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All Journal Jurnal Matematika & Sains Jurnal Pendidikan dan Pembelajaran Kimia (JPPK) Journal of Mathematical and Fundamental Sciences Jurnal Pendidikan Kimia Universitas Riau Jurnal Tadris Kimiya Jurnal Pendidikan Kimia (JPKim) JOURNAL OF SCIENCE AND SOCIAL RESEARCH Jurnal Inovasi Pembelajaran Kimia (Journal Of Innovation in Chemistry Education) Indonesian Journal of Chemical Science and Technology Jurnal Teknologi Pendidikan : Jurnal Penelitian dan Pengembangan Pembelajaran SCIENCE : Jurnal Inovasi Pendidikan Matematika dan IPA Ensiklopedia: Jurnal Pendidikan dan Inovasi Pembelajaran Saburai Educenter: Jurnal Ilmiah Pendidikan Jurnal Sains dan Teknologi Makara Journal of Science Panthera : Jurnal Ilmiah Pendidikan Sains dan Terapan Jurnal Sains dan Ilmu Terapan EDUCENTER JURNAL PENDIDIKAN Journal of Humanities Education Management Accounting and Transportation Indonesian Journal of Jamu
Iis Siti Jahro
Universitas Negeri Medan
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Journal : Jurnal Pendidikan Kimia (JPKim)

 1 
Effectiveness of sulfuric acid and hydrochloric acid catalysts in the esterification of frankincense cinnamic acid with ethanol and methanol Sitorus, Marham; Suyanti, Retno Dwi; Jahro, Iis Siti; Siahaan, Suria Bersinar; Saragih, Innovayani; Sitorus, Francisca T. A
Jurnal Pendidikan Kimia Vol. 16 No. 1 (2024): April
Publisher : Pascasarjana Universitas Negeri Medan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24114/jpkim.v16i1.53231

Abstract

This research aims to compare the effectiveness of sulfuric acid and hydrochloric acid catalysts in the esterification of frankincense cinnamic acid (STYRAX paraleoncomud PERK). Esterification of sulfuric acid catalyst is carried out with ethanol and for hydrochloric acid catalyst with methanol. Esterification was carried out by refluxing a mixture of 1:20 cinnamic acid - ethanol and methanol, with 3 mL of each catalyst at a temperature of 60oC for one hour. The results were rinsed with 3 x 50 mL distilled water and dried with anhydrous sodium sulfate. The results were filtered and verified for functional groups using FTIR and composition analysis using GC “ MS. The results of FTIR interpretation show a decrease in absorption intensity (-OH) at 3500 cm-1 as a functional group that reacts compared to the ester results as an indication of the ongoing esterification reaction. The resulting ethyl cinnamate has a high conversion of 84.42%. Methyl cinnamate also has a distinctive ester aroma but is clearer and based on GC-MS, the content of methyl cinnamate is relatively low, namely 34.40%, the remaining cinnamic acid is 37.28%, and various side products of 28.32%. Thus, the catalyst that provides better conversion is sulfuric acid, but it requires further purification by examining the appropriate absorbent and bleaching agent. The brown color of the ester product catalyzed by sulfuric acid is thought to occur due to the oxidation of the cinnamic acid double bond by the catalyst.
Co-Authors Adelia Yesya Putri Hasibuan Agnes Yuniarty Simbolon Amalia, Meisya Angin, Jansen Riko Perangin Ani Sutiani Ani Sutiani Anisa Nursalsabillah Nasution Annisa Rahayu Annisa Rahayu Ardiansyah Ardiansyah Asep Wahyu Nugraha Asep Wahyu Nugraha Aulianti, Dita Ayi Darmana Ayi Darmana Ayi Darmana, Ayi Banu Nursanni Bohari M. Yamin Bohari M. Yamin Br Bangun, Kurnia Wati Catur Kurniawan CINDY CINDY Daeli, Dinastini Damanik, Syifa Namira Debora Putri Sitorus Debora Putri Sitorus Desri Berliana Daeli Djulia Onggo Djulia Onggo Djulia Onggo Dwi Rahmanisa Efrio Angelina Sitio Esther Jacoba Martha Vertelman Fadhila, Nabila Nur Fahimah Martak Fitria Febrianti, Fitria Gavril Orlando Tumio Manalu Gurning, Mita Agresia Hutagalung, Tien Parsaulian Hutagaol, Rahul Hutauruk, Rafli Intan Ayu Safitri Intan Fahira Yuzan Ismunandar Ismunandar . Ismunandar Ismu Izwani, Putri Khairi Jasmidi Jasmidi Jasmidi Juwitaningsih, Tita Khaira, Mutiah Khuzaimah Dasopang Maibang, Siti Rahmah MANIK, INDA WATI Manullang, Marisa Marham Sitorus Marpaung, Mutiara Evelin Yoseva Meli Sartika Silaban Moondra Zubir Nasution, Anisa Nursalsabillah Nasution, Fadiya Malona Nursanni, Banu Petra van Koningsbruggen Pratama, Muhammad Rizky Putri Faradilla Putri Yustika Sary Ratu Evina Dibyantini Ratu Evina Dibyantini Regina Gresella Br Panjaitan Retno Dwi Suyanti Rode Juwita Sinaga Sakinah, Sheila Saragih, Innovayani Sarah, Arina Sami Sary, Putri Yustika SATI, NAFFA Sembiring, Niki Arih Ersada Br Sembiring, Silvia Gressiela Br Siahaan, Suria Bersinar Sihombing, Cindy Monalisa Sijabat, Hotman Priwaldi SIMANJUNTAK, PUTRINA Simanullang, Selafionita Simaremare, Happy G. Maritoma Siregar, Anggita Rahma Siregar, Eka Guspi Anti Sitorus, Francisca T. A Situmorang, Elsa Hasri Novensa Sri Adelia Sari Suryani Suryani Suryani Suryani Susanto Imam Rahayu Susanto Imam Rahayu Sutiani, Ani Syafitri, Amelia Syahputra, Ricky Andi Tama, Gita Citra Tania Evelin Turnip, Yulika Hotrina Vebilla May Ningsih Veronika, Christy Chirona Windayani, Neneng