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Nurdin Bukit
Universitas Negeri Medan
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Journal : JURNAL PENELITIAN SAINTIKA

 1 
PREPARASI BENTONIT ALAM MENJADI NANO PARTIKEL Bukit, Nurdin; Ginting, Eva Marlina; Harahap, Mukti Hamjah
JURNAL PENELITIAN SAINTIKA VOL 15, NO 2 (2014): JURNAL PENELITIAN SAINTIKA
Publisher : JURNAL PENELITIAN SAINTIKA

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Abstract

The purpose of this study is the manufacture of natural bentonite into  nano  particles  and  is  used  as  a  filer  on  thermoplastic  high-density polyethylene  (  HDPE  )  .  The  method  used  in  the  manufacture  of  nanoparticles  of  bentonite  are  two  ways  ;  The  first  synthesis  method  using surfactant  cetyl  trimethyl  ammonium  bromide  (  CTAB  )  and  the  second way  in  ballmill  for  10  hours  .  Characterization  of  the  particle  size analyzer  (  PSA  )  ,  morphological  analysis  with  scanning  electron microscope ( SEM ) and analysis of the structure by X  -  ray diffraction ( XRD  )  was  performed  .  Nano  particles  with  variation  of composition  of natural  bentonite  (  2  ,  4  ,  6  ,  8  ,  10  %  w  t)  blends   with  HDPE  and compatibilizer  PE  -  g-  MA  on  the  appliance  s  internal  mixer  at  a temperature  of  150oC  and  laboplatomil  rate  of  60  rpm  for  10 minute.Berdasarkan PSA analysis and X  -  ray , natural bentonite having an average size of 75 nm for synthesis with CTAB , and 97.5 nm for the ball  mill  .  from  the  results  of  XRD  analysis  of  minerals  crystoballite  ( SiO2 ) and phase annite ( Al3.448Fe3K0.99Na  0.01O12Si  2.552  ) . In testing the mechanical  properties  of  the  resulting  increase  in  tensile  strength  and breaking up the composition perpajangan 2 to 6 % and a decline in the composition  of  8  %  .  The  results  of  SEM  analysis  showed  that homogeneous  mixing  of  ingredients  and  the  bentonite  particle agglomeration on the composition of 10 % wt.
PREPARASI BENTONIT ALAM MENJADI NANO PARTIKEL SEBAGAI FILLER PADA TERMOPLASTIK HDPE Bukit, Nurdin; Ginting, Eva Marlina; Harahap, Mukti Hamzah
JURNAL PENELITIAN SAINTIKA Vol 14, No 2 (2014): SEPTEMBER 2014
Publisher : JURNAL PENELITIAN SAINTIKA

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Abstract

The purpose of this study is the manufacture of natural bentoniteinto nano particles and is used as a filer on thermoplastic high-densitypolyethylene ( HDPE ) . The method used in the manufacture of nano-particles of bentonite are two ways ; The first synthesis method usingsurfactant cetyl trimethyl ammonium bromide ( CTAB ) and the secondway in ballmill for 10 hours . Characterization of the particle sizeanalyzer ( PSA ) , morphological analysis with scanning electronmicroscope ( SEM ) and analysis of the structure by X - ray diffraction (XRD ) was performed . Nano particles with variation of composition ofnatural bentonite ( 2 , 4 , 6 , 8 , 10 % w t) blends with HDPE andcompatibilizer PE - g- MA on the appliance 's internal mixer at atemperature of 150 C and laboplatomil rate of 60 rpm for 10 minute.Berdasarkan PSA analysis and X - ray , natural bentonite having an average size of 75 nm for synthesis with CTAB , and 97.5 nm for the ball mill . from the results of XRD analysis of minerals crystoballite (SiO2 ) and phase annite ( Al3.448Fe3K0.99Na 0.01O12Si 2.552 ) . In testing the mechanical properties of the resulting increase in tensile strength and breaking up the composition perpajangan 2 to 6 % and a decline in the composition of 8 % . The results of SEM analysis showed that homogeneous mixing of ingredients and the bentonite particle agglomeration on the composition of 10 % wt. 
Co-Authors Abd. Hakim Anggili Pratama Apriana Apriana Asrul Karim Asrul Karim Br Ginting, Anayosi Bunga Fisikanta Bukit S.Si, M.Si Dalimunthe, Jumlia Syaulani Rizki Derlina . Derlina Derlina Dongoran, Jhonas Edi Surya Edi Surya, Edi Edy Surya Edy Surya Elfariska Sidebang Erna Frida EVA FARIDAH Eva Faridah Eva Marlina Ginting Eva Marlina Ginting Eva Marlina Ginting Eveb Adonai Hutagalung Fasti Rola Ferry Rahmat A. Bukit Fitri Mawaddah Lubis, Fitri Mawaddah Fitriani Fitriani Gea, Hepi Arman Gea, Hepi Armen Harahap, Linda Rahmadhani Harahap, Mukti Hamzah Hepi Arman Gea Hepi Armen Gea Hutagalung, Eveb Adonai Idawati Idawati Idawati Idawati Karya Sinulingga Makmur Sirait Mara Bangun Harahap Mara Bangun Harahap Mariati P S, Mariati P Martha M. Padang Martha Marchofinece Padang Marzuki Marzuki Motlan . Muhammad Affan Siregar Mukti Hamjah Harahap, Mukti Hamjah Mukti Hamzah Harahap Muliati, Sri Nainggolan, Raivita Jesica Nora Deselia Saragih Norma Septiani Novita . Prapti Ningsih Rini Lestari Rita Juliani Rizki Maulida, Rizki Sahyar . Saniman Saniman, Saniman Sarah Fazilla Septiani, Norma Sidebang, Elfariska Simanjutak, Mariati Purnama Sinaga, Sufri Siregar, Muhammad Affan Siregar, Shinta Marito Siti Habsari Pratiwi, Siti Solikin Solikin Sriadhi Sriadhi Susilawati, Sri Mila Syahrul Humaidi, Syahrul Tota Tota Martaida Usler Simarmata Yenni Dwi Aprilita Sagala Yohanna Lestari Zaskya Laksmita Utami