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All Journal Jurnal Biologi Udayana MEDIA KOMUNIKASI TEKNIK SIPIL SAINS DAN MATEMATIKA JURNAL KIMIA SAINS DAN APLIKASI Jurnal Ilmu Lingkungan Bulletin of Chemical Reaction Engineering & Catalysis Elkawnie Jurnal Noken: Ilmu-Ilmu Sosial Indonesian Journal of Chemistry Pendas : Jurnah Ilmiah Pendidikan Dasar Molekul: Jurnal Ilmiah Kimia Community Development Journal: Jurnal Pengabdian Masyarakat International Journal of Sustainable Transportation Technology Jurnal Sains dan Edukasi Sains Journal of Science and Science Education Humanism : Jurnal Pengabdian Masyarakat JSIP: Jurnal Studi Ilmu Pemerintahan Greensphere: Journal of Environmental Chemistry jurnal administrasi politik dan sosial Buletin Edukasi Indonesia Jurnal Edukasi dan Pengabdian kepada Masyarakat (JEPKM) Molekul: Jurnal Ilmiah Kimia Bulletin of Chemical Reaction Engineering & Catalysis Journal of Community Empowerment JURNAL REKAYASA KIMIA & LINGKUNGAN Economy Bring Ultimate Information All About Development Journal
Yayuk Astuti
Chemistry Department, Faculty Of Science And Mathematics, Universitas Diponegoro, Jl. Prof. Jacob Rais, Tembalang, Semarang 50275
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Journal : Elkawnie

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Production and Characterization of Adsorbent from Oyster Shell (Crassostrea gigas) Using Physics and Chemical Activation with ZnCl2 and Its Application for Removal of Hexavalent Chromium Lia Handayani; Azwar Thaib; Nurhayati Nurhayati; Yayuk Astuti; Adi Darmawan
Elkawnie: Journal of Islamic Science and Technology Vol 6, No 2 (2020)
Publisher : Universitas Islam Negeri Ar-Raniry Banda Aceh

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22373/ekw.v6i2.7333

Abstract

Abstract: Oyster shell waste has been investigated as a raw material for making adsorbents that will be activated. Physical activation uses temperatures of 500 ºC, 600 ºC, 700 ºC, 800 ºC, 900 ºC and chemical activation uses ZnCl2 with a concentration of 1 %, 5 %, 10 % and 15 %. Based on the analysis of the characteristics that have been carried out for physically activated adsorbents, the oyster shell calcined at 800 ºC produces the best characteristics, it is a radius of 35.11 Å with a percentage of removal of 38.04 %, as well as the results of the FTIR, XRF and SEM analysis gives the best results among others. Whereas for chemically activated adsorbents, the use of activator ZnCl2 10% produces adsorbents with the best characteristics among others with a radius of 84.14 Å and removal percentage of 65.68 %, the best results for adsorbents activated using 10% ZnCl2 are also supported by analysis results given by FTIR, XRF, and SEM.Keywords: Adsorbent; BET; Cr6+; Oyster Shell Waste; XRF Abstrak: Cangkang tiram (Crassostrea gigas) telah diteliti sebagai bahan baku pembuatan adsorben yang akan diaktivasi secara fisika dan kimia. Pembuatan adsorben dengan aktivasi secara fisika menggunakan variasi suhu 500 ºC, 600 ºC, 700 ºC, 800 ºC dan 900 ºC. sedangkan aktivasi kimia yaitu menggunakan aktivator ZnCl2 menggunakan variasi konsentrasi 1 %, 5 %, 10% dan 15 %. Berdasarkan analisa karakteristik yang telah dilakukan untuk adsorben-adsorben yang telah diaktivasi secara fisika, cangkang tiram yang di kalsinasi pada suhu 800ºC menghasilkan karakteristik yang paling baik, yaitu radius pori-pori 35,11 Å dengan persentase penyisihan sebesar 38,04 %, begitu pula dengan hasil analisa FTIR, XRF dan SEM memberikan hasil terbaik diantara yang lain. sedangkan untuk adsorben-adsorben yang diaktivasi secara kimia, penggunaan aktivator ZnCl2 10% menghasilkan adsorben dengan karakteristik yang paling baik diantara lainnya dengan radius pori-pori 84,14 Å dan persentase penyisihan sebesar 65,68%, hasil terbaik untuk adsorben yang diaktivasi menggunakan ZnCl2 10 % juga didukung oleh hasil analisa dari FTIR, XRF dan SEM.
The Characterization of Oyster Shell (Crassostrea gigas) as Adsorbent in The Removal of Cr(VI) Ions. A Study of NaOH and H2SO4 Activation Effect Lia Handayani; Cut Rahmawati; Nurhayati Nurhayati; Yayuk Astuti; Adi Darmawan
Elkawnie: Journal of Islamic Science and Technology Vol 6, No 1 (2020)
Publisher : Universitas Islam Negeri Ar-Raniry Banda Aceh

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22373/ekw.v6i1.5543

Abstract

Abstract : Oyster shell as one of the highest bio-waste in Alue Naga Aceh Besar District, Indonesia, was used as an adsorbent to remove a heavy metal Cr (VI) ion. The study was started by calcinating oyster shells at a high temperature of 800 ºC for 3 hours. The effect of various acid (H2SO4) and base (NaOH) activator was studied using characterization and adsorption experiments. The characterization obtained the sample activated by 10% NaOH (Na10-ACT) and 10% H2SO4 (H10-ACT) had the highest surface area which had 14.23 m2/g, 10.77 m2/g, respectively. Furthermore, the adsorption experiments confirmed the highest surface area by showing the highest Cr (IV) ion removal of 57.66%, 70.7%, respectively. The further investigation using X-ray fluorescence (XRF) determined that the Na10-ACT adsorbent has a better composition compared to the H10-ACT due to its high purities.Abstrak : Cangkang tiram sebagai salah satu bio-limbah padat di Desa Alue Naga Kabupaten Aceh Besar, digunakan sebagai adsorben untuk menghilangkan ion logam berat Cr (IV). Penelitian ini diawali dengan mengkalsinasi cangkang tiram pada temperatur tinggi 800ºC selama tiga jam. Pengaruh penambahan aktivator asam (H2SO4) dan basa (NaOH) juga dipelajari melalui karakterisasi dan pengujian adsorpsi. Hasil karakterisasi menunjukkan sampel yang diaktivasi dengan 10% NaOH (Na10-ACT) dan 10% H2SO4 (H10-ACT) memiliki luas permukaan tertinggi yaitu 14,23 m2/g, 10,77 m2/g, masing-masing. Lebih lanjut, pengujian adsorpsi juga mendukung luas permukaan yang tinggi dengan menghilangkan ion Cr (IV) sebesar 57,66%, 70,7%, masing-masing. Investigasi melalui analisa XRF menyimpulkan bahwa Na10-ACT memiliki komposisi yang lebih baik dibanding H10-ACT karena memiliki kemurnian yang tinggi.
Co-Authors Abdul Jabbar Adi Darmawan ADI SANTOSO Agriccia Pangestica Saputry Ahmad Suseno Alfi Saadah Alfiansyah Alfiansyah Amilia Fauziyah Anisyah Anisyah Annisa Syifaurrahma Arnelli Arnelli Arum Dista Wulansari Aulia Zahra Ekaningsih Azwar Thaib Bara Yunianto Fathoni Brainy Happy Ana Tasiman Brainy Happy Ana Tasiman Brigita Maria Listyani Cut Rahmawati Daniswara, Lufthansyah Dayadi, Dayadi Didi Dwi Anggoro Didik Setyo Widodo Esti Ayu Faisal Syahputra Fandi Nasrun Cholis Faradina Azahra Zaqia Fauzan Musthafa Febrianti, Devi Fitriani Solichah Galih N. R. Pargiman Gaurav A. Bhaduri Gunawan Gunawan HARTATI Hartati Hartati Hasanuddin, Fenny Hasim Muzadi Hendri Widiyandari Hendri Widiyandari Hendri Widyandari Hermasnyah, Sam Husnayani, Husnayani Iis Nurhasanah Iis Nurhasanah Irman, Iriani Isumarni, Isumarni Jamaluddin Ahmad Jufri, Al Jafar Jumiati Jumiati Khalik, Suhartini Khalik, Suhartini Khoiri, Rahma Lia Handayani Lia Handayani Lia Handayani Linda Suyati Luqman Buchori M. S.H. Yoga S. Majid, Abdul Majid Zainuddin Mega Bara Cahyantari Muh. Fajar, Muh. Muh. Rohady Ramadhan Muhammad Hanafi Muhammad Rusdi Muslim, Agus Mustanir, Ahmad Nabila Amalia Izaaz Aanisa Narita Rizki Nayla Zahra Kamalia Nonci, Nurjannah Noor Afifah Nur Hidayati Nurhayati Nurhayati Nurhayati Nurhayati Nurlaelah Nurlaelah, Nurlaelah Nurul Latifah Nurwidah, Andi Pandji Triadiyaksa Pardoyo Pardoyo Pardoyo Pardoyo Popi Hadi Wisnu Wardhani Prasetya, Eko Fery Prisca Putri Elesta Pungki Hanipa R Kasau, Nurzin Rahayu, R.A. Yunita Suci Rahayu, Yunita Suci Rahmatul Fazira Rahmawati Rahmawati Ramdan, Ramdan Rasman Ratna Balgis Redi Joko Prasetyo Richard Leonardo Sianturi Rissa Kharismawati Rizka Andianingrum Roni Adi Wijaya Saade, Muhammad Faisal Samratusabri Subehan Siringoringo, Eliezer Patardo Siti Fatimah Siti Nurhayati Siti Susanti, Siti Slamet Priyono Subehan, Samratusabri Tamrin, Muh Tang, Jusman Taslimah Taslimah Teguh Iman Prastyo Titik Lestariningsih Titik Lestariningsih Tri Windarti Tri Windarti Triadiyaksa, Pandji Trie Nanda Mulyana Trisnasari, Damayanti Ulya Hanifah Henrika Putri Vega Norma Rafika Putri Wijayanti, Septi Yeni Aprilia Yusrianti Yusrianti, Yusrianti Zulfahmi Zulfahmi