Claim Missing Document
Check
Articles

Effect of Variation H2SO4 on the Manufacture of Nanocellulose from Corn Cobs Pertiwi, Mega; Manurung, Posman; Suciyati, Sri Wahyu; Karo, Pulung Karo
Journal of Energy, Material, and Instrumentation Technology Vol 5 No 3 (2024): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v5i3.173

Abstract

The acid hydrolysis method has been used to manufacture nanocellulose from corn cobs. This study aims to determine the effect of variations in the concentration of H2SO4 on the characteristics of nanocellulose produced from corn cobs and their surface morphology. The variations of H2SO4 used were 5, 10, 15, and 20%. X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) are characterizations used. The results of XRD characterization showed that the crystallite size obtained followed the nanocellulose crystallite size, which was 1.79-2.59 nm. The SEM characterization showed that the resulting nanocellulose's surface morphology was lumpy and non-porous.
Production of Nanocellulose from Kepok Banana Peel Waste Using Acid Hydrolysis Method Putri, Faradilla Nabila; Manurung, Posman; Suciyati, Sri Wahyu; Karo, Pulung Karo
Journal of Energy, Material, and Instrumentation Technology Vol 4 No 3 (2023): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v4i3.174

Abstract

Research on the production of nanocellulose from kepok banana peel waste has been carried out using the Acid Hydrolysis method with H2SO4 Sulfuric Acid. This study aims to determine the effect of giving H2SO4 on kepok banana peels and the crystal structure and surface morphology of nanocellulose on kepok banana peels. The production of nanocellulose was carried out in three stages: delignification using 10% NaOH, bleaching using 10% H2O2, and isolation of nanocellulose using H2SO4 with various concentrations of 5, 10, 15, and 20%. This research uses X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) as its characterization. The resulting crystallite size ranges from 3.58 to 4.15 nm, producing a lump-like morphological structure.
PEMBUATAN NANOSELULOSA DARI KAYU LUNAK PINUS (Pinus merkusii) MENGGUNAKAN METODE HIDROLISIS ASAM Anggraini, Anisyah; Manurung, Posman; Suciyati, Sri Wahyu; Yulianti, Yanti
Journal of Energy, Material, and Instrumentation Technology Vol 4 No 4 (2023): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v4i4.186

Abstract

Pengaruh Variasi Konsentrasi Zn(NO3)2·6H2O Terhadap Gugus Fungsi, Ukuran Partikel, dan Morfologi Partikel Nanopartikel ZnO dengan Metode Sintesis Hijau Menggunakan Ekstrak Daun Kelor Benyamin, Chairunissa A; Manurung, Posman; Suprihatin, Suprihatin
Journal of Energy, Material, and Instrumentation Technology Vol 4 No 3 (2023): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v4i3.208

Abstract

This research was conducted to determine the effect of varying concentrations of Zn(NO3)2·6H2O (zinc nitrate hexahydrate) on functional groups, particle size, and particle morphology of ZnO nanoparticles using the green synthesis method using Moringa leaves. The materials was used in this study were moringa leaf extract, Zn(NO3)2·6H2O with various concentrations of 0.2, 0.4, 0.6, and 0.8 M, and NaOH of 0.1 M. Based on the results of characterization using FTIR, it shows that the functional groups in the content of Moringa leaves play a role in the formation of ZnO nanoparticles. Meanwhile, the results of the XRD characterization showed a diffractogram difference with standard ZnO at concentrations of 0.6 M and 0.8 M Zn(NO3)2·6H2O with the appearance of the NaNO3 phase. SEM characterization results show that the morphology of ZnO nanoparticles using the green synthesis method is irregular in shape.
Study on Crystal Structure, Surface Area, and Energy Gap Behaviors of Nanotitania Polymorphs Prepared Using Monoethanolamine Manurung, Posman; Maharani, Renita; Rahmayanti, Dita; Yulianti, Yanti; Junaidi; Marjunus, Ronius
Science and Technology Indonesia Vol. 9 No. 2 (2024): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2024.9.2.345-353

Abstract

Polymorphous nanotitania samples were prepared from titanium butoxide (TTB) as a precursor using sol-gel processing in ethanol as a solvent, without and with monoethanolamine (MEA). The experiments used 5.25 mL TTB and MEA with varied volumes of 0.5, 1.0, 1.5, and 2.0 mL. The sample without MEA was specified as sample A, and the samples produced using MEA were specified as samples B, C, D, and E, respectively. All samples were calcined at 500 °C for 4 h and then collected data by X-ray Diffraction (XRD), the Brunauer-Emmett-Teller (BET) method used to analyze Surface Area Analyzer (SAA), Transmission Electron Microscopy (TEM), Raman Spectroscopy, and UV-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS). The results of XRD characterization indicate that samples A and B form anatase phase, while samples C and D are composed of anatase, brookite, and rutile phases, and sample E is consisted of anatase and brookite phases with weight percentages of (94.53 ± 1.72) % and (5.47 ± 0.36) %, respectively. The presence of the three phases of titania is also confirmed by Raman spectroscopy analysis, which showed anatase peaks at 146, 197, 398, and 513 cm-1, brookite peaks at 245 and 402 cm-1, and rutile peaks at 319, 436, and 612 cm-1. According to XRD, the samples have the particle size in the range of 14-19 nm. A representative sample (sample C) was also characterized using TEM, revealing a particle size of 16.0 ± 0.3 nm. This representative sample revealed the largest surface area of 172.2 m2/g, as seen by BET, and the lowest energy gap of 3.03 eV.
Pengaruh Hidrolisis Asam pada Pembuatan Nanoselulosa dari Swietenia mahagoni Gultom, Rysa Sonya Reni Paulin; Manurung, Posman; Karo Karo, Pulung; Suciyati, Sri Wahyu
Journal of Energy, Material, and Instrumentation Technology Vol 5 No 4 (2024): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v5i4.184

Abstract

The extraction of the mahogany pulp as the main ingredient for the preparation of nanocellulose was carried out using the acid hydrolysis method. Sulfuric acid (H2SO4) was used to hydrolyze the primary constituent and sodium hydroxide (NaOH) was utilized in the delignification process. The purpose of this study is to identify the properties of nanocellulose made from mahogany hardwood on fluctuations in H2SO4 concentrations, particularly on concentration 19, 29, 39, and 45%. A Fourier Transform Infrared (FTIR) spectrophotometer, Scanning Electron Microscopy (SEM) and X-ray diffraction (XRD) were used to analyze the sample product, which is cellulose nanocrystal powder. The XRD results stated that the diameter of the nanocellulose crystal size ranged from 3-6 nm, while the SEM results showed that the sample's morphology resembled a stacked arrangement of stones. Meanwhile, the results of the FTIR indicated that the functional groups produced consisted of hydroxyl, aliphatic, aromatic rings, aryl carbonyls, and pyranose. Based on the tests, the best sample is obtained as a concentration variation of H2SO4 39%, which produces a diameter of 3.6 nm with a crystallinity index as high as 80.48%.
Extraction of Nanocellulose from Bagasse Using Acid Hydrolysis Method Zaharani, Rethanita; Manurung, Posman; Firdaus, Iqbal; Asmi, Dwi; Abdurrahman, Ahmad Faruq
Journal of Energy, Material, and Instrumentation Technology Vol 5 No 4 (2024): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v5i4.192

Abstract

The acid hydrolysis method was used to extract nanocellulose from bagasse. This study aims to prepare nanocellulose from sugarcane bagasse by acid hydrolysis method and to know the results of characterization with X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and Fourier Transform Infrared (FTIR). In this study, 4 samples were made with variations of H2SO4 of 19, 29, 39 and 45%. XRD analysis shows that with the increase of sulfuric acid, the percentage of each sample increases, but in the 39% sample, there is a decrease in purity because there are still areas of cellulose that have yet to disappear. The phase identification results show that in the sample with 19, 29, and 39% addition, H2SO4 Iα, Iβ, and thenardite phases were formed. In the sample, 45% only form Iα and Iβ phases with a resulting particle size of 2.83 nm and a degree of crystallinity of 55.52%. The results of the SEM test analysis show that the image pattern has stone structures that overlap each other. The results of FTIR analysis show that the functional groups detected are O – H, C – H, C ≡ C, C = C, H – C – H, C – O, and C – O – C, which indicates the presence of nanocellulose.
CORONA DISCHARGE SEBAGAI TEKNOLOGI STERILISASI RAMAH LINGKUNGAN UNTUK PENGENDALIAN BAKTERI Abdurrahman, Ahmad Faruq; Manurung, Posman; Sumardi, Sumardi; Firdaus, Iqbal; Asmi, Dwi
Jurnal Fisika : Fisika Sains dan Aplikasinya Vol 10 No 1 (2025): Jurnal Fisika : Fisika Sains dan Aplikasinya
Publisher : Universitas Nusa Cendana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35508/fisa.v10i1.20632

Abstract

Lucutan corona merupakan salah satu bentuk teknologi plasma dingin yang menjanjikan dalam aplikasi sterilisasi karena kemampuannya menghasilkan radikal oksigen reaktif (ROS) yang efektif dalam menonaktifkan mikroorganisme. Penelitian ini mengkaji karakteristik geometri, konfigurasi elektroda, serta parameter operasi lucutan corona dalam berbagai studi yang telah dipublikasikan. Hasil analisis menunjukkan bahwa konfigurasi pin-to-plate lebih banyak digunakan dibandingkan surface discharge karena kemampuannya menghasilkan medan listrik terfokus dengan intensitas tinggi. Tegangan operasi berkisar antara 10–30 kV dengan frekuensi 0.5–20 kHz, tergantung pada lingkungan bakteri uji. Beberapa jenis bakteri patogen, seperti Pseudomonas aeruginosa, Staphylococcus aureus, Serratia liquefaciens, Salmonella typhimurium, Listeria monocytogene, dan Escherichia coli, terbukti dapat dinonaktifkan secara efektif oleh plasma corona. Namun, tantangan dalam optimasi parameter, efisiensi energi, dan penerapan dalam skala industri masih menjadi hambatan yang perlu diselesaikan. Oleh karena itu, diperlukan penelitian lebih lanjut untuk meningkatkan efektivitas dan efisiensi teknologi ini dalam berbagai aplikasi, termasuk di bidang medis, pangan, dan pengolahan limbah.
Penggunaan Modul Visual Interaktif untuk Meningkatkan Literasi Numerik Mahasiswa Baru di Jurusan Fisika Unila Ayu Aprilia; Suprihatin Suprihatin; Posman Manurung
Jurnal Kemitraan Masyarakat Vol. 2 No. 2 (2025): Jurnal Kemitraan Masyarakat
Publisher : Lembaga Pengembangan Kinerja Dosen

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.62383/jkm.v2i2.1602

Abstract

Numerical literacy is a fundamental skill that plays a crucial role in the learning process, particularly in the field of science, especially physics. However, the reality is that many freshmen struggle with numerical literacy. This significantly impacts their foundational mathematical skills, which can hinder the academic learning process. This community service activity aims to enhance the numerical literacy of freshmen in the Physics Department at the University of Lampung by utilizing interactive visual modules. The activity was conducted over two sessions in January 2025, involving 28 new students. The students were divided into heterogeneous groups to support collaborative learning. Pre-test and post-test assessments were conducted to measure the effectiveness of the modules. The results showed an average score improvement from 36.25% to 56.6%. Addionally, the satisfaction survey results showed positive responses regarding the module’s appearance, clarity and benefits. Based on this activity, it was concluded that collaborative learning supported by interactive visual media can enhance students numerical literacy skills.
Penerapan model inverted class sebagai upaya peningkatana kualitas pembelajaran matematika untuk mahasiswa baru di Jurusan Fisika Universitas Lampung Aprilia, Ayu; Pauzi, Gurum Ahmad; Supriyanto, Amir; Abdurrahman, Ahmad Faruq; Syafriadi, Syafriadi; Karo-karo, Pulung; Suprihatin, Suprihatin; Manurung, Posman
SELAPARANG: Jurnal Pengabdian Masyarakat Berkemajuan Vol 9, No 3 (2025): May
Publisher : Universitas Muhammadiyah Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31764/jpmb.v9i3.30205

Abstract

Abstrak Matematika merupakan fondasi utama dalam penyelesaian berbagai masalah dalam bidang ilmu fisika. Namun, banyak mahasiswa mengalami kesulitan dalam mengusasai konsep-konsep dasar matematika sehingga menganggu prestasi akademik mahasiswa. Pengabdian ini bertujuan mengimplementasi metode inverted class untuk melihat bagaimana keberhasilannya dalam menyelesaikan permasalahan ini. Kegiatan pengabdian dilaksanakan pada minggu ke 3 dan 4 bulan Januari 2025. Kegiatan ini  dibagi menjadi menjadi tiga kegiatan yaitu persiapan kegiatan, pelaksanan kegiatan di kelas serta evaluasi keberhasilan dengan sasaran 55 mahasiswa baru Fisika Unila. Dalam masa persiapakan disusun modul interaktif, menarik dan modern. Lalu dilakukan test pemahaman awal konsep matematika dengan hasil 42,9%. Selanjutnya dilakukan 2 kali pembelajaran dengan inverted class. Pada tahap evaluasi diperoleh peningkatan pemahaman mahasiswa menjadi 60.5%. Dengan tambahan kesan positif terhadap pelaksanaan kegiatan dan modul yang diberikan. Pengabdian ini berhasil menunjukkan bahwa inverted class dapat menjadi solusi untuk mencarik pendekatan yang efektif dalam meningkatkan pemahaman konsep sekaligus melatih kemandirian belajar mahasiswa.  Kata kunci: fisika; inverted class ; mahasiswa baru; pemahaman matematika AbstractHowever, many students struggle to grasp basic mathematical concepts, which negatively impacts their academic performance. This community service program aims to implement the Inverted Class method to evaluate its effectiveness in addressing this issue. The program activities were carried out in 3th dan 4th weeks of January 2025. This program was divided into three stages: preparation, classroom implementation, and evaluation of its success, involving 55 first-year physics students at Universitas Lampung. During the preparation phase, an interactive, engaging, and modern module was developed. An initial test was conducted to assess students' understanding of basic mathematical concepts, yielding an average score of 42.9%. The implementation phase involved two Inverted Class learning sessions. In the evaluation phase, the students' understanding improved significantly, with an average score increase to 60.5%. Additionally, students provided positive feedback on the learning process and the module used. This program successfully demonstrated that the Inverted Class method can serve as an effective approach to improving conceptual understanding while fostering students' independent learning skills. Keywords: inverted class; first-year students; physics; mathematical understanding; independence
Co-Authors Abdurrahman, Ahmad Faruq Agnesia, Donna Agus Riyanto Agus Riyanto Agus Riyanto Agus Riyanto Agus Suyatna Ahmad Rosadi Alfin Edo Kaisar Lubis Amir Supriyanto Anggi Puspita Dewi Anggi Stevani Anggraini, Adeliya Ayu Anggraini, Anisyah Aprilia, Ayu Arya R. Syah Ayu Aprilia Benyamin, Chairunissa A Chandra Ertikanto Craig Buckley Delfi Oktavia Amrani Della M. Andini Dita Rahmayanti Dwi Asmi Ediman Ginting Ediman Ginting Ediman Ginting Suka Erika Sempana Ginting Fajar Nurjaman Faradilla Syani Fath, Yusril Al Fatia Ulfah Fegi Liani Firdaus, Iqbal Futichah Futichah Gregorius N. Susanto Gultom, Rysa Sonya Reni Paulin Hasni Handayani Imaniar Romaeni Indra Pardede Iqbal Firdaus It Meng Low Jayanti Pusvitasari Johar Sitohang Junaidi - Junaidi Junaidi Junaidi Junaidi Junaidi Junaidi Juniati Br Simbolon Karo Karo, Pulung Karo, Pulung Karo Ketut Putra Wijaya Lady Permatasari Lusi Vusfita Sari Maharani, Renita Marjunus, Ronius Marjunus, Roniyus Mega Pertiwi, Mega Mey Puji Astuti Miranti Syafitri Mitra Septanto Nabilah Rafidiyah Nadia Febriyanti Nita Susanti Nola Fricilia Nurcahayaniati, Hikmah Nurqori Setiawati Pauzi, Gurum Ahmad Pertiwi, Salwa Dian Prihanto, Surya Pulung Karo-Karo Putri, Faradilla Nabila R. Supryanto Rahayu, Sri Rahma Fauza Rahmayanti, Dita Renita Maharani Fauzi Rika Rahayu Riska Trisna Nuraini Riyanto, Agus Rizki Amalia Rudy Situmeang Rudy Situmeang Rudy T M Situmeang S Suprihatin Sahtoni Sahtoni Sari, Tria Permata Sembiring, Simon Sempana, Erika Shabrina, Shabrina Yakosati Simon Sembiring Simon Sembiring Simon Sembiring Simon Sembiring Siti Fadilah Sitohang, Rosanti sri wahyu suciayti Sri Wahyu Suciyati Sri Wahyu Suciyati Sukma Wibowo Sumardi . Sumardi, Sumardi Sumiyati Sumiyati Supardi Supardi Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Suprihatin Supriyanto, Amir Syafriadi Syafriadi Syafriadi Syafriadi Trianasari, Trianasari Vega Rahmawati Ar Vidi Nurhidayah Wasinton Simanjuntak Windhini Anggraeni Yanti Yulianti Yanti Yulianti Yanti Yulianti Yanti Yulianti Yanti Yulianti Yanti Yulianti Yuant Tiandho Yudhistira Novita Handayani Yunita Yunita Zaharani, Rethanita Zahra Maria Ulfa