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JKPK (Jurnal Kimia dan Pendidikan Kimia)
Published by Universitas Sebelas Maret
ISSN : 25034146     EISSN : 25034154     DOI : -
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Chemistry
The JKPK (Jurnal Kimia dan Pendidikan Kimia) is a national journal, published three times a year in April, August, and December, containing research articles on Chemistry and Chemistry education.
Arjuna Subject : -
Articles 255 Documents
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Study on Varied Bagasse Fiber and Epoxy Resin Compositions with Rice Bran Filler to Biocomposite Characteristics Budiyati, Eni; Saputri, Fauzia Zeinandi; Prasasti, Radeva Intan Kurnia; Elwin, Muhammad Rishad
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 1 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i1.72587

Abstract

Natural fibers, with environmental, economic, and cost advantages, are highly sought-after for biocomposite materials. In the present study, the biocomposite samples of epoxy resin (as a matrix), bagasse fiber (as reinforcement), and rice bran (as a filler) were prepared. Tensile strength, strain, and Young's modulus will be the parameters concerning which the quality of the biocomposite can be tested. On the one hand, bagasse fiber is to be a strength enhancer in the resulting biocomposite. On the other hand, rice bran may increase the biocomposite's density. The process research comprises fiber yarn from milled bagasse, alkalized fiber with KMnO4, specimen printing process, and analysis. All the fibers were treated by soaking them in 3 grams of KMnO4 solution for 30 and 45 minutes. The fiber is drained in an oven at 50 °C for ±1.5 hours. The printed fiber onto a specimen mold was printed with a mixture of epoxy resin and rice bran (1:1 w/w) and left for one day. Variation in the fiber mass was at 3, 4, and 5 grams. The sizes of the specimens were similar to the size of the mold according to ASTM D-638 type IV. Then, the fibers were removed from the mold and tested for tensile strength, strain, and Young's modulus. The results show that the greater the fiber mass, the greater the tensile strength value. These findings indicate that the tensile strength was optimized after soaking for 45 minutes with 5-gram fiber weight, which resulted in the tensile strength of 26.32±0.25 MPa, strain of 9.65±0.14%, Young's Modulus of 3.29±0.05 MPa, and water absorption of 41.99%.
MES surfactant-based liquid soaps added with eco-enzyme and pandan wangi leaf extract (Pandanus amaryllifolius Roxb) on physical-chemistry properties, and antibacterial activity," Riawati, Riawati; Mardiana, Diah; Srihardyastutie, Arie
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.88856

Abstract

The growing demand for liquid soap has spurred innovations in soap formulations, particularly using methyl ester sulfonate (MES) as a surfactant base combined with natural ingredients like eco-enzyme and fragrant pandan leaf extract. This study aimed to determine the optimal liquid soap formulation by evaluating physicochemical properties and antibacterial activity against Staphylococcus aureus. The research was conducted in two stages. First, liquid soap was produced at different temperatures (20°C, 50°C, and 100°C) to identify the optimal temperature based on maximum lipase activity. In the second stage, various formulations were prepared, incorporating eco-enzyme and fragrant pandan leaf extract at the identified optimal temperature. The six formulations tested were: F1 (MES-based soap), F2 (20% eco-enzyme), F3 (15% eco-enzyme and 5% fragrant pandan leaf extract), F4 (10% eco-enzyme and 10% fragrant pandan leaf extract), F5 (5% eco-enzyme and 15% fragrant pandan leaf extract), and F6 (20% fragrant pandan leaf extract). The formulations were assessed for lipase activity, pH, density, and viscosity. The most effective formulation was further tested for antibacterial activity using the disc diffusion method with six treatments, including MES-based soap and controls. Statistical analysis using One-Way ANOVA revealed that adding eco-enzyme and fragrant pandan leaf extract significantly affected the soap's properties. The optimal formulation, containing 5% eco-enzyme and 15% fragrant pandan leaf extract, exhibited a lipase activity of 15,778 U/mL, a pH of 5.02, a density of 1.06 g/mL, a viscosity of 3.59 cP, and an antibacterial zone of 37.22 mm, making it the best candidate for further development
Non-Enzymatic Detection of Glucose and Ketones in Urine using Paper-Based Analytical Devices 'Aisy, Kamila Rohadatul; Fahmi, Ahmad Luthfi; Sulistyarti, Hermin; Wulandari, Ika Oktavia; Sabarudin, Akhmad
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.87294

Abstract

Diabetes, driven by unbalanced diets and unhealthy lifestyles, is highly prevalent. In Indonesia, its prevalence is projected to reach 28.6 million by 2045. Microfluidic paper-based analytical devices (μPADs) are paper-based analytical tools that use hydrophilic paper for measurement and hydrophobic barriers to control fluid flow. This research aims to develop a non-enzymatic method for detecting glucose and ketones in artificial urine using S2Z-μPADs. The fabrication of S2Z-μPADs involves printing the design on Whatman No. 1 paper using wax printing and applying silver nanoparticles for glucose detection and the Schiff base reaction for ketone detection. The results show that the optimum condition for glucose detection is achieved with an AgNO3 concentration of 500 mM. A NaOH concentration of 10 M. Acetoacetate detection is optimized with a glycine concentration of 1 M, sodium nitroprusside concentration of 15%, NaOH concentration of 1 M, a drying time of 8 minutes, and a reaction time of 10 minutes. Validation results demonstrate good linearity for glucose (R² = 0.9821) and ketones (R² = 0.995). High precision was achieved with relative standard deviation (RSD) values of 3.792% for glucose and 1.482% for ketones. The obtained limits of detection (LOD) and limits of quantification (LOQ) indicate that the developed S2Z-μPADs can differentiate between each category of diabetes. The accuracy of glucose and ketone detection ranges from 87.463% to 97.374%. The high accuracy of the μPADs highlights their potential for reliable diabetes management and effective disease monitoring.
Chitosan Crosslinking from Clam Shells (Cerithidea obtusa) with Tripolyphosphate for Cadmium (II) Adsorption Koesnarpadi, Soerja; Anuar, Hajar; Widodo, Nanang Tri; Hastuti, Budi; Hadi, Saptono
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.80996

Abstract

The study investigates chitosan crosslinking from clam shells (Cerithidea obtusa) with tripolyphosphate for cadmium (II) adsorption. Chitosan was prepared by deacetylating chitin using 60% NaOH and heating at 140°C for 60 minutes. Chitin was isolated from Cerithidea obtusa shells, an abundant waste in East Kalimantan. Crosslinking of chitosan with tripolyphosphate was synthesized via gelation methods, dissolving 5 g of chitosan in acetic acid and adding 0.1% tripolyphosphate as a crosslinker. The chitosan-tripolyphosphate characterization was conducted using FTIR, XRD, and SEM. FTIR spectra revealed an N-H vibration at 1635 cm−1, NH3+ deformation at 1534 cm−1, C-O stretching at 1072 cm−1, and P-O vibration at 1026.91 cm−1, indicating the presence of tripolyphosphate in chitosan. The XRD pattern showed broad peaks at 19.85° and 23.50°, characteristic of amorphous chitosan-tripolyphosphate. SEM images depicted a flat sheet without pores and a tight surface. Cadmium (II) adsorption on chitosan-tripolyphosphate at an optimum pH of 4 followed a pseudo-second-order kinetic model. It adhered to the Langmuir isotherm model, with a maximum adsorption capacity of 27.8 mg/g. The results demonstrate that chitosan crosslinked with tripolyphosphate effectively for cadmium (II) adsorption.
Synthesis and Characterization of Polyaniline/CuO Nanocomposites with Various Temperature Sunarya, Risa Rahmawati; Sidik, Yosi Yosiva; Islamiati, Fitri Nur
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.90819

Abstract

Polyaniline (PANI) metal oxide composites are known for their high electrical conductivity, environmental stability, and enhanced mechanical strength, making them valuable in applications such as sensors, batteries, and electromagnetic shielding. This study focuses on synthesizing and characterizing PANI/CuO nanocomposites to examine their structural, morphological, and functional properties at different synthesis temperatures. By integrating the conductive polymer PANI with copper oxide (CuO), a p-type semiconductor with a narrow band gap, the material’s capabilities are significantly enhanced. The oxidative polymerization of aniline, the process by which PANI is formed, requires precise control of oxidizing agents and reaction conditions, as these factors directly affect the polymerization, conductivity, and overall properties of the resulting nanocomposite. The PANI/CuO nanocomposites were synthesized at three different temperatures: 10℃, 25℃, and 50℃, to determine how temperature affects their characteristics. Fourier Transform Infrared (FTIR) spectroscopy and Scanning Electron Microscopy (SEM) were employed to analyze these nanocomposites. FTIR results revealed shifts in the quinoid and benzenoid rings, indicating hydrogen bonding between the NH group of PANI and the CuO surface, which accelerates charge transfer. The SEM analysis showed that while pure PANI exhibits a uniform globular morphology, the PANI/CuO nanocomposites display a nanorod morphology. These morphological differences impact the surface area and electrical conductivity of the composites, highlighting the significance of temperature in tailoring the material's properties for specific applications.
In Silico Analysis of Antibacterial Activity of Fatty Acids in Swietenia humilis Zucc. Seed Extract Against Staphylococcus aureus sortase A enzyme Asmara, Anjar Purba; Hernawan, Hernawan; Nuzlia, Cut
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.87473

Abstract

This study utilised molecular docking to predict the binding affinity of various fatty acids (FAs) found in Swietenia humilis to the sortase A (SrtA) protein target from Staphylococcus aureus. Binding energies, measured in kcal/mol, indicated the strength and stability of ligand-protein interactions, with lower values signifying stronger binding. The binding affinities of eight FAs as the active constituents in n-hexane extract of S. humilis and the positive control, gentamicin, were compared to assess their theoretical antibacterial activity. Palmitoleic acid exhibited the strongest binding affinity (-5.6 kcal/mol) among the FAs, suggesting the highest potential antibacterial activity, followed by linoleic, palmitic, linolenic, arachidic, tricosanoic, stearic, and oleic acids in decreasing order of affinity. Despite having weaker binding energies than gentamicin, a common gram-positive inhibitor from aminoglycoside derivative, FAs showed multiple hydrogen bonds and van der Waals interactions with key residues like ARG197, VAL168, VAL166, and ILE182, contributing to their binding stability. Palmitoleic acid formed multiple hydrogen bonds (ARG197 and GLY119) and significant van der Waals interactions, highlighting its strong theoretical binding. Stearic and oleic acids, although having higher binding energies, also formed critical hydrogen bonds, suggesting moderate potential activity. Gentamicin's single hydrogen bond suggests a highly specific binding site, which may result in high antibacterial activity despite fewer interaction points. The study indicated that FAs like palmitoleic and oleic acid show substantial potential as supplementary antibacterial agents, especially in the context of combating antibiotic resistance. This finding can pave a path for drug design and development to address the S. aureus's resistance.
Enhancing Conceptual Understanding of Buffer Solutions with an Intertextual E-Book Prototype Dewi, Nur Sehasari; Mulyani, Sri; wiji, Wiji
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.85269

Abstract

The intertextual-based e-book prototype helps students understand buffer solutions by connecting the three levels of chemical representation: macroscopic, submicroscopic, and symbolic. This connection allows students to visualize chemical phenomena from simple to complex. The study aims to enhance students' conceptual understanding using this e-book prototype. The research and development (R&D) method followed five stages: research and information gathering, product development planning, initial product development, limited trials, and initial product revision. This process yielded a highly validated e-book prototype that promotes innovation. The validation results showed high feasibility in substance (85.71%), instructional methods (90.90%), and language (100%). Experts deemed the e-book prototype highly effective in improving conceptual understanding through its intertextual approach. Pretest and posttest assessments of 30 students indicated improved conceptual understanding after using the e-book. Initially, students demonstrated macroscopic and symbolic level abilities without associating the three levels of representation. After using the e-book, they could connect these levels, enhancing their understanding and conceptual understanding. The N_Gain scores for pretest and posttest assessments were 0.48 for the high category, 0.45 for the medium category, and 0.44 for the low category, showing moderate improvement. The t-test results (Sig. (2-tailed) = 0.000 < 0.05) confirmed the effectiveness of the e-Book. Teacher and student responses averaged 90% and 85.5%, respectively, indicating that the intertextual-based e-book on buffer solutions is highly suitable as a self-learning resource to improve conceptual understanding.
Development of PBL-Based Chemistry E-Modules for Colloidal Systems Sari, Sri Adelila; Nasution, Nurfadillah Syam
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.85301

Abstract

Integrating digital learning tools has become increasingly important for enhancing student engagement and learning outcomes in the rapidly evolving educational landscape. This research aimed to assess the feasibility of a developed e-module and its impact on student learning outcomes. The development process followed the ADDIE Model, comprising five stages: Analysis, Design, Development, Implementation, and Evaluation. The instruments used included interview sheets, e-module validation sheets, student response questionnaires, and a 20-item test instrument. The e-module was validated by experts based on content, presentation, language, and graphic criteria, achieving an average validity score of 91.6%, indicating strong validity. Following validation, the e-module was implemented with 36 eleventh-grade Science Program (XI MIA) students at a high Islamic school in Medan during the 2023/2024 academic year. The results demonstrated a significant improvement in student learning outcomes, as evidenced by an N-gain score of 0.76, which falls within the high criteria. Additionally, student responses to the e-module were overwhelmingly positive, with an average approval rating of 87%, categorising their feedback as "very good." The findings suggest that the developed e-module is feasible and effective in enhancing student learning outcomes. The high validation scores and positive student feedback indicate that the e-module is well-designed and meets educational standards. It is a valuable tool for improving student engagement and achievement in the classroom.
Effectiveness of the pH Master Application on Acid-Base Concepts as a Digital Alternative to Conventional Laboratory Practices for Enhancing Student Learning Outcomes" Kusumawati, Agnys Dewi; Ariani, Sri Retno Dwi; Indriyanti, Nurma Yunita
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.89855

Abstract

Traditional Chemistry Laboratories, such as acid-base reactions, are hard to demonstrate for present-day students in their lab classes when they need to have the knowledge exchange we had, graduating (and teaching) with mortar boards lined up and ready for weddings. The Evaluation Of The Digital Platform “pH Master” For Enhancing Chemistry Student Performance Through A Virtual Imitation of Traditional Lab Practices The study used Akker's research and development model, including initial studies, product design, testing products, and trials. Validation was done using the Aiken formula by two expert validators and three practitioners for all items with a V value greater than 0.87. Surveys for needs analysis involved 45 students, and the learning effects were assessed with 90 students across three schools. Results Students responded favourably to the pH Master app and perceived ineffable pedagogical value. Most students agreed on the necessity of doing practical activities about what was being learned, and almost all also had trouble understanding study materials specifically related to acids and bases. The results showed a statistically higher mean n-gain value in the experimental group than in control one (0.6622 versus 0.5691) by independent t-test across three schools at p < 0,001 significance level between the two groups. This then confirms that the media created did support student learning. This study highlights the potential of the pH Master app to enhance student learning experience and active involvement in chemical education, which suggests a promising approach towards digitalising conventional practical work.
Green Synthesis and Characterization of 4'-Hydroxy-4-Nitro Chalcone using Grinding Techniques Susanti VH, Elfi; Ariani, Sri Retno Dwi; Mulyani, Sri; Utomo, Suryadi Budi; Wathon, Muhammad Hizbul
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 9, No 2 (2024): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/jkpk.v9i2.80153

Abstract

The challenge of developing environmentally friendly synthesis methods for biologically active compounds remains a significant focus in green chemistry. This study aimed to synthesize 4'-hydroxy-4-nitro chalcone from 4-hydroxyacetophenone and 4-nitrobenzaldehyde using a grinding technique and then characterize the synthesized compounds. The 4'-hydroxy-4-nitro chalcone was synthesized via the Claisen-Schmidt grinding method for 45 minutes at room temperature. The grinding results were extracted with chloroform. The formed crystals were tested for purity by thin-layer chromatography (TLC), and further purification was carried out by recrystallization. The synthesized chalcone was characterized using FTIR, 1H-NMR, and 13C-NMR  spectroscopy. The chalcone was also tested for antibacterial activity using the disc diffusion method against Staphylococcus aureus and Escherichia coli. The results showed that 4'-hydroxy-4-nitro chalcone could be successfully synthesized from 4-hydroxyacetophenone and 4-nitrobenzaldehyde using the grinding technique, yielding orangish-white crystals with a 70.63% yield and a melting point of 173°C. Purity was confirmed by TLC, and structural characterization was achieved through FTIR, 1H-NMR and 13C-NMR spectroscopy. Antibacterial testing revealed that the synthesized chalcone produced a clear zone diameter of 9.27 mm against S. aureus and 27.88 mm against E. coli. These results indicate that the compound has relatively strong antibacterial activity against E. coli and relatively weak activity against S. aureus. This study demonstrates the effectiveness of the green synthesis method and provides valuable insights into the antibacterial properties of 4'-hydroxy-4-nitro chalcone

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