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Non Dispersive Chemical Deacidification of Crude Palm Oil in Hollow Fiber Membrane Contactor Purwasasmita, Mubiar; Nabu, Eryk Bone Pratama; Khoiruddin, K.; Wenten, I Gede
Journal of Engineering and Technological Sciences Vol 47, No 4 (2015)
Publisher : ITB Journal Publisher, LPPM ITB

Performance of chemical deacidification of crude palm oil (CPO) using aqueous NaOH solution in a polysulfone hollow fiber ultrafiltration membrane wasÂ investigated. The effects of operating temperature, NaOH concentration and flow rates on percentage of free fatty acids (FFA) removal, oil loss, soap entrainment and overall mass transfer coefficientÂ wereÂ evaluated. Overall mass transfer coefficients, soap content in oil and neutral oil loss all increasedÂ when theÂ temperatureÂ was increased from 60 to 70Â°C due to an increase of the FFA distribution value. A minimum 0.25 N of NaOH or a NaOH to FFAÂ molar ratioÂ of about 7.62 wasÂ required to facilitate the expected extraction efficiency. The increased oil flowrate slightly enhanced the solute transport kinetics,Â while theÂ aqueous phase flowrate did not significantly influence deacidification efficiency or mass transfer coefficient. About 97% of FFA removal was achieved within 4 hours. The maximum oil loss observed was 11% and the highestÂ soap content in theÂ oil without separation step was 3150 ppm. The valuesÂ of theÂ overall mass transfer coefficient variedÂ from 2.97Ã10-7 to 7.71Ã10-7 m/s. These results show the potential of using the non dispersive membrane contacting process for chemical deacidification of CPO as well as other vegetable oils.

Investigation of Electrochemical and Morphological Properties of Mixed Matrix Polysulfone-Silica Anion Exchange Membrane Khoiruddin, Khoiruddin; Wenten, I Gede
Journal of Engineering and Technological Sciences Vol 48, No 1 (2016)
Publisher : ITB Journal Publisher, LPPM ITB

Mixed matrix anion exchange membranes (AEMs) were synthesized using dry-wet phase inversion. The casting solutions were prepared by dispersing finely ground anion-exchange resin particles in N,N-dimethylacetamide (DMAc) solutions of polysulfone (PSf). Subsequently, nanosilica particles were introduced into the membranes. The results show that evaporation time (tev) and solution composition contributed to membrane properties formation. A longer tev produces membranes with reduced void fraction inside the membranes, thus the amount of water adsorbed and membrane conductivity are reduced. Meanwhile, the permselectivity was improved by increasing tev, since a longer tev produces membranes with a narrower channel for ion migration and more effective Donnan exclusion. The incorporation of 0.5 %-wt nanosilica particles into the polymer matrix led to conductivity improvement (from 2.27 to 3.41 mS.cm-1). This may be associated with additional pathway formation by hydroxyl groups on the silica surface that entraps water and assists ion migration. However, at further silica loading (1.0 and 1.5 %-wt), these properties decreased (to 1.9 and 1.4 mS.cm-1 respectively), which attributed to inaccessibility of ion-exchange functional groups due to membrane compactness. It was found from the results that nanosilica contributes to membrane formation (increases casting solution viscosity then reduces void fraction) and membrane functional group addition (provides hydroxyl groups).

Impurity Removal of Waste Cooking Oil Using Hydrophobic Polypropylene Hollow Fiber Membrane Aliwarga, Lienda; Widodo, Setyo; Suwardana, Novika; Darmawan, Hanna; Khoiruddin, Khoiruddin; Wenten, I Gede
Journal of Engineering and Technological Sciences Vol 51, No 2 (2019)
Publisher : ITB Journal Publisher, LPPM ITB

Removal of impurities from cooking oil is an important step in providing the possibility of WCO reuse to extend the life cycle of cooking oil, leading to a reduction of WCO disposal. This study was conducted to investigate the performance of a polypropylene (PP) hollow fiber ultrafiltration (UF) membrane for removal of impurities from WCO. The results showed that the membrane could remove water content up to 95% (at 0.1 MPa and 30 °C), but the color improvement was only 9.5% as indicated by the absorbance reduction. Within the range of the operation conditions (i.e. a trans-membrane pressure of 0.1-0.2 MPa and a temperature of 30-50 °C), the oil flux varied from 0.3 L.m‑2.h‑1 to 1.3 L.m-2.h-1. In long-term operation, the membrane wettability was improved as shown by the oil contact angle decreasing from 28.2 ± 1.5° to 14.4 ± 0.5°. This resulted in a higher oil flux. At the same time, the hydrophobicity was also increased, as indicated by an increase in the water contact angle from 95.4 ± 0.7° to 97.3 ± 1.1°.

Non Dispersive Chemical Deacidification of Crude Palm Oil in Hollow Fiber Membrane Contactor Mubiar Purwasasmita; Eryk Bone Pratama Nabu; K. Khoiruddin; I Gede Wenten
Journal of Engineering and Technological Sciences Vol. 47 No. 4 (2015)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2015.47.4.6

Performance of chemical deacidification of crude palm oil (CPO) using aqueous NaOH solution in a polysulfone hollow fiber ultrafiltration membrane was investigated. The effects of operating temperature, NaOH concentration and flow rates on percentage of free fatty acids (FFA) removal, oil loss, soap entrainment and overall mass transfer coefficient were evaluated. Overall mass transfer coefficients, soap content in oil and neutral oil loss all increased when the temperature was increased from 60 to 70°C due to an increase of the FFA distribution value. A minimum 0.25 N of NaOH or a NaOH to FFA molar ratio of about 7.62 was required to facilitate the expected extraction efficiency. The increased oil flowrate slightly enhanced the solute transport kinetics, while the aqueous phase flowrate did not significantly influence deacidification efficiency or mass transfer coefficient. About 97% of FFA removal was achieved within 4 hours. The maximum oil loss observed was 11% and the highest soap content in the oil without separation step was 3150 ppm. The values of the overall mass transfer coefficient varied from 2.97Ã—10-7 to 7.71Ã—10-7 m/s. These results show the potential of using the non dispersive membrane contacting process for chemical deacidification of CPO as well as other vegetable oils.

Investigation of Electrochemical and Morphological Properties of Mixed Matrix Polysulfone-Silica Anion Exchange Membrane Khoiruddin Khoiruddin; I Gede Wenten
Journal of Engineering and Technological Sciences Vol. 48 No. 1 (2016)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2016.48.1.1

Mixed matrix anion exchange membranes (AEMs) were synthesized using dry-wet phase inversion. The casting solutions were prepared by dispersing finely ground anion-exchange resin particles in N,N-dimethylacetamide (DMAc) solutions of polysulfone (PSf). Subsequently, nanosilica particles were introduced into the membranes. The results show that evaporation time (tev) and solution composition contributed to membrane properties formation. A longer tev produces membranes with reduced void fraction inside the membranes, thus the amount of water adsorbed and membrane conductivity are reduced. Meanwhile, the permselectivity was improved by increasing tev, since a longer tev produces membranes with a narrower channel for ion migration and more effective Donnan exclusion. The incorporation of 0.5 %-wt nanosilica particles into the polymer matrix led to conductivity improvement (from 2.27 to 3.41 mS.cm-1). This may be associated with additional pathway formation by hydroxyl groups on the silica surface that entraps water and assists ion migration. However, at further silica loading (1.0 and 1.5 %-wt), these properties decreased (to 1.9 and 1.4 mS.cm-1 respectively), which attributed to inaccessibility of ion-exchange functional groups due to membrane compactness. It was found from the results that nanosilica contributes to membrane formation (increases casting solution viscosity then reduces void fraction) and membrane functional group addition (provides hydroxyl groups).

Impurity Removal of Waste Cooking Oil Using Hydrophobic Polypropylene Hollow Fiber Membrane Lienda Aliwarga; Setyo Widodo; Novika Suwardana; Hanna Darmawan; Khoiruddin Khoiruddin; I Gede Wenten
Journal of Engineering and Technological Sciences Vol. 51 No. 2 (2019)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2019.51.2.5

Removal of impurities from cooking oil is an important step in providing the possibility of WCO reuse to extend the life cycle of cooking oil, leading to a reduction of WCO disposal. This study was conducted to investigate the performance of a polypropylene (PP) hollow fiber ultrafiltration (UF) membrane for removal of impurities from WCO. The results showed that the membrane could remove water content up to 95% (at 0.1 MPa and 30 °C), but the color improvement was only 9.5% as indicated by the absorbance reduction. Within the range of the operation conditions (i.e. a trans-membrane pressure of 0.1-0.2 MPa and a temperature of 30-50 °C), the oil flux varied from 0.3 L.m"‘2.h"‘1 to 1.3 L.m-2.h-1. In long-term operation, the membrane wettability was improved as shown by the oil contact angle decreasing from 28.2 ± 1.5° to 14.4 ± 0.5°. This resulted in a higher oil flux. At the same time, the hydrophobicity was also increased, as indicated by an increase in the water contact angle from 95.4 ± 0.7° to 97.3 ± 1.1°.

Long-Term Performance of a Pilot Scale Combined Chemical Precipitation-Ultrafiltration Technique for Waste Brine Regeneration at Chevron Steam Flooding Plant I Gede Wenten; Khoiruddin Khoiruddin; Ahmad Nurul Hakim; Putu T.P. Aryanti; Nengsi Rova
Journal of Engineering and Technological Sciences Vol. 52 No. 4 (2020)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2020.52.4.4

In this work, chemical precipitation-ultrafiltration (UF) was applied for waste brine regeneration from a steam flooding plant at Duri Field, Chevron. A mixture of sodium hydroxide and sodium carbonate solution was used as chemical agent. A polypropylene (PP) UF membrane was used to remove precipitate formed in the chemical precipitation. It was found that the combined process could be used to regenerate waste brine, removing up to 100% (±0.1) of calcium and up to 99.6% (±0.3) of magnesium. High hardness removal was achieved when the chemical dosage was 1.3 to 1.7 mole of chemical/mole of hardness. Rapid permeability decline was observed in the UF membrane due to the high turbidity and TSS values of the chemically treated waste brine. Backwash with an acid solution could recover the UF membrane's permeability effectively. However, pH adjustment is needed due to the high pH value of the UF permeate (up to ~12).

Membrane Oxygenator for Extracorporeal Blood Oxygenation Enny Ratnaningsih; Putu T.P. Aryanti; Nurul F. Himma; Anita K. Wardani; K. Khoiruddin; Grandprix T.M. Kadja; Nicholaus Prasetya; I Gede Wenten
Journal of Engineering and Technological Sciences Vol. 53 No. 5 (2021)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2021.53.5.2

Extracorporeal blood oxygenation has become an alternative to supply O2 and remove CO2 from the bloodstream, especially when mechanical ventilation provides insufficient oxygenation. The use of a membrane oxygenator offers the advantage of lower airway pressure than a mechanical ventilator to deliver oxygen to the patient’s blood. However, research and development are still needed to find appropriate membrane materials, module configuration, and to optimize hydrodynamic conditions for achieving high efficient gas transfer and excellent biocompatibility of the membrane oxygenator. This review aims to provide a comprehensive description of the basic principle of the membrane oxygenator and its development. It also discusses the role and challenges in the use of membrane oxygenators for extracorporeal oxygenation on respiratory and cardiac failure patients.

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