Fitri Rizkiana; Viqhi Aswie; Badril Azhar
Jurnal Teknik Kimia dan Lingkungan Vol. 7 No. 1 (2023): April 2023
Publisher : Politeknik Negeri Malang

The noodles in the market are dry noodles with 8-10% water content. Dried noodles have a longer shelf life because they are less prone to mold growth. Drying noodles with the help of the sun and tray dryers are currently an option because they are efficient and do not require a lot of energy. Reduction of water content is also optimized by soaking wet noodles in salt water. This study aims to determine the effect of soaking noodles in salt water and the flow rate to decrease the water content of noodles. The study began with soaking wet noodles in a salt solution with a variation of 50-150 g/L, then dried for 1 hour using a hybrid method and tray dryer with a flow rate variation of 1.2-3.3 m/s. Observations were made at intervals of 0-1 hour. The results showed that the time and speed of the flow rate can reduce the humidity in the drying chamber of the tray dryer. The lowest water content reduction of up to 11% was obtained when soaking wet noodles in 150 g/L salt solution and at the highest flow rate of 3.3 m/s. The ANOVA results show that the drying method with tray dryer is more optimal than hybrid drying. Thus, this method can be a solution to optimize the noodle drying process quickly and efficiently.

Application of Sequencing Batch Biofilm Reactor (SBBR) Using Microalgae Chorella sp. to Removal Nutrient in Grey Water Shinta Elystia; Rika Kristin; David Andrio
Jurnal Teknik Kimia dan Lingkungan Vol. 7 No. 1 (2023): April 2023
Publisher : Politeknik Negeri Malang

Grey water contains organic matter that is directly disposed to the environment without any treatment previously, will cause pollution and impacting life in the water. Treatment that can be done is using microorganisms. One of its kind is the microalgae Chlorella sp. which utilizes organic matter as a source of nutrients for its growth. In this study, the Kaldness 1 (K1) bio carrier was added as a medium for attaching microorganisms using the Sequencing Batch Biofilm Reactor (SBBR) process. The research objectives were (1) to know the maximum number of Chlorella sp. both attached and suspended in the Sequencing Batch Biofilm Reactor (SBBR), (2) to obtain the best cycle time and stabilization time in the removal of COD, Ammonia, and MLSS in grey water. The research was conducted by varying the stabilization time (1.5; 2 and 2.5 hours) in each cycle for four cycles with a constant variation of charging time 30 minutes, reaction 120 minutes, 45 minutes, separation 45 minutes, and carried out with four cycles, stirring speed at 60 rpm, the concentration of algae suspension in SBBR was 25% and the volume of Kaldness K1 medium was 20%. The results showed the number of microalgae cells Chlorella sp. was suspended and attached to 1.85 x 106 and 1.46 x 106 cells/ml. The best removal of COD, ammonia, and MLSS was found in the stabilization time variation of 1.5 hours in 4 cycles with a removal efficiency of 84% and 76%, respectively, and an increase in the concentration of suspended and attached MLSS by 4780 mg/l and 4720 mg/l. It can be concluded that the faster stabilization time, the more removal efficient will be.

Utilization of Yellow Shells (Cypraea moneta) in the Treatment of Cadmium Heavy Metal (Cd) Waste Noor Isnaini Azkiya; Rosita Dwi Chrisnandari; Wianthi Septia Witasari
Jurnal Teknik Kimia dan Lingkungan Vol. 7 No. 1 (2023): April 2023
Publisher : Politeknik Negeri Malang

Cadmium (Cd) metal is a heavy metal that can cause environmental pollution if its levels are above the environmental quality standard value. Generally, industrial wastes such as paper industry waste contain heavy metal Cd with levels reaching 0.026 ppm. Meanwhile, the quality standard for Cd metal in the environment is 0.005 ppm. For this reason, it is necessary to process it to reduce the levels of Cd metal in the waste before being discharged into the environment. One way that can be used to reduce the levels of Cd metal is by adsorption method using Cypraea moneta clamshells containing chitin. This study used variations in the particle size of the shellfish adsorbent of 6 and 12 mesh. In addition, the ratio of the amount of adsorbate and adsorbent (mg:mg) is 1 : 0.5x106; 1 : 1x106; and 1 : 1.5x106. Based on the results obtained, it showed that the use of shellfish as an adsorbent was able to reduce Cd metal content up to 89%.

Comparison of Oil Palm Empty Fruit Bunch Delignification at Room and Mild Temperature Lidya Elizabeth; Emmanuela Maria Widyanti; Bambang Soeswanto; Dini Sri Wahyuni; Kartika Dian Pratiwi
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 2 (2022): October 2022
Publisher : Politeknik Negeri Malang

Oil palm empty fruit bunches (OPEFB) is one kind of palm oil industry solid waste. OPEFB contains high lignocellulose for about 81-89% that can be used for production of fertilizer, paper, filler, and composite. The separating method of lignocellulose into cellulose, lignin, and hemicellulose can be carried out by delignification using H2O2 and MnSO4.H2O as catalyst. Two experimental designs were performed using the Minitab 21 program with Response Surface Methodology (RSM). Both designs have temperature as their dependent variable. The processes are carried out at 36oC and room temperature with the same variable independent, such as delignification time and concentration of the catalyst. The difference between these two designs is in their stirring process. Delignification that occured at 36oC is processed under constant stirring, while delignification that occured at room temperature is processed without stirring. This experiment aims to determine the optimum conditions for using Mn-catalyst in delignification by varying the time and catalyst concentration. The results show that the lowest lignin content in delignification with reflux is 19.71% (w/w), and for delignification without reflux is 18.24% (w/w). The optimum condition obtained by RSM for reflux delignification was at 6,83 hours with use of 11,03% (w/w) catalyst. Meanwhile, without reflux delignification, the optimum condition was at 3,38 days with a 3.76% (w/w) catalyst.

Techno-Economic Analysis of Extractive Butanol Fermentation by Immobilized Cells with Large Extractant Volume Darmayanti, Rizki Fitria; Muharja, Maktum; Zhao, Tao; Gao, Ming; Tashiro, Yukihiro; Sakai, Kenji; Sonomoto, Kenji
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 2 (2022): October 2022
Publisher : Politeknik Negeri Malang

There are several challenges for ABE fermentation to be used in an industrial scale including the low of butanol yield, the high energy requirement for separation and purification, and the competeness of sugar with food demand as substrat. In this study, techno-economical aspects of ABE fermentation by using immobilized cells with large extractant volume were studied. Overall production process was designed using rice straw as raw material which is semi-hydrolyzed to produce cellobiose, glucose, xylose, and arabinose mixture. Concentrated sugar was then fed to extractive fed-batch fermentation using immobilized cells. Finally, extractant was recovered and products were purified by distillation column. By evaluating this process design for the small scale capacity of 238 kg-butanol and acetone/day, the energy requirement was 41.3 MJ/kg-butanol and acetone and the cost was 1.91 $/kg-butanol and acetone. Although the cost was higher than butanol produced by petrochemical process of 1.08 $/kg-butanol, it may reduce if the scale is increased.

Optimization of Essential Oil Extraction of Beluntas (Pluchea Indica L.) Leaves by Using Solvent-Free Microwave Extraction Nur Karima; Nova Chintya Kurniawati; Boy Arief Fachri; Istiqomah Rahmawati; Bekti Palupi; Mahfud Mahfud; Ditta Kharisma Yolanda Putri; Atiqa Rahmawati; Badril Azhar; Maktum Muharja
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 2 (2022): October 2022
Publisher : Politeknik Negeri Malang

Beluntas (Pluchea Indica L.) which commonly used as astringent and antipyretic has a high potential for the feedstock of essential oil production. The objective of this work is to optimize solvent-free microwave extraction (SFME) of Beluntas leaves by using response surface methodology (RSM). Box-Behnken Design with the variations of extraction time (60-120 min), feed/distiller ratio (0.06-0.1 g/ml), and heating power (150-450 W) was utilized to optimize essential oil yield. The feed/distiller ratio factor had the highest significant effect on the essential oil yield (P<0.05). Essential oil yield increased as the increase of oil heating power and time extraction, and vice versa. On the other hand, the increase in the feed/distiller ratio gave a negative impact on the essential oil yield. The maximum essential oil yield using SFME method of 0.2728 b/b% was obtained for the optimized condition of extraction time of 90 min, microwave heating power of 450 W, and feed/distiller ratio of 0.06.

Effect the Addition of Biodiesel from Nyamplung Oil (Calophyllum Inophyllum) on Performance and Emission Characteristics of Diesel Engines Abdul Hamid; Amin Jakfar; Saiful Saiful; Ike Dayi Febriana; Faizatur Rohmah
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 2 (2022): October 2022
Publisher : Politeknik Negeri Malang

In this study, the use of biodiesel from nyamplung oil (Calophyllum Inophyllum) was studied through a transesterification reaction using a heterogeneous catalyst of CaO from limestone originating from Pamekasan, Madura. The composition ratio used between nyamplung oil and methanol in the transesterification reaction was 1:12 (mol/mol) with the addition of 4% CaO catalyst. The biodiesel that is formed is then tested for its performance and emission characteristics in diesel engines with various fuel mixtures between pure diesel and biodiesel (B-10, B-20, B-30, B-40, B-100 and S-100). The test results for biodiesel blends with the highest power produced from B-10, B-20, B-30 and B-100 fuels were 0.26 kW each at a load of 250 watts. While at a load of 500 watts, the highest power is obtained from the B-40 fuel, which is 0.58 kW. The results of performance testing using S-100 fuel obtained the highest power values of 0.27 and 0.58 kW, respectively, with a load of 250 and 500 watts. Performance testing for biodiesel blends, the highest torque value was obtained when using B-10, B-20, B-30 and B-100 fuels, which were 1.65 N.m each with a load of 250 watts. While at a load of 500 watts, the highest torque is obtained on B-40 fuel, which is 3.69 N.m. The fuel S-100 produces torque of 1.71 and 3.69 N.m, respectively, with a load of 250 and 500 watts. Emission gases characteristics of carbon monoxide (CO), nitrogen monoxide (NO) and nitrogen oxides (NOx) showed the lowest concentrations obtained in B-100 fuel were 387 ppm, 92 ppm and 96 ppm, respectively. Meanwhile, the highest concentrations of CO, NO and NOx emissions were produced from pure diesel fuel (S-100), namely 574 ppm, 126 ppm and 132 ppm, respectively.

Delignification of Cassava Peel by Using Alkaline Hydrogen Peroxide Method: Study of Peroxide Concentration, Solid/Liquid Ratio, and pH Dini Nur Afifah; Neni Damajanti; Maulani Mustholidah; Hariyanti
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 2 (2022): October 2022
Publisher : Politeknik Negeri Malang

Cassava peel is a natural material with cellulose content reaching 33.33%. In order to utilize cassava peel as a biodegradable polymer and renewable energy alternative, a delignification process is essential to separate cellulose from hemicellulose and lignin, which prevents the penetration of cellulose hydrolyzer. The delignification method chosen in this study was alkaline hydrogen peroxide (AHP). The AHP is based on the autoxidation of lignin using hydrogen peroxide (H2O2) in an alkaline environment. This method was chosen because it can damage the lignocellulosic structure with relatively low energy and is more selective for lignin. However, under certain conditions, AHP can trigger carbohydrate depolymerization, which decreases yield. Therefore, it is necessary to study the effect of H2O2 concentration, Solid/Liquid ratio (S/L) (w/v), and pH to evaluate the effectiveness of lignin removal in cassava peel. The concentration of H2O2 was varied into 1.5%, 3%, 4.5%, 6%, and 7.5%. The S/L ratio is varied to 1:3, 1:5, 1:7, 1:9,1:12. The pH of the solution was varied to 8, 9, 10, 11, and 12. The reaction temperature was maintained at 70-90 °C for 3 hours. The results showed that lignin could be reduced to 84.05% for 3 hours by using 6% H2O2, an S/L ratio of 1:5, and a pH of 11. The reaction carried out under these conditions can also increase the amount of cellulose from 33.33% to 49.00%.

Vegetable Waste Biodrying Treatment for Energy Recovery as Refuse Derived Fuel Potential Iva Yenis Septiariva; I Wayan Koko Suryawan; Mega Mutiara Sari
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 2 (2022): October 2022
Publisher : Politeknik Negeri Malang

Vegetable waste is a type of biodegradable organic waste found in every location in Indonesia. In addition, vegetable waste also dominates food waste. One of the ways to use vegetable waste is to use energy recovery. Energy recovery of vegetable waste can be done by time-dependent biodrying and bioactivator. This study aimed to determine the effect of time and activator application on the vegetable waste biodrying process. In this study, 0.5 kg of waste is used with an airflow rate of 15 liters/minute, the temperature in the process is in the range of 28.4-34.1°C. The bioactivators used in this study were baker's yeast, tempeh, and tape. The maximum decrease in mass occurs in the biodrying process with the addition of a bioactivator. The multivariate effect test results showed an effect of time and bioactivator on changes in water content and caloric value. However, the interaction between time and bioactivator only affects the water content. This is because the degradation process occurs utilizing microorganisms stored in the bioactivator liquid and water in vegetable waste. Further research is needed to know the effect of other variables in the biodrying process, especially the right detention time and bioactivators that accelerate the rate of degradation.

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Home Page

OAI Link

Editorial Team

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Reviewer

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Contact Name Agung Ari Wibowo

Contact Email agung.ari@polinema.ac.id

Phone +62341404424

Journal Mail Official jtkl@polinema.ac.id

Editorial Address Jl. Soekarno Hatta No. 9, Malang, Indonesia

Location Kota malang, Jawa timur INDONESIA

Abstract

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Contact Name
Agung Ari Wibowo

Contact Email
agung.ari@polinema.ac.id

Phone
+62341404424

Journal Mail Official
jtkl@polinema.ac.id

Editorial Address
Jl. Soekarno Hatta No. 9, Malang, Indonesia

Location
Kota malang,

Jawa timur

INDONESIA