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All Journal Rekayasa Mesin Jurnal Teknologi Mineral dan Batubara Syntax Literate: Jurnal Ilmiah Indonesia Abdimas Universal International Journal of Community Service INDONESIAN JOURNAL OF URBAN AND ENVIRONMENTAL TECHNOLOGY Jurnal AKAL: Abdimas dan Kearifan Lokal Indonesian Mining and Energy Journal JURNAL ABDI MASYARAKAT INDONESIA (JAMIN) Journal of Earth Energy Science, Engineering, and Technology International Journal of Innovation in Mechanical Engineering and Advanced Materials Jurnal Teknologi Mineral dan Batubara
Kurniawati, Riskaviana
Universitas Trisakti
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Journal : Rekayasa Mesin

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PYROMETALLURGICAL PROCESS FOR ZINC ANALYSIS IN SPHALERITE APPLYING XRD AND XRF Dahani, Wiwik; Kurniawati, Riskaviana; Sundari, Rita; Marwanza, Irfan; Rachman, Faisal
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1525

Abstract

This paper has analyzed dominant zinc element in sphalerite naturally found together with galena in mineral ore. Since pyrometallurgical route related to roasting process is very common to mineral dressing, therefore, this investigation has studied the effect of varied roasting time (30 min, 60 min, and 90 min) and temperature (500oC, 600oC, and 700oC) on zinc mineral examination using XRD (X-Ray Diffraction) and zinc element using XRF (X-Ray Fluorescence) analyses. Previous studies usually applied cheaper AAS (Atomic Absorption Spectrometer) for zinc analysis in aqueous solution, however, sphalerite is a solid matrix and therefore, this study has applied XRF to analyze zinc. Pyrometallurgical process of zinc mineral in sphalerite is related to mineral transformation in the form of ZnSO4, ZnS, and ZnO that cannot be detected by XRF. Therefore, this study has used XRD that can observe mineral transformation.   The XRD pattern shows four intense peaks at 2θ (28o, 47o, 56o, and 76o) justified sphalerite (ZnS) sample with little amount of pyrite (FeS2) and galena (PbS) as impurities. The XRF analysis shows from 30 min to 90 min, the Zn content has increased remarkably at 700oC and Zn content looked stagnant at 500oC, while Zn content increased dramatically from 60 min to 90 min at 600oC. During roasting process at high temperature, ZnS mineral converted to ZnO and expelled SO2 gas due to oxidation reaction causing weight reduction. The study is valuable for mineral processing in searching for optimization.
PYROMETALLURGICAL PROCESS FOR ZINC ANALYSIS IN SPHALERITE APPLYING XRD AND XRF Dahani, Wiwik; Kurniawati, Riskaviana; Sundari, Rita; Marwanza, Irfan; Rachman, Faisal
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1525

Abstract

This paper has analyzed dominant zinc element in sphalerite naturally found together with galena in mineral ore. Since pyrometallurgical route related to roasting process is very common to mineral dressing, therefore, this investigation has studied the effect of varied roasting time (30 min, 60 min, and 90 min) and temperature (500oC, 600oC, and 700oC) on zinc mineral examination using XRD (X-Ray Diffraction) and zinc element using XRF (X-Ray Fluorescence) analyses. Previous studies usually applied cheaper AAS (Atomic Absorption Spectrometer) for zinc analysis in aqueous solution, however, sphalerite is a solid matrix and therefore, this study has applied XRF to analyze zinc. Pyrometallurgical process of zinc mineral in sphalerite is related to mineral transformation in the form of ZnSO4, ZnS, and ZnO that cannot be detected by XRF. Therefore, this study has used XRD that can observe mineral transformation.   The XRD pattern shows four intense peaks at 2θ (28o, 47o, 56o, and 76o) justified sphalerite (ZnS) sample with little amount of pyrite (FeS2) and galena (PbS) as impurities. The XRF analysis shows from 30 min to 90 min, the Zn content has increased remarkably at 700oC and Zn content looked stagnant at 500oC, while Zn content increased dramatically from 60 min to 90 min at 600oC. During roasting process at high temperature, ZnS mineral converted to ZnO and expelled SO2 gas due to oxidation reaction causing weight reduction. The study is valuable for mineral processing in searching for optimization.
Co-Authors Afiat Anugrahadi Afiat Anugrahadi, Afiat Ananta Ihza Hiswara, M Mirza Andry Prima Aqlyna Fattahanisa Arinda Ristawati Aryandi, Firman Aryanto, Reza Azizi, Masagus Ahmad Chairul Nas Damarizky, Rico Darren, Franko Sajow Devin Indra Novega Dewandaru, Sawung Panggali Dina Asmaul Chusniyah Dolfina Kilmas, Theresia Emmy Fatmi Budhya Fachry Abda El Rahman Fadliah Fadliah Fadliah Fadliah, Fadliah Fadliah, Fadliah Faisal Rachman Faldo Matulessy Feni Maulindani, Sri Firman Aryandi Fitra Yuda, Himmes Hadi Purnomo Hari Karyadi Oetomo, R. Harin Widiyatni Hartono, Kartika Fajarwati Havidh Pramadika Himmes Fitra Yuda iputu rama aryawan Irfan Marwanza Kalasnikova Suparmanto , Albert kartika fajarwati hartono Kurniawan Saputra, Ade Lailatul Wastiyah Lie, Nobel Alief Maulani, Mustamina Maulindani, Sri Feni Muhammad Napis Fikri Mustamina Maulani Nas, Chairul Nugraeni, Crhistine Dyta Nugraheni, Rosmalia Nur Hayati Palit, Christin Patian, Syamidi Pauhesti, Pauhesti Puri Wijayanti, Puri Puspitosari, Meldinar Riska Raihan Azica , Muhammad Reno Pratiwi Reno Pratiwi Ridaliani Prapansya, Onnie Ristawati, Arinda Rosmalia Nugraheni Said, Ardhia Regita Cahyani Samura, Lisa Saputra, Ade Kurniawan Septiano, Michael Shima Parameswari Adji Siahaan, Muhammad Dian Syahputra Subandrio Subandrio Subandrio, Subandrio Suherman Dwi Nuriana Suherman Dwi Nuryana Suliestyah Suliestyah, Suliestyah Sumotarto, Untung Sundari, Rita Sunny Yulia, Prayang Syamidi Patian Syamidi Patian Syarif, Iif Ahmad Taat Tri Purwiyono Tuheteru, Edy Jamal Untung Sumotarto Wastiyah, Lailatul Wayan Nanik Juliantari, Ni Wiwik Dahani Wiwik Dahani Wiwik Dahani Wiwik Dahani Wiwik Dahani wiwik dahani, wiwik Yulia, Prayang Sunny Yulianti, Ririn ‘Adany, Fildzah