Claim Missing Document
Check
Articles

Found 40 Documents
Search

Preparation and Characterization of Cellulose Acetate from Pandanus tectorius via Microwave Irradiation Rizkiana, Meta Fitri; Amrullah, Abdul Malik Karim; Elisah, Nor; Amini, Helda Wika; Palupi, Bekti; Rahmawati, Istiqomah; Fachri, Boy Arief
Indonesian Journal of Chemical Research Vol 12 No 1 (2024): Edition for May 2024
Publisher : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2024.12-riz

Abstract

This research focuses on extracting cellulose from thorn pandan and evaluating its potential as a raw material for cellulose acetate. Thorn pandan contains polysaccharides, especially cellulose. In its fabrication process, cellulose acetate is produced from cellulose acetylation reaction. Cellulose is extracted using the Microwave-assisted Extraction method with variations in NaOH concentration (1, 2, and 3%), H2O2 concentration (10, 20, and 30%), and time variables (20, 40, and 60 minutes). Extraction optimization was performed with Response Surface Methodology (RSM) model BBD (Box-Behken Design). Several characterizations were carried out to determine the characteristics of cellulose acetate, namely Degree of Acetylation, FT-IR spectroscopy and X-Ray Diffraction (XRD). The highest cellulose yield obtained in the extraction process was 50.7% with a variable of 3% NaOH, 30% H2O2 and 60 minutes. XRD analysis shows the angle value 2θ = 22.53798° of thorn pandan cellulose structure is almost similar to commercial cellulose. FTIR functional group identification of cellulose acetate showed the presence of carbonyl (C=O) and (C-O Acetyl) group, respectively seen at wave numbers 1734 cm-1 and 1256 cm-1. The acetyl content of cellulose acetate from thorn pandan produced is 35.475%. Therefore, thorn pandan biomass has the potential as a raw material for making cellulose acetate.
Polyphenol Extraction from Musa corniculata Peel Using Microwave Assisted Extraction (MAE) Method with Ethanol Solvent Rahmawati, Istiqomah; Sa’roni, Achmad; Wardhani, Maharani Tri; Fachri, Boy Arief; Palupi, Bekti; Rizkiana, Meta Fitri; Amini, Helda Wika; Reza, Muhammad
BERKALA SAINSTEK Vol 12 No 2 (2024)
Publisher : Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/bst.v12i2.41494

Abstract

Banana peel (Musa corniculata) is one of the superior plants in Indonesia which is rich in polyphenolic compounds as a source of antioxidants. The potential of polyphenolic compounds as antioxidants can be used as an alternative to reduce banana peel waste. This study aims to determine the total content of polyphenols and antioxidant activity of horn banana peel extract. Extraction used the Microwave Assisted Extraction (MAE) method with ethanol solvent and the variables were extraction time (4, 7, and 10 minutes), solvent concentration (50, 73 and 96 %), ratio of simplicia mass to solvent volume (1:12, 1 :8, 1:6 g/mL) with a microwave power of 150 Watt. Determination of polyphenol content using the Folin-Ciocalteau method and the ability of polyphenols as antioxidants were analyzed by DPPH test. This study used the Design Expert 13 Response Surface Methodology software, the Box Behnken type, to determine the extraction parameters for the total polyphenol content. The highest total polyphenol content was obtained at 354.02 mg GAE/g from the combination of parameters 50% solvent concentration, 10 minutes extraction time, and the ratio of horn banana peel powder to 1:8 g/mL solvent.
EKSTRAKSI PROTEIN DARI SPIRULINA SP DALAM PELARUT ETANOL TERBANTUKAN GELOMBANG ULTRASONIK Boy Arief Fachri; Bekti Palupi; Istiqomah Rahmawati; Meta Fitri Rizkiana; Helda Wika Amini
Jurnal Penelitian Sains dan Teknologi Indonesia Vol 1 No 1 (2022): Jurnal Hasil Penelitian UNIVERSITAS JEMBER
Publisher : Lembaga Penelitian dan Pengabdian Kepada Masyarakat (LP2M) Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jpsti.v1i1.90

Abstract

Protein merupakan komponen nutrisi yang dibutuhkan oleh manusia untuk kesehatan tubuh. Salah satu sumber protein yang melimpah di Indonesia adalah alga Spirulina Sp. Ekstraksi protein alga, sulit dilakukan. Hal ini dikarenakan, protein tersimpan dalam sel-sel alga yang memiliki dinding yang sangat keras. Metode konvensional yang selama ini dilakukan membutuhkan waktu yang sangat lama, dan energi yang besar. Untuk mengatasi hal itu, sebuah metode alternatif yang diajukan dalam penelitian ini, adalah metode ekstraksi ultrasonik. Tujuan penelitian ini adalah untuk menentukan kondisi optimum ekstraksi protein dari Spirulina Sp dan mengetahui pengaruh parameter ekstraksi terhadap yield. Sprirulina Sp yang tekah dikeringkan dan dihaluskan diumpankan ke dalam ekstraktor yang berisi etanol. Gelombang ultrasonic, kemudian dialirkan ke dalam ekstraktor melalui probe. Setelah, eaktu ekstraksi tercapai, ekstrak dan residu dipisahkan dengan cara sentrifugasi dengan kecepatan 10000 rpm pada suhu kamar. Selanjutnya, yield protein ekstrak dihitung dengan analisa Lowry-Bradford. Pengaruh parameter proses seperti rasio bahan baku-pelarut (0:1-0.5) g/mL, ukuran partikel bahan baku (600-800) mesh dan waktu ekstraksi 15-45 menit) terhadap yield akan diamati dalam penelitian ini. Berdasarkan hasil penelitian, dapat disimpulkan bahwa yield tertinggi sebesar 80,87 % diperoleh pada kondisi rasio bahan baku-pelarut 0.2 g/mL, ukuran partikel bahan baku 700 mesh dan waktu ekstraksi 30 menit. Sementara itu, ukuran partikel merupakan parameter yang paling signifikan.
BUDIDAYA LELE DENGAN METODE BUDIKDAMBER SEBAGAI SOLUSI PENINGKATAN PRODUKTIVITAS MASYARAKAT DIKALA PANDEMI COVID- 19 Meta Fitri Rizkiana; Ditta Kharisma Yolanda Putri; Intan Hardiatama
Jurnal Hasil Pengabdian kepada Masyarakat Universitas Jember Vol 1 No 1 (2022): Jurnal Hasil Pengabdian Kepada Masyarakat Universitas Jember
Publisher : LP2M Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jpmunej.v1i1.69

Abstract

Ketidakstabilan perekonomian akibat pandemi Covid-19 semakin dirasakan dalam kehidupan masyarakat Indonesia khususnya sektor rumah tangga. Konsumsi rumah tangga, sebagai penopang utama perekonomian melambat secara signifikan, dimana mempengaruhi kinerja industri dan usaha mikro, kecil dan menengah. Seperti halnya terjadi pada mitra yaitu kelompok pedagang warung makan lesehan yang berada di Jl. Jawa sekitaran Universitas Jember. Menurunnya daya beli masyarakat, masih diberlakukannya protokol kesehatan yang mengharuskan sistem perkuliahan dilakukan online serta menurunnya pendapatan masyarakat sangat berdampak pada penjualan makanan dan mengubah pola konsumsi. Peternakan lele dengan menggunakan sistem Budikdamber yang menggabungkan antara beternak lele dengan Hidroponik sayuran kangkung dapat menjadi salah satu solusi untuk menunjang perekonomian di kala pandemi Covid-19. Sistem Budikdamber (Budidaya ikan dalam ember) plus akuatik ini adalah membudidayakan ikan dan sayuran dalam satu ember yang merupakan sistem akuaponik (polikultur ikan dan sayuran). Tujuan dari pengabdian masyarakat ini adalah diharapkan sistem budidaya ikan dan sayuran ini dapat meningkatkan ekonomi masyarakat dan menjaga ketahanan pangan dikala pandemi. Metode pelaksanaan berupa pembinaan dan pelatihan dari akademisi Universitas Jember. Kegiatan pengabdian yang dilaksanakan direspon dengan baik oleh masyarakat terlihat dari antusiame dan peran aktifnya dalam pembuatan wadah dan media tanam Budikdamber.
OPTIMASI EKSTRAKSI SENYAWA FENOLIK DAUN SIRIH MERAH (Piper Crocatum Ruitz & Pav) MENGGUNAKAN METODE MICROWAVE ASSISTED EXTRACTION (MAE) Amini, Helda Wika; Nugroho, Yeremia Prasetya; Rahman, Agus; Rizkiana, Meta Fitri; Rahmawati, Istiqomah; Palupi, Bekti; Fachri, Boy Arief
Dalton : Jurnal Pendidikan Kimia dan Ilmu Kimia Vol 7, No 3 (2024)
Publisher : Universitas Islam Kalimantan MAB Banjarmasin

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31602/dl.v7i3.16431

Abstract

Karena efek samping yang lebih sedikit daripada pengobatan sintetik, pengobatan menggunakan bahan alami menjadi pilihan populer di Indonesia. Oleh karena itu, diperlukan penelitian lebih lanjut mengenai bahan alami yang dapat digunakan sebagai obat, salah satunya adalah sirih merah. Penelitian ini bertujuan mengetahui kondisi optimal untuk mengekstraksi senyawa fenolik daun sirih merah dengan menggunakan metode Microwave Assisted Extraction (MAE). Penelitian ini menggunakan daun sirih merah ukuran 60 mesh yang telah dikeringkan. Dengan pelarut etanol 96%, daun sirih merah diekstraksi dengan variabel daya microwave 150 watt, 300 watt, dan 450 watt. Rasio bahan terhadap pelarut adalah 0,05 gram/mL, 0,1 gram/mL, dan 0,15 gram/mL. Ekstraksi berlangsung selama 5-15 menit. Analisis hasil penelitian dilakukan dengan analisis total fenol menggunakan metode Folin-Ciocalteu. Pada run ke-8, total fenol tertinggi adalah 0,0736 mg GAE/g, dengan rasio pelarut 0,05 g/mL, waktu ekstraksi 5 menit, dan daya microwave 300 watt.
Pelet Unggul: Inovasi Teknologi Tepat Guna dari Sampah untuk Peningkatan Produktivitas Ternak Lele di Lamigot Ys Farm Pakusari Palupi, Bekti; Rahmawati, Istiqomah; Rizkiana, Meta Fitri; Rafif, M. Attar; Tarigan, Eigiya Nina; Herdianto, Dimas Nur; Yohanes, Yohanes; Shofiah , Laila Nur
Sewagati Vol 9 No 1 (2025)
Publisher : Pusat Publikasi ITS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12962/j26139960.v9i1.2488

Abstract

Sektor peternakan dan perikanan merupakan pilar utama ketahanan pangan di Indonesia, dengan budidaya ikan lele menjadi pilihan utama karena kemudahannya dan tingginya konsumsi oleh masyarakat. Data BPS Jawa Timur menunjukkan peningkatan produksi ikan lele dari 127.539 ton pada tahun 2020 menjadi 136.437 ton pada tahun 2021. Namun, masalah utama yang dihadapi peternak, khususnya skala kecil dan menengah seperti UMKM Lamigot YS Farm di Kabupaten Jember, adalah mahalnya harga pelet pakan ikan. Untuk mengatasi kendala ini, program pengabdian masyarakat ini menawarkan solusi berupa pengembangan Teknologi Tepat Guna (TTG) dengan menciptakan mesin pencetak pelet menggunakan bahan baku sampah organik. Solusi ini bertujuan untuk mengurangi biaya produksi, mendukung pengelolaan limbah berkelanjutan, dan meningkatkan produktivitas serta kemandirian peternak. Kegiatan ini meliputi sosialisasi, pelatihan, dan pendampingan teknis, diharapkan dapat meningkatkan pemahaman dan keterampilan peternak dalam memproduksi pelet pakan ikan secara mandiri. Dari hasil pengamatan selama 2 minggu, lele yang diberi pelet sampah organik bertambah massanya menjadi 9 gram, sementara yang diberi pelet komersial hanya memiliki massa 8,3 gram. Hal ini menunjukkan bahwa inovasi pelet dari sampah organik memiliki kualitas yang lebih baik daripada pelet komersial sehingga layak dikembangkan.
The Optimization of Chlorophyll Extraction from Ulva Sp. with Ultrasound-Assisted Liquid Biphasic Systems Method Susilowati; Fakhri Arkaan Humaidi; Boy Fachri; Bekti Palupi; Meta Fitri Rizkiana; Istiqomah Rahmawati; Helda Wika Amini
Indonesian Journal of Science and Education Vol. 8 No. 1 (2024): Indonesian Journal of Science and Education
Publisher : Universitas Tidar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31002/ijose.v8i1.1085

Abstract

Ulva sp. is a type of green algae that is easily found in the shallow seas of Indonesia and contains various bioactive compounds. Chlorophyll is a bioactive compound that functions as a natural dye, free radical scavenger, and antioxidant in the body. Chlorophyll extraction with conventional methods requires a relatively long time and large amount of solvent. In this research, chlorophyll extraction from Ulva sp. with the Ultrasound-Assisted Liquid Biphasic System (UALBS) method. Ulva sp. as much as 2.5 grams mixed in acetone solvent, added K2HPO4 solution, and carried out the sonification process in a dark room. The extraction process performs at a parameter range of 5-15 minutes, ratio 0.05-0.1 g/mL, and 60-100 mesh particle size. The extracted filtrate was added with petroleum ether and distilled water to form a biphasic condition. The extracted chlorophyll was analyzed with chromatography and spectrophotometry method. Antioxidant activity was analyzed using the DPPH method. The optimum result of Ulva sp. chlorophyll extraction at an extraction time of 10 minutes, the ratio of solids to solvent was 0.1, the particle size of 60 mesh produced a yield of 1.88% with chlorophyll a 20.13664%, chlorophyll b 21.58672% and total chlorophyll 41.71012%, and the percentage inhibition 45.32%.
Pelatihan Pembuatan Pupuk Organik Cair dari Limbah Kulit Kopi di Desa Pakis Jember Amini, Helda Wika; Rizkiana, Meta Fitri; Palupi, Bekti; Hidayati, Nurul; Raharjo, Sonya Hakim; Nurani, Yukti; Aziz, Mohamad Naufal Nizaar; Saputri, Ocha; Permatasari, Intan; Fandora, Ardan Jauza; Adriansyah, Muhamad; Nurjannah, Lailia; Rachman, Darryl Akeyla; Firmansyah, Alex; Devara, Arighy Zahirah Faiqy; Ulfiani, Khoirun Nisya'
JURNAL TEPAT : Teknologi Terapan untuk Pengabdian Masyarakat Vol 8 No 1 (2025): Community Empowerment through Higher Education Community Service Programs
Publisher : Faculty of Engineering UNHAS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25042/jurnal_tepat.v8i1.583

Abstract

Indonesia is one of the largest coffee-producing countries in the world. Indonesia recorded a large coffee harvest capacity reaching 774.96 thousand tons in 2022. The coffee processing naturally results in coffee hull waste that continues to be produced in large quantities. About 40 to 48% of the coffee hull composition contained in a coffee cherry is often discarded during processing and is not optimally utilized. One sustainable solution that can be implemented is processing coffee hull waste into liquid organic fertilizer (POC) through fermentation with EM4. This community service program was implemented in Pakis Village, Panti District, Jember Regency, which has 441.40 hectares of coffee plantations with an annual production of around 1,200 tons of robusta coffee. The program includes bioreactor development, socialization, and training for the community regarding the processing of coffee hull waste into POC. The result is increased community knowledge and skills as well as economic benefits for coffee farmers in Pakis Village through improved soil productivity. The results of the activities showed that the clarity of the knowledge with community needs increased to 70%, public interest in POC activities increased to 85%, and resulted in public satisfaction of 95%.
Microwave-Assisted Deep Eutectic Solvent Extraction of Lipids from Ulva sp.: Optimization and Fatty Acid Profiling Rizkiana, Meta Fitri; Lestari, Afrila Tutut Dwijati; Sholeha, Irdatus; Palupi, Bekti; Putri, Ditta Kharisma Yolanda; Rahmawati, Istiqomah; Amini, Helda Wika; Fachri, Boy Arief
Jurnal Pijar Mipa Vol. 20 No. 5 (2025)
Publisher : Department of Mathematics and Science Education, Faculty of Teacher Training and Education, University of Mataram. Jurnal Pijar MIPA colaborates with Perkumpulan Pendidik IPA Indonesia Wilayah Nusa Tenggara Barat

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpm.v20i5.9588

Abstract

Ulva sp. is a green alga commonly found in Indonesian waters. It contains approximately 60% carbohydrates, 10–47% protein, and 1–3% lipids. This study aimed to determine the optimum conditions for lipid extraction from Ulva sp. A pre-treatment step was carried out by adding a Deep Eutectic Solvent (DES) and distilled water. The DES used was a mixture of zinc chloride and urea in a 1:2 molar ratio. The sample was then mixed with a chloroform-methanol solvent (2:1 v/v) and subjected to Microwave-Assisted Extraction (MAE). The variables investigated in this study included microwave power (150, 300, and 450 W), extraction time (10, 15, and 20 min), and solvent volume (45, 60, and 75 mL). The organic phase obtained from the extraction process was separated and evaporated to determine the lipid yield. The highest yield, 15.8%, was achieved under conditions of 20 min extraction time, 75 mL solvent volume, and 300 W of power. GC-MS analysis of the highest-yield sample revealed the presence of fatty acids including palmitic acid, oleic acid, and palmitoleic acid. This optimized method supports future applications in biodiesel production and green extraction processes for algae-based bioresources.
The Optimization of Chlorophyll Extraction from Ulva Sp. with Ultrasound-Assisted Liquid Biphasic Systems Method Susilowati; Humaidi, Fakhri Arkaan; Fachri, Boy; Palupi, Bekti; Rizkiana, Meta Fitri; Rahmawati, Istiqomah; Amini, Helda Wika
Indonesian Journal of Science and Education Vol. 8 No. 1 (2024): Indonesian Journal of Science and Education
Publisher : Universitas Tidar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31002/ijose.v8i1.1085

Abstract

Ulva sp. is a type of green algae that is easily found in the shallow seas of Indonesia and contains various bioactive compounds. Chlorophyll is a bioactive compound that functions as a natural dye, free radical scavenger, and antioxidant in the body. Chlorophyll extraction with conventional methods requires a relatively long time and large amount of solvent. In this research, chlorophyll extraction from Ulva sp. with the Ultrasound-Assisted Liquid Biphasic System (UALBS) method. Ulva sp. as much as 2.5 grams mixed in acetone solvent, added K2HPO4 solution, and carried out the sonification process in a dark room. The extraction process performs at a parameter range of 5-15 minutes, ratio 0.05-0.1 g/mL, and 60-100 mesh particle size. The extracted filtrate was added with petroleum ether and distilled water to form a biphasic condition. The extracted chlorophyll was analyzed with chromatography and spectrophotometry method. Antioxidant activity was analyzed using the DPPH method. The optimum result of Ulva sp. chlorophyll extraction at an extraction time of 10 minutes, the ratio of solids to solvent was 0.1, the particle size of 60 mesh produced a yield of 1.88% with chlorophyll a 20.13664%, chlorophyll b 21.58672% and total chlorophyll 41.71012%, and the percentage inhibition 45.32%.
Co-Authors Abdul Malik Karim Amrullah Abdur Rohman Achri Isnan Khamil Adinda Yufriza Adrian, Febri Adriansyah, Muhamad Afwal, Diza Raudhatul Aina Christalia Rinastiti Amal Bahariawan Andreyan Poerwo Negoro Anggraini, Ranita Anggi Annisa, Yasmin Ari Susanti Ari Susanti Ari Susanti Ariel Seanhan Haezer Atiqa Rahmawati Atiqa Rahmawati Aziz, Mohamad Naufal Nizaar Badril Azhar Bekti Palupi Bimo Bayu Aji Boy Arief Fachri Boy Fachri Devara, Arighy Zahirah Faiqy Dianita Ivana Permata Dini Rahmawaty Ditta Kharisma Yolanda Putri Elisah, Nor Fachri, Boy Fakhri Arkaan Humaidi Fandora, Ardan Jauza Faqih, Hana Farwah, Zilma Aliyah Felix Arie Setiawan Firmansyah, Alex Firsta Retnaningtyas Udroto Gregah Pangayoman Hartanto P Habib Ihza Mahendra Habibatul Inayah Harti Arini Helda Wika Amini Helda Wika Amini Herdianto, Dimas Nur Humaidi, Fakhri Arkaan Husna Wardati Indrayani, Lilin Intan Hardiatama Intan Permatasari Istiqomah Rahmawati Istiqomah Rahmawati Iswahyono Iswahyono Joseph Dwi Kurniawan Manno Kenji Sakai Kenji Sanomoto Lailatul Krisna Abdullah Lestari, Afrila Tutut Dwijati Maharani, Regita Gustiayu Pramisti Maktum Muharja Mizanurafi’ Ghifarhadi Prasiefa Mohammad Nor Muhammad Ilham Muhammad Reza Muhammad Reza Muharja, Maktum Nanda Ayudiyah Andriani Nikita Meidi Nugraha, Reva Edra Nugroho, Yeremia Prasetya Nurani, Yukti Nurjannah, Lailia Nurtsulutsiyah Nurtsulutsiyah Nurtsulutsiyah Nurtsulutsiyah Nurtsulutsiyah, Nurtsulutsiyah Nurul Hidayati Pradipta, Shima Nuril Putri Agustin, Mawardhi Nabilla Rachman, Darryl Akeyla Rafif, M. Attar Rahman, Agus Rahmawati, Atiqa Raygita May Hastuti Regita Gustiayu Pramisti Maharani Reswara Musyafa Retno Utami Agung Wiyono Rizalluddin, Muhammad Rizki Fitria Darmayanti Rizki Fitria Darmayanti Rizki Fitria Darmayanti Rohmah, Fira Ulvatur Sakai, Kenji Sanomoto, Kenji Santosa, Iliya Kartika Saputri, Ocha Sa’roni, Achmad Septianti, Kiki Shabrina, Nadhilah Shofiah , Laila Nur Sholeha, Irdatus Siska Nuri Fadilah Siti Djamila Sonya Hakim Raharjo Susilowati Susilowati Tarigan, Eigiya Nina Tashiro, Yukihiro Ulfiani, Khoirun Nisya' Viqhi Aswie Wardani, Salza Belila Kusuma Wardhani, Maharani Tri Wiwik Pratiwi Yakub Hendrikson Manurung Yohanes Yohanes Yukihiro Tashiro Zuhriah Mumtazah