Claim Missing Document
Check
Articles

Found 19 Documents
Search
Journal : Alotrop Jurnal Pendidikan dan Ilmu Kimia

Pembuatan Biofuel dari Limbah Cair PMKS dengan Katalis MoCo-HZ Tyas Sri Muryati; Agus Sundaryono; Dewi Handayani
ALOTROP Vol 2, No 2 (2018)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v2i2.7486

Abstract

This research aims to convert vegetable oils contained in Palm Oil Mill waste (PMKS) into biofuels through the cracking process with MoCo-HZ catalyst . PMKS Liquid waste will be prepared with a process of a filtering, degumming, bleaching, warming, and free Fatty Acids determination.  The results obtained are then converted into biofuel with catalytic cracking with use of MoCo-HZ catalyst . Then the cracking products will to test for specified physical characteristics of biofuel eq : acid number , density, viscosity, pour point and cloud point. . The research results showed that the MoCo-HZ catalyst is able to convert vegetable oils contained in the PMKS liquid waste will be cracked into biofuel. Conversion yield obtained is amounting to 48.19%. The physical characteristics of the test results against biofuels produced from the cracking process has not met the standard of comparison from gasoline and kerosene. This is shown by the still high number of biofuel produced acids amounting to 1.72 mg KOH/gr. higher than the numbers of  sour gasoline (0.748 mg KOH/gr) and Kerosene (0.935 mg KOH/gr). The result of the test of density, viscosity, pour point and cloud point against biofuels produced from the cracking process have meet standard compared to gasoline and kerosene respectively 0.807 gr/cm for density, 1.056 cSt viscosity for viscosity , and 0 º C and 1.33 each º C to the freezing point and the cloud point..
UJI FRAKSI ETIL ASETAT DAUN Peronema canescens TERHADAP Plasmodium berghei PADA Mus musculus Fuji Ramadenti; Agus Sundaryono; Dewi Handayani
ALOTROP Vol 1, No 2 (2017)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v1i2.3508

Abstract

[DETERMINATION OF ETHYL ACETATE FRACTION FROM Peronema canescens LEAF EXTRACT  AGAINST Plasmodium berghei  INFECTED  Mus musculus] This study was conducted to identify secondary metabolite compounds contained in ethanol extract and ethyl acetate fraction from Peronema canescens leaf (sungkai) and to measure the effect of ethyl acetate fraction on anti plasmodium  activity on Mus musculus infected by  Plasmodium berghei. The ethyl acetate extract was obtained by maceration of leaves with 96% ethanol solution in3 days followed by fractionation by ethyl acetate for further test. 25 of male white  M. musculus  with the weight 20-40 g and 6-8 weeks old , divided into 5 groups with 5 head / group. Groups 3, 4 and 5 are treated and groups 1 and 2 are controls. The negative control will be given food and drink only, and for positive control group will be given chloroquine with dose  0,028,  0,056, and  0,084 g / KgBW.  Development of levels of parasitemia were calculated by by observing a thin blood smear with giemsa staining under a microscope , observed until the parasitemia in the blood had reached 20-30% to be given a 3-day follow-up treatment, and then for the next 7 days after it was given treatment.. Anti-plasmodium activity test is determined by the number of parasitemia, percent growth and resistance of parasitemia in the blood. Data were analyzed by using one way anova method (? = 0,05 and 0,01). The results showed that the secondary metabolite compounds found in the ethyl acetate fraction of  P.canescens leaf, namely alkaloids, flavonoids, tannins and phenolics and at a dose of 0.056 g / KgBW  ethyl acetate fraction  can inhibit the growth of parasitemia in the blood of  M. musculus by 50 , 89% , with greater percentage of parasitemic inhibition compared with positive and negative control group.
Preparasi dan Karakterisasi Katalis Mo-Ni/HZ dengan Metode Impregnasi untuk Cracking Katalitik Minyak Limbah Cair Pengolahan Kelapa Sawit menjadi Bahan Bakar Nabati Shinta Lestari; Agus Sundaryono; Rina Elvia
ALOTROP Vol 3, No 1 (2019)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v3i1.9047

Abstract

This study aims to determine the characteristics of Mo-Ni/HZ catalysts and test the ability of Mo-Ni/HZ catalysts in converting vegetable oils into biofuels through catalytic cracking reactions.Catalyst preparation is carried out by the impregnation method which begins with activation of natural zeolite.Impregnation is carried out by dissolution, reflux, filtration, drying and calcination.Catalyst characterization included the determination of the distribution of metals in zeolites using IR spectroscopic analysis and total acidity of the catalyst by ammonia adsorption gravimetric method.Preparation of samples prior to cracking is heating, degumming and bleaching.Catalytic cracking was carried out at 280oC using Mo-Ni/HZ catalyst for 100 minutes.The constituent components of the cracking results were analyzed by GC-MS and IR spectroscopy.The results obtained from the catalytic cracking process were then determined by physical characteristics which included density, viscosity, fog point and pour point test.Based on the shift of wave number in IR spectroscopy, it can be concluded that the Ni and Mo metals are embedded in the HZ.This Mo-Ni/HZ catalyst has total acidity of 8.39 mmol/gammonia.The results of the study prove that the Mo-Ni/HZ experiment proved to be able to crack oil frompalm oil processing wastewater by 91.46% to composition C=O ester CH aliphatic.The physical characteristics of cracking productshave parameters density of 0.93 g/cm3, a viscosity of 26.60 cSt, a fog point of 15oC and pour point of 11.67oC.
PENGEMBANGAN E-MODUL KIMIA BERBASIS METAKOGNISI MENGGUNAKAN APLIKASI EDMODO Shiba Meike Indira; Agus Sundaryono; Rina Elvia
ALOTROP Vol 4, No 1 (2020)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v4i1.13707

Abstract

Metacognition is one of the factors that influence academic achievement, so it is very important in each student's learning activities. The objective of this research was to find out the level of feasibility and students response to E-chemistry-based metacognition using the edmodo application as teaching material to train students' knowledge and metacognition experience of students of the XI MIPA class of SMA Negeri 2 Kota Bengkulu T/P 2018/2019 on acid-base material. This research was an Research & Development (R&D) using the 4D development model limited to the development stage. The development of this emodule uses the edmodo application and in its using the flipped classroom learning model. Information worthy of being used as teaching of expert assessments and student responses to limited testing and field testing. The assessment of e-module was carried out by media experts, it was obtained that e-module is very feadible to use without revision with an evaluation percentage of 93%, an assessment by material experts and practitioners ( chemistry teacher) was very feasible to use without revision with an evaluation percentage of 92%, then the metacognition –based was assessed by material experts was obtained e- module was very feasible to use without revision with a percentage of 88% so that based on the results of expert evaluations, e-module could testedon a limited trial class and field trial. Sample selection in limited trials and field trials obtained from the results of normality tests conducted on january 3,2019 from the popuation of class XI Mipa A- XI Mipa F as many 190 students obtained 15 students XI Mipa C as samples ini limited trials and 31 students XI Mipa E in the field trial. Response of students in limited trials carried out on january 14,2019 and field tests on january 30,2019 amounting to 86% and 84% this shows that the use of emodules is very teasible to use as teaching materials and obtained information that e-module can train the ability of metacognition students of the XI MIPA SMA Negeri 2 Kota Bengkulu T/P 2018/2019 in particular the knowledge and metacognition experience of student from less trained to being trained.
KARAKTERISASI NANOPARTIKEL KITOSAN EKSTRAK DAUN UBIJALAR (Ipomoea batatas L.) MENGGUNAKAN METODE GELASI IONIK Ade Indriani Putri; Agus Sundaryono; I Nyoman Chandra
ALOTROP Vol 2, No 2 (2018)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v2i2.7561

Abstract

The purpose of this study is to determine and measure the results of the characterization of Chitosan nanoparticle synthetized from leaves of sweet potato (Ipomoea batatas l.) extracts . The methods used to make nanoparticles is made with Ionic Gelation method based on electrostatic interaction between the Hydroxyl Amine on Chitosan with cluster of negative charge from the polianion NaTPP with conditioned surfactant Tween 80 used as surfactant. Characterization test of nanoparticle morphology in this study obtained using the Fourier Transformation  Infra Red (FTIR), and Particle Size Analyzer (PSA). Results with FTIR characterization test from the obtained Chitosan-white purple sweet potato leaf extract nanoparticles has a cluster of N-H and P = O that show the occurrence of ammonium ion interaction between Chitosan with polianion from NaTPP and sweet potato leaves. The interaction seen from wave number and intensities  O-H shifting from pure Chitosan at 3425.56 cm-1 to 3427, 51 cm-1, as well as on pure Chitosan N-H absorption  undergoes a shift from 1597, 06 cm-1 to becomes 1629.85-1 cm-1, which shows that there has been a cross connective between ammonium ion on Chitosan and Posphat from NaTPP and white purple sweet potato leaf extract. The results of the analysis from the PSA, is known to the average Nanokitosan particle sizes extracts from white purple sweet potato leaf extracts with the addition of NaTPP i.e. of 302.6 nm and that the aim of the research on Chitosan nanoparticle synthesis has been successfully done.
EKSTRAKSI METABOLIT SEKUNDER DAN UJI ANTIOKSIDAN DARI DAUN MEDANG PERAWAS (Litsera Odorifera val) DENGAN METODE 1,1-DIPHENYL 2-PICRYLHIDRAZYL (DPPH) I Nyoman Candra; Theo Kuntara; Agus Sundaryono
ALOTROP Vol 6, No 1 (2022)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/alo.v6i1.22398

Abstract

Litseaodoriferaval.(MedangPerawas) is well recognized in Muko-Mukoregency, Bengkulu Province and used as construction material. In Serawai and Lembak Ethnic groups, it is traditionally used as medication for mouth sprue, stomachache,and boil as well as used for inducing lactation. This research aims to extract secondary metabolite compound group contained in Litseraodorifera val. leaf and to examine its antioxidant activity potency against 1,1-diphenyl 2-picrylhidrazyl (DPPH). A Fresh leaves from Litseraodorifera val. collected from Tahura Forest, Central Bengkulu area were separated into two parts: one run into chemical screeningand the second was used for extraction experiment using ethanol, ethyl acetate, hexane and acetone. Secondary metabolite compound groups contained in those extracts were tested for antioxidantactivity potency. The results showed that the extract of Litseraodorifera val. leaf contained compound group of flavonoid, saponin, tannin, phenolicand terpenoid. The extract of Litseraodorifera val. Leafincrude extract, ethyl acetate, acetone, ethanol and hexane can reduce free radical of  DPPH with IC50 of 250.7; 66.7; 69.7; 100.3 and 181.9 ppm respectively. Those are higher compared to vitamin C whose IC50 was 28.3 ppm. The extract of Litseraodorifera val. leaf haspotency as antioxidant activity that can be developed through further research.
PENGEMBANGAN LEMBAR KERJA PRAKTIKUM MAHASISWA BERBASIS RISET SOLID LIPID NANOPARTIKEL (SLN) TRIMIRISTIN HASIL ISOLASI BIJI PALA (Myristica fragrans) Pramesthi Regita Putri; Agus Sundaryono; Hermansyah Amir
ALOTROP Vol 6, No 1 (2022)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/alo.v6i1.22399

Abstract

This research aims to determine the feasibility, practicality, and effectiveness of LKPM based on solid lipid research of trimiristin nanoparticles resulting from nutmeg seed insulation as a guide sheet of organic chemical practicum II in lipid matter. This research uses 4-D methods, consisting of 4 stages, namely define, design, develop, and disseminate. However, in this study the researchers only performed until the third stage which is the development stage (develope). This research data is obtained from the results of material and media expert validation questionnaires, product practicality questionnaires as well as pretest and posttest results tested to fourth semester students who participated in organic chemistry course II.LKPM based on Research Solid Lipid Nanoparticle (SLN) Trimiristin resulting from Nutmeg Seed Isolation that has been developed obtained a value of 83.75% on media validation and obtained a value of 87.3% on material validation, which means it is in the category of highly feasible. While the practicality percentage result of 88.36 % on the small-scale test, which goes into the category strongly agrees, The average result that means students strongly agree that the products that have been developed are very practical to use. The average value of N-Gain Small Scale Test Score is 0.43, meaning it can be concluded that The Student Practicum Worksheet (LKPM) based on Solid Lipid Nanoparticle (SLN) trimiristin research resulting from Nutmeg Seed Isolation (Myristica fragrans) has moderate effectiveness value.
PENGEMBANGAN SUPLEMEN BAHAN AJAR CARA-CARA ISOLASI DAN IDENTIFIKASI SENYAWA BAHAN ALAM DENGAN PENDEKATAN STEM’S BERBASIS ANDORID Krisandini, Triana; Sundaryono, Agus; Elvia, Rina
ALOTROP Vol. 8 No. 1 (2024): Penelitian Kimia dan Pembelajaran Kimia
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/alo.v8i1.34531

Abstract

Penelitian ini bertujuan untuk mengetahui tingkat kelayakan, respon mahasiswa terhadap suplemen bahan ajar bahan ajar Kimia Organik Bahan Alam (KOBA KIM 413, KD 2) dengan pendekatan STEM’S bebasis android dan hasil belajar mahasiswa  setelah menggunakan suplemen bahan ajar tersebut. Penelitian ini dilaksanakan pada bulan Februari-Juli 2020. Model yang digunakan pada penelitian pengembangan ini adalah ADDI (adaptasi dari model ADDIE) yang terdiri dari tahap analisis, perencanaan, pengembangan, penerapan. Penelitian ini dilakukan di Univeristas Bengkulu dengan subjek mahasiswa pendidikan kimia Universitas Bengkulu yang mengambil mata kuliah KOBA TA 2019/2020. Mahasiswa dengan NPM genap berjumlah 9 orang untuk uji coba skala kecil dan mahasiswa dengan NPM ganjil berjumlah 21 orang untuk  uji coba skala besar. Instrumen penelitian yang digunakan berupa angket kebutuhan, lembar validasi, angket respon, serta lembar evaluasi. Hasil penelitian ini diperoleh: (1) tingkat kelayakan suplemen bahan ajar dengan pendekatan STEM’S berbasis android, persentase kelayakan dari segi materi  yang didapat yaitu 92,86 % dengan kategori sangat layak sedangkan dari segi media yaitu 80,21 % dengan kategori sangat layak sehingga bahan ajar dinilai layak untuk diujicobakan; (2) Hasil uji coba skala kecil didapatkan respon baik dengan persentasi rata-rata 89,75% dengan ada perbaikan; (3) Hasil belajar mahasiswa setelah menggunakan suplemen bahan ajar KOBA didapatkan nilai rata-rata sebesar 57,3 yang masuk pada kategori lulus. sehingga dapat disimpulkan bahwa suplemen bahan ajar cara-cara isolasi dan identifikasi senyawa bahan alam dengan pendekatan STEM’S bebasis android yang telah dikembangkan dapat digunakan sebagai suplemen dalam proses pembelajaran KOBA
EKSTRAK BATANG “AKAR KAIK-KAIK” ( Uncaria Cordata Lour. ) Merr SEBAGAI ANTIDIABETES PADA MENCIT YANG DI INDUKSI ALOKSAN Kirent Arikhsa Putri; Nurhamidah; Agus Sundaryono
ALOTROP Vol. 9 No. 1 (2025): Jurnal Pendidikan dan Ilmu Kimia
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/alo.v9i1.42208

Abstract

[EXTRACT OF “KAIK-KAIK ROOT” STEM (Uncaria Cordata Lour.) Merr AS AN ANTIDIABETES IN ALLOXAN-INDUCED MICE] This research aims to determine the effect of giving kaik-kaik root stem extract (Uncaria cordata Lour. Merr) on the blood sugar levels of mice (Mus musculus) induced by alloxan. This reseacrh began with a phytochemical test conducted to determine the secondary metabolite compounds contained in the root stem of kaik-kaik (Uncaria cordata Lour. Merr). Extraction is done by maceration method. Antidiabetic activity test was carried out on male mice induced by alloxan. The results of the phytochemical test showed that the stem extract of Uncaria cordata contained alkaloids, flavonoids, tannins, saponins and terpenoids. The results of the antidiabetic activity test showed that the Uncaria cordata stem extract was able to reduce blood glucose levels in alloxan-induced mice with the optimal dose of Uncaria cordata stem extract at a dose of 0.043 g/kgBB. Based on the results of this study, it can be concluded that the stem of Uncaria cordata has antidiabetic activity. Keywords: Antidiabetic, Kaik-Kaik Root Stem, Uncaria cordata Lour. Merr, Alloxan
Co-Authors ACENG RUYANI Ade Indriani Putri Alfia Novera Indah Esa Kasih Arina Fatharani Arsela Eko Listiono Bedah Rupaedah Bedah Rupaedah, Bedah Bhakti Karyadi BHAKTI KARYADI Bhakti Karyadi Bonodikun Bonodikun Candrawati, Emilia Candrawati, Emilia Chyntia Margareta Cici Romayanti Dapot Parulian Manurung Devi Silsia Devi Silsia Dewi Handayani Dhea Prasiwi Dian Kartika Sari Eko Swistoro Elvinawati Elvinawati Emi Hartati Emilia Candrawati Emilia Candrawati Endang Widi Winarni Endang Widi Winarni Ernis, Gustria Euis Nursa’adah Fahrurrozi, Fahrurrozi Fenny Andriani Fitri Yuwita Fuji Ramadenti Hadi Apriyoanda Hadi Apriyonda Henny Johan Herison, Catur Hermansyah Amir I Nyoman Candra I Nyoman Chandra Ilham Agus Saputra Jertadi Putri Dhani Kirent Arikhsa Putri Krisandini, Triana Lina Widawati M Lutfi Firdaus M. Farid M. Lutfi Firdaus M. Lutfi Firdaus Maya Wahyunarti Mayshah Purnamasari Megasari Megasari Meizul Zuki Mellyta Uliyadari Mina Sihite Hutasoit Muchammad Farid Mukhsin Mukhsin Muzanip Alperi Nur Wakidatul Khasanah Nurhamidah Nurhamidah Nurhamidah Nurhamidah Nurhamidah Nurhamidah Nurleli Nurleli Nurlia Latifah Nursaa'adah, Euis Nursaadah, Euis Pandu Imam Sudibyo Adib Pandu Imam Sudibyo Adib Pramesthi Regita Putri Putri Suci Asriani Rantika Khumairah Rasie Janika Reni Jumika Ridwan Yahya Rika Partika Sari Rina Elvia Rina Elvia Rina Elvia, Rina Rina Endriani Ririn Trinanda Rofiqa Asri Sari Puspita Ningsih Shiba Meike Indira Shinta Lestari Sipriyadi Sri Astuti Sumpono Sumpono Sumpono Sumpono Sumpono, Sumpono Suryadi Suryadi Theo Kuntara Tuti Maryana Tyas Sri Muryati Ulfah Anis Umaya Umi kalsum Wuri Marsigit Yenni Okfrianti Yohannes Adimar Marbun Yulia Suparti Zulman Efendi