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Journal : Journal of Research and Technology

Optimization of Ultrasound-Assisted Extraction Parameters from Indigofera Tinctoria L using Response Surface Methodology Achmad Qodim Syafaatullah; Variyana, Yeni; Ni’matur Rohmah; Iid Mufaidah; Ayu Qurota A’yun
Journal of Research and Technology Vol. 7 No. 2 (2021): JRT Volume 7 No 2 Des 2021
Publisher : 2477 - 6165

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Nowadays, the natural dyes are commonly used in textile industry. One of them is Indigofera tinctoria L leaves extracting natural dyes that produce blue color and have various potential utilization. However, the extraction time required usually takes a long time using conventional extraction. Thus, some researches reported that ultrasound-assisted extraction can accelerate and increase the extraction yield. The mechanism of ultrasonography is able to assist matrix cell rupture through the ultrasound cavitation. The present research aimed to study and to evaluate the Indigofera tinctoria L dye using ultrasound-assisted extraction. Response surface methodology (RSM) in conjunction with box-behnken design (BBD) was applied to optimize and to analyze the extraction conditions. The independent factors were ratio feed to solvent (0.02-0.1 g/ml), ultrasound temperature (50-60oC), and extraction time (50-90 minutes). Further, feed to solvent ratio was the most significant factor of extraction process in comparison with temperature and extraction time. The optimum extraction conditions were 58oC, 0.02 g/ml, and 50 minutes. The predicted model obtained was 6.025% which close to the actual data (5.75%). Moreover, the extract dye compounds were analyzed by FTIR test and the result was 64.07% for presence of Indigo dye. Therefore, the natural dyes can be alternative and sustainable dye as environmentally friendly
Optimization of Ultrasound-Assisted Extraction Parameters from Indigofera Tinctoria L using Response Surface Methodology Achmad Qodim Syafaatullah; Variyana, Yeni; Ni’matur Rohmah; Iid Mufaidah; Ayu Qurota A’yun
Journal of Research and Technology Vol. 7 No. 2 (2021): JRT Volume 7 No 2 Des 2021
Publisher : 2477 - 6165

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55732/jrt.v7i2.450

Abstract

Nowadays, the natural dyes are commonly used in textile industry. One of them is Indigofera tinctoria L leaves extracting natural dyes that produce blue color and have various potential utilization. However, the extraction time required usually takes a long time using conventional extraction. Thus, some researches reported that ultrasound-assisted extraction can accelerate and increase the extraction yield. The mechanism of ultrasonography is able to assist matrix cell rupture through the ultrasound cavitation. The present research aimed to study and to evaluate the Indigofera tinctoria L dye using ultrasound-assisted extraction. Response surface methodology (RSM) in conjunction with box-behnken design (BBD) was applied to optimize and to analyze the extraction conditions. The independent factors were ratio feed to solvent (0.02-0.1 g/ml), ultrasound temperature (50-60oC), and extraction time (50-90 minutes). Further, feed to solvent ratio was the most significant factor of extraction process in comparison with temperature and extraction time. The optimum extraction conditions were 58oC, 0.02 g/ml, and 50 minutes. The predicted model obtained was 6.025% which close to the actual data (5.75%). Moreover, the extract dye compounds were analyzed by FTIR test and the result was 64.07% for presence of Indigo dye. Therefore, the natural dyes can be alternative and sustainable dye as environmentally friendly
Co-Authors Achmad Qodim Syafaatullah Afifah, Dian Ayu Agus Triono Amelia Sri Rezki Andika Wahyu Purnama anggi saputra Aphrodita Luthfania Eka Putri Arga Bayramadhan Arga Bayramadhan Ariski Putra, Feby Ayu Qurota A’yun Bayramadhan, Arga Dedi Teguh Dennis Farina Nury Deviany Deviany Devy Cendekia Devy Cendekia Dewi Ermaya Dewi Ermaya Dewi Ermaya Dewi Ermaya Dian Ayu Afifah DIDIK PURWANTO Donny Satria Bhuana Dwi Setyorini Elsyana, Vida Evita Karlina Fadian Farisan Silmi Fahni, Yunita Feerzet Achmad Firmansyah, Muhammad Arif Fitria, Murni Gelegar, Iyappateya Hanifah, Windia Iid Mufaidah Indradewa, Rhian Iyappateya Gelegar Kurniawan, Dodi Kurniawan, Lukman Haris Livia Rhea Alvita Lukman Haris Kurniawan Lutvianto Pebri Handoko M. Mahfud M. Yogi Riyantama Isjoni Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mega Arum Ariyani Mochamad Asrofi Muhammad Zulfikar Luthfi Muslimin Nasution Muslimin Nasution Najlaa Ariibah Meutia Nasution, Muslimin Ni'matur Rohmah Ni’matur Rohmah Ni’matur Rohmah Ni’matur Rohmah Nugroho, Muhammad Erwin Cahyo Nurwijayanti Panjaitan , Renova R. A. Ilyas Rahma, Aulia Nabila Rahmat Hidayat Reni Yuniarti Rezki, Amelia Sri Rhea Alvita, Livia Ria Wulandari Rohmah, Ni'matur Rustiawan Jody, Rafli Satria, Muh. Nova Setyo Pambudi Shintawati Shintawati Shintawati Shintawati Shintawati Shintawati Shintawati Sri Rahayu Widyaningrum Sudibyo Sudibyo Sukma, Vinda Avri Syafaatullah, Achmad Qodim Teguh, Dedi Tri Haryono Windia Hanifah Yuni Susanti Yuni Susanti Yunita Fahni Zuhdi Ma’sum