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All Journal Jurnal Ilmu Dasar Jurnal Sains Materi Indonesia JFA (Jurnal Fisika dan Aplikasinya) JURNAL ILMIAH PENDIDIKAN FISIKA AL BIRUNI Science and Technology Indonesia International Journal of Science and Applied Science: Conference Series Indonesian Journal of Chemistry SELAPARANG: Jurnal Pengabdian Masyarakat Berkemajuan Jurnal Kreativitas PKM JIEMS (Journal of Industrial Engineering and Management Systems) Jurnal Fisika : Fisika Sains dan Aplikasinya Jurnal Aplikasi dan Teori Fisika JASIEK (Jurnal Aplikasi Sains, Informasi, Elektronika dan Komputer) Jurnal Fisika Indonesia Jurnal Pengabdian Masyarakat Khatulistiwa Journal of Energy, Material, and Instrumentation Technology NEAR: Jurnal Pengabdian kepada Masyarakat Jurnal Kemitraan Masyarakat
Posman Manurung
Departement Of Physics, Faculty Of Mathematic And Natural Science, University Of Lampung
Agriculture, Biological Sciences & Forestry Arts Humanities Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Control & Systems Engineering Decision Sciences, Operations Research & Management Earth & Planetary Sciences Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Health Professions Industrial & Manufacturing Engineering Languange, Linguistic, Communication & Media Law, Crime, Criminology & Criminal Justice Library & Information Science Materials Science & Nanotechnology Mathematics Mechanical Engineering Medicine & Pharmacology Nursing Physics Public Health Social Sciences Transportation Other

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Journal : Science and Technology Indonesia

 1 
Study on Crystal Structure, Surface Area, and Energy Gap Behaviors of Nanotitania Polymorphs Prepared Using Monoethanolamine Manurung, Posman; Maharani, Renita; Rahmayanti, Dita; Yulianti, Yanti; Junaidi; Marjunus, Ronius
Science and Technology Indonesia Vol. 9 No. 2 (2024): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2024.9.2.345-353

Abstract

Polymorphous nanotitania samples were prepared from titanium butoxide (TTB) as a precursor using sol-gel processing in ethanol as a solvent, without and with monoethanolamine (MEA). The experiments used 5.25 mL TTB and MEA with varied volumes of 0.5, 1.0, 1.5, and 2.0 mL. The sample without MEA was specified as sample A, and the samples produced using MEA were specified as samples B, C, D, and E, respectively. All samples were calcined at 500 °C for 4 h and then collected data by X-ray Diffraction (XRD), the Brunauer-Emmett-Teller (BET) method used to analyze Surface Area Analyzer (SAA), Transmission Electron Microscopy (TEM), Raman Spectroscopy, and UV-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS). The results of XRD characterization indicate that samples A and B form anatase phase, while samples C and D are composed of anatase, brookite, and rutile phases, and sample E is consisted of anatase and brookite phases with weight percentages of (94.53 ± 1.72) % and (5.47 ± 0.36) %, respectively. The presence of the three phases of titania is also confirmed by Raman spectroscopy analysis, which showed anatase peaks at 146, 197, 398, and 513 cm-1, brookite peaks at 245 and 402 cm-1, and rutile peaks at 319, 436, and 612 cm-1. According to XRD, the samples have the particle size in the range of 14-19 nm. A representative sample (sample C) was also characterized using TEM, revealing a particle size of 16.0 ± 0.3 nm. This representative sample revealed the largest surface area of 172.2 m2/g, as seen by BET, and the lowest energy gap of 3.03 eV.
Co-Authors Abdurrahman, Ahmad Faruq Adeliya Ayu Anggraini Agnesia, Donna Agus Riyanto Agus Riyanto Agus Riyanto Agus Riyanto Agus Suyatna Ahmad Faruq Abdurrahman Ahmad Rosadi Alfin Edo Kaisar Lubis Amir Supriyanto Anggi Puspita Dewi Anggi Stevani Anggraini, Adeliya Ayu Anggraini, Anisyah Aprilia, Ayu Arya R. Syah Ayu Aprilia Ayu Aprilia Benyamin, Chairunissa A Chandra Ertikanto Craig Buckley Delfi Oktavia Amrani Della M. Andini Dita Rahmayanti Dwi Asmi Edi Suharyadi Ediman Ginting Ediman Ginting Ediman Ginting Ediman Ginting Suka Erika Sempana Erika Sempana Ginting Fajar Nurjaman Faradilla Syani Fath, Yusril Al Fatia Ulfah Fegi Liani Firdaus, Iqbal Flora Rosdiana Lumbansiantar Futichah Futichah Futichah Futichah Gregorius N. Susanto Gultom, Rysa Sonya Reni Paulin Gurum Ahmad Pauzi Hasni Handayani Hesti Wahyu Handani Imaniar Romaeni Indra Pardede Iqbal Firdaus Irma Yulianti It Meng Low Jayanti Pusvitasari Johar Sitohang Junaidi Junaidi - Junaidi Junaidi Junaidi Junaidi Junaidi Junaidi Junaidi Junaidi Juniati Br Simbolon Karo Karo, Pulung Karo, Pulung Karo Ketut Putra Wijaya Lady Permatasari Lusi Vusfita Sari Maharani Maharani Maharani, Renita Marjunus, Ronius Marjunus, Roniyus Mega Pertiwi, Mega Mey Puji Astuti Miranti Syafitri Mitra Septanto Nabilah Rafidiyah Nadia Febriyanti Nita Susanti Nola Fricilia Nurcahayaniati, Hikmah Nurqori Setiawati Nurul Oktavia Pertiwi, Salwa Dian Prastica, Lusia Prihanto, Surya Puji Lestari Pulung Karo-Karo Pulung Karo-karo Pulung Karo-Karo Putri, Faradilla Nabila R. Supryanto Rahayu, Sri Rahma Fauza Rahmayanti, Dita Renita Maharani Fauzi Rika Rahayu Riska Trisna Nuraini Riyanto, Agus Rizki Amalia Rudy Situmeang Rudy Situmeang Rudy T M Situmeang S Suprihatin Sahtoni Sahtoni Sari, Tria Permata Sembiring, Simon Sempana, Erika Shabrina, Shabrina Yakosati Simon Sembiring Simon Sembiring Simon Sembiring Simon Sembiring Siti Fadilah Sitohang, Rosanti Sri Rahayu Sri Ratna Sulistiyanti sri wahyu suciayti Sri Wahyu Suciyati Sri Wahyu Suciyati Suharyadi, Edy Sukma Wibowo Sumardi . Sumardi, Sumardi Sumiyati Sumiyati Supardi Supardi Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Supriyanto, Amir Syafriadi Syafriadi Syafriadi Syafriadi Syafriadi Tria Permata Sari Trianasari Trianasari Trianasari, Trianasari Vega Rahmawati Ar Vidi Nurhidayah Wasinton Simanjuntak Windhini Anggraeni Yanti Yulianti Yanti Yulianti Yanti Yulianti Yanti Yulianti Yanti Yulianti Yanti Yulianti Yuant Tiandho Yudhistira Novita Handayani Yunita Yunita Zaharani, Rethanita Zahra Maria Ulfa