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All Journal Jurnal Pengolahan Hasil Perikanan Indonesia Jurnal Ilmu dan Teknologi Kelautan Tropis MARINA CHIMICA ACTA Jurnal Kimia Khatulistiwa BERKALA SAINSTEK Al-Kimia ALCHEMY Jurnal Penelitian Kimia Indonesian Journal of Pure and Applied Chemistry CHEESA: Chemical Engineering Research Articles Dalton : Jurnal Pendidikan Kimia dan Ilmu Kimia Molekul: Jurnal Ilmiah Kimia Abdimas Galuh: Jurnal Pengabdian Kepada Masyarakat Jurnal Inovasi Pembelajaran Kimia (Journal Of Innovation in Chemistry Education) Hydrogen: Jurnal Kependidikan Kimia Jurnal Teknologi Kimia Unimal Jurnal Ilmiah Berkala: Sains dan Terapan Kimia Jurnal Akademika Kimia al Kimiya : Jurnal Ilmu Kimia dan Terapan Jurnal Akademika Kimia

Ajuk Sapar

Department Of Chemistry, Tanjungpura University

Author-ID : 2734335

Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Decision Sciences, Operations Research & Management Economics, Econometrics & Finance Education Energy Engineering Environmental Science Industrial & Manufacturing Engineering Law, Crime, Criminology & Criminal Justice Library & Information Science Materials Science & Nanotechnology Mathematics Nursing Physics Social Sciences

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A Preliminary Study of Bioactivity and Identification of Secondary Metabolite Functional Groups in Extracts of Agelas nakamurai Hoshino Sponge from Spermonde Archipelago, Indonesia Ajuk Sapar; Alfian Noor; Nunuk Hariani Soekamto; Tri Aryono Hadi
Marina Chimica Acta Vol. 14 No. 2 (2013): Volume 14 No. 2 (2013)
Publisher : Hasanuddin University

Uji pendahuluan bioaktivitas dan identifikasi gugus fungsi metabolit sekunder ekstrak dalam metanol, n-heksan and metilen klorida dari spons Agelas nakamurai Hoshino, asal pulau Kapoposang, kepulauan Spermonde telah dilakukan. Juga test bioaktivitas dilakukan menggunakan Artemia salina (LC50) untuk mendapatkan konsentrasi letalnya. Hasilnya LC50 adalah 187.932 ppm yang menunjukkan potensi ekstrak sebagai obat anti kanker. Identifikasi komponen dengan reagensia spesifik seperti Lieberman- Burchard, Mayer, Wagner, Dragendorff dan Salkowski ditambah hasil analisis FTIR menunjukkan kandungan komponen ekstrak seperti alkaloid, steroid and terpenoid. Karakteristik pita serapan alkaloid adalah for alkaloid adalah stretching NH at 3600 to 3400 cm-1 dan stretching pendukung C-N at 1250 to 1930 cm-1. Komponen spesifik untuk Agelas nakamurai adalah substitusi bromo dalam alkaloid yang ditandai oleh munculnya pita serapan C-Br medium pada 760 to 745 cm-1.

ISOLATION, IDENTIFICATION AND BIOACTIVITY TEST OF NON POLAR COMPOUNDS ON n-HEXANE EXTRACT OF Haliclona (Reniera) fascigera FROM SAMALONA ISLAND-SPERMONDE ARCHIPELAGO Hafiludin Uli; Alfian Noor; Fredryk Welliam Mandey; Ajuk Sapar
Marina Chimica Acta Vol. 17 No. 2 (2016): Volume 17 No. 2 (2016)
Publisher : Hasanuddin University

Isolation, identification and bioactivity test of nonpolar compunds has been conducted on n-hexane extract sponge Haliclona (Reniera) fascigera of the island Samalona, Makassar, South Sulawesi. Isolation techniques consist of maceration, partition, fractionation using 2 steps using vacuum column chromatography and flash column chromatography and also purification step. Identification of isolate was analyzed with TLC, FTIR, GC-MS, and 1H NMR. The research result was obtained isolate as much as 4 mg and clear solid form. FTIR analysis indicate functional group OH, CH2, CH3, C=O, =CH and C-O. Identification of spot TLC under UV light and spotting solvent show that the spot was active on UV long and short waves and dark brown with cerium sulphate. The results show that isolate A contain aliphatic and alcohol compounds. Bioactivity test results indicate that these isolate A be able to inhibit the growth of bacteria Staphylococus aureus with inhibition zone diameter were 11.60 mm (100 ppm); 10.40 mm (50 ppm); 9.50 mm (25 ppm); 6.50 mm (10 ppm); 6,60 mm (negative control); 17.40 mm (positive control) and against bacteria Escherichia coli with inhibition zone diameter were 6.70 mm (100 ppm); 6,10 mm (50 ppm); 5,90 mm (25 ppm); 5.85 mm (10 ppm); 5,20 mm (negative control); 18.60 mm (positive control).

TOXICITY ASSESSMENT ON NINE SPONGES SPECIES FROM SPERMONDE ARCHIPELAGO Ajuk Sapar; Alfian Noor; Nunuk Hariani Soekamto; Ahyar Ahmad; Tri Aryono Hadi
Marina Chimica Acta Vol. 16 No. 2 (2015): Volume 16 No. 2 (2015)
Publisher : Hasanuddin University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20956/mca.v16i2.2542

Toxicity assessment have been conducted on nine sponges species collected from Spermonde Archipelago namely Kapoposang Island, Samalona Island and Lanjukang Island. Toxicity assessment was using Brine Shrimp lethality Test (BST) method againts sponge extracts. Theresults test were expressed as 50% lethal concentration (LC50) to Artemia salina and correlated with prospecting extract potential as anticancer. All extracts obtained from smallscale extraction by methanol. Test results as follows: Acanthostrongylophora ingens (24.830 μg/mL), Hytios erectus (46.140 μg/mL), Stylissa massa (>1000 μg/mL), Theonella sp (35.010 μg/mL), Niphates olemda (87.500 ppm), Haliclona (Reniera) fascigera (78.160 μg/mL), Petrosia (Petrosia) sp (3.008), Callyspongia (Euplacella) biru (0.515 μg/mL). The test results showed that seven species are potential as anticancer with LC50 value ≤ 500 ppm and only Stylissa massa extracts was not potential as anticancer.

Identifikasi komponen lipofilik fraksi n-heksan spons Agelas nakamurai asal Pulau Randayan Kalimantan Barat (Identification of lipophilic component of n-hexane fraction on Agelas nakamurai Sponge from Randayan Island, West Kalimantan) Ajuk Sapar; Hamzi Anwari; Gusrizal Gusrizal
Marina Chimica Acta Vol. 14 No. 1 (2013): Volume 14 No. 1 (2013)
Publisher : Hasanuddin University

The isolation of lipophilic component of CC_7 on n-hexane fraction of Agelas nakamurai sponge has been conducted. The isolates are liquid oil colorless in 5.1 mg from 53,7 g sample. The isolates were analyzed by GC-MS and FTIR. The results of the analysis isolate CC_7 by FTIR showed the typical vibration of stretching at 2956,87 (asym. –CH3), 2924,09 (asym. –CH2), 2854,65 (sym. -CH3), 1730,15 (C=O), 1662,64 (C=C), 1595,13 (C-C(O)), 1269,16 (C-O), 1186,22 (C-C(O)-O), 1111,00 (O-C-C), 1020,34 (C-O-C-C), 962,48 (=C-H), 678,94 and 657,73 (cis –HC=CH–), bending rocking (-CH2-) at 731,02, bending (-CH2) dan (-CH3) at 1460,11 dan 1373,32. The results of GC-MS analysis showed the lipophilic component such as methyl palmitate (tR 19,77; m/z = 270), ethyl palmitate (tR 21,07; m/z = 284), palmitic acid (tR 21,18; m/z = 256, ethyl oleate (tR 24,09; m/z 310), tributyl asonitate (tR 24,38; m/z = 342), tributyl citrate (tR 24,95), tributyl acetyl (tR 26,41; m/z = 402), dioctyl adipate (tR 28,11; m/z =m 370, and squalene (tR 30,30; m/z 410).

Co-Authors . Daryati . Kadarisno Abrori, Sayyidus Dzaki Adhitiyawarman, Adhitiyawarman Adiwijaya, Margharet Esterlita Ahyar Ahmad Ahyar Ahmad Alfian Noor Alfian Noor Alfian Noor Alfian Noor Alimunddin, Andi Hairil Andi Hairil Alimuddin Andi Hairil Alimuddin Anis Shofiyani Anita Anita Anthoni B. Aritonang Ari Widiyantoro Aritonang, Anthoni Batahan Asma, Al Desi Listiani Eka Pebri Malinda Eka Wahyuni Endah Sayekti Erlina Erlina Erlina Ersando, Ersando Fitriani Fitriani Fredryk Welliam Mandey Guntur Guntur Gusrizal Gusrizal Hafiludin Uli Hamzi Anwari Hariyanti, Weni Harlia Harlia Harlia, Harlia Khofifah Aditha Parawansa Lestari, Titiek M Agus Wibowo Masriani . Millenia Millenia Millenia, Millenia Nelly Wahyuni Nunuk Hariani Soekamto Parawansa, Khofifah Aditha Prayitno, Dwi Imam Puji Ardiningsih Puji Ardiningsih Rahayu, Warsi Kurnia Risa Nofiani Risa Nofiani Risya Sasri Rizki Noviani Ridwan Rudiyansyah Rudiyansyah Rudiyansyah Rudiyansyah Rudiyansyah Rudiyansyah Rudiyansyah Rudiyansyah Sari, Heni Puspita Sasri, Risya Septian Triadi Syahputra Siti Nurbetty Sri Juari Santosa Sri Wahyuni Sulistyo, Luthfi Imam Thamrin Usman Titin Anita Zahara, Titin Anita Titin Anita Zaharah Tri Aryono Hadi Tri Aryono Hadi Uci Pradina Uswatun Hasanah Wardani, Fina Rika Warsidah Warsidah Wibowo, M. Agus Wibowo, Muhamad Agus Widiyananta, Surya Winda Rahmalia Winda Rahmalia Zaharah, Titin Anita

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