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All Journal VALENSI CAKRA KIMIA (Indonesian E-Journal of Applied Chemistry) Jurnal Kimia (Journal of Chemistry) CHEMISTRY PROGRESS International Journal of Science and Engineering (IJSE) Jurnal Penelitian Sains (JPS) Jurnal Kedokteran Brawijaya Jurnal Matematika & Sains Bulletin of Chemical Reaction Engineering & Catalysis The Journal of Pure and Applied Chemistry Research AGRIVITA, Journal of Agricultural Science Jurnal Penelitian Sains (JPS) IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) JPSriwijaya Indonesian Journal of Chemical Science Science and Technology Indonesia Jurnal Penelitian Sains Indonesian Journal of Chemistry Communications in Science and Technology IJEMS (Indonesian Journal of Environmental Management and Sustainability) Riau Journal of Empowerment Molekul: Jurnal Ilmiah Kimia Sains dan Matematika SRIWIJAYA JOURNAL OF ENVIRONMENT Makara Journal of Science Makara Journal of Technology Aceh International Journal of Science and Technology Karunia: Jurnal Hasil Pengabdian Masyarakat Indonesia Bulletin of Chemical Reaction Engineering & Catalysis Indonesian Journal of Material Research Bumi: Jurnal Hasil Kegiatan Sosialisasi Pengabdian Kepada Masyarakat
Aldes Lesbani
Universitas Sriwijaya
Agriculture, Biological Sciences & Forestry Humanities Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Decision Sciences, Operations Research & Management Earth & Planetary Sciences Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Health Professions Law, Crime, Criminology & Criminal Justice Materials Science & Nanotechnology Mathematics Mechanical Engineering Medicine & Pharmacology Neuroscience Physics Public Health Social Sciences

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Journal : VALENSI

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Sintesis Satu Langkah Senyawa Oksotrinuklir dengan Terminal Ligan Piridin [Ru3O(OOCC6H5)6(C5H5N)3]ClO4 Aldes Lesbani; Risfidian Mohadi; Eliza Eliza
Jurnal Kimia Valensi Jurnal Valensi Volume 3, No.2, November 2013
Publisher : Syarif Hidayatullah State Islamic University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (351.263 KB) | DOI: 10.15408/jkv.v3i2.508

Abstract

Abstrak Telah disintesis senyawa oksotrinuklir dengan terminal ligan piridin [Ru3O(OOCC6H5)6(C5H5N)3]ClO4. Senyawa oksotrinuklir hasil sintesis dikarakterisasi menggunakan spektrofotometer FT-IR dan spektrometer massa. Hasil identifikasi dengan spektrofotometer FT-IR menunjukkan senyawa oksotrinuklir hasil sintesis memiliki vibrasi khas pada bilangan gelombang 698 cm-1. Pengukuran menggunakan spektrometer massa menkonfirmasi bahwa senyawa oksotrinuklir memiliki ligan terminal piridin yang mudah terfragmentasi yang ditandai dengan puncak ion molekul pada m/z 1283,14 dan puncak ion fragmen pada m/z 1205,09 yang mengindikasikan lepasnya satu molekul piridin sebagai terminal ligan. Kata kunci : senyawa oksotrinuklir, sintesis satu langkah, ruthenium, piridin.   Abstract Synthesis of oxotrinuclear with pyridine as terminal ligand [Ru3O(OOCC6H5)6 (C5H5N)3]ClO4 has been carried out. Oxotrinuclear compound from synthesis was characterized using FT-IR spectrophotometer and mass spectrometer. The FTIR spectrum shows that oxotrinuclear compound has vibration at wavelength 698 cm-1 and mass spectrometer spectrum shows oxotrinuclear compound has pyridine as terminal ligand which easily fragmented indicated by molecular ion peak at m/z 1283.14 and ion fragment peak at m/z 1205.09. These values revealed one molecule of pyridine lost from terminal ligand. Keywords : oxotrinuclear compound, one step synthesis, ruthenium, pyridine.
Sintesis Tris(4-metoksifenil)tolilsilan dengan Teknik Reaksi Kopling Menggunakan Katalis Paladium Tersier Tributil Fosfin Aldes Lesbani; Risfidian Mohadi; Eliza Eliza
Jurnal Kimia Valensi Jurnal Valensi Volume 3, No.1, Mei 2013
Publisher : Syarif Hidayatullah State Islamic University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (272.857 KB) | DOI: 10.15408/jkv.v3i1.332

Abstract

Telah disintesis senyawa tris(4-metoksifenil)tolilsilan (TMT) dengan teknik reaksi kopling menggunakan tolilsilan dan 4-iodida anisol yang dikatalis senyawa paladium. Reaksi dilakukan dalam kondisi inert dan suasana basa. Senyawa TMT hasil sintesis dikarakterisasi menggunakan kromatografi gas-spektrometri massa dan spektrometer 1H dan 13C NMR. Hasil penelitian menunjukkan bahwa senyawa TMT hasil sintesis memiliki rendemen sebesar 30%. Pengukuran menggunakan kromatografi gas-spektrometri massa menghasilkan nilai m/z sebesar 440. Spektrum 1H NMR menunjukkan lima puncak proton ekivalen dan spektrum 13C NMR menghasilkan sepuluh puncak karbon ekivalen. Hasil karakterisasi tersebut bersesuaian dengan struktur senyawa TMT hasil sintesis.   Kata kunci: tris(4-metoksifenil)tolilsilan, reaksi kopling, paladium
Co-Authors A. Agnes Abi Sueb Abriyanto, Danang Addy Rachmat Adi Saputra Adi Saputra Adi Saputra Adi Saputra Afifah Rahma Dian Ahmad Fatoni Ahmad Fatoni Alfan Wijaya Alfan Wijaya Alfan Wijaya Amiruddin Supu Amri Amri Amri Andi Wijaya Andreas, Roy Andriani Azora Andriani Azora Anggraini, Ana Arini Fousty Badri Arini Fousty Badri Arison Musri Arison Musri Arsyad, Fitri Suryani Aslihati Aslihati Aslihayati Aslihayati Azhar Kholiq Badri, Arini Fousty Bakri Rio Rahayu Bakri Rio Rahayu Benyamin Lakitan Dedi Rohendi Dedi Setiabudidaya Desnelli Desnelli Dian Monariqsa Dian Monariqsa Didi Jasantri Dormian A N Haloho Dormian A N Haloho Eiffel Ostan Jeski Gultom Elfita Elfita . Elfita Elfita Eliza . Eliza Eliza Eliza Eliza Ema Veronika Turnip Endri Junaidi Eriza Sativa Erviana, Desti Fahma Riyanti Fatmawati Fatmawati Ferlinahayati Ferlinahayati Fitri Suryani Arsyad Fitri, Erni Salasia Fitriliana Fitriliana Hanifah, Yulizah Haris Kriswantoro Hermansyah Hermansyah Hermansyah Hermansyah Hesti A. Harahap Hesti A. Harahap, Hesti Hidayatullah, Muhammad Hilda Zulkifli Hilda Zulkifli Hilda Zulkifli Hiroshi Nishihara Hitoshi Kondo Idha Royani Intan Permata Sari Irfannuddin Irfannuddin Jasantri, Didi Jefri Jefri Jeri Ramadhan Juleanti, Novie Kiki Anggraini Kiki Anggraini Kiki Anggraini, Kiki Komis Krisna Murti Laila Hanum Leni Sinaga Lestari Simanjuntak Lestari Simanjuntak Liasari, Beta Riana Lingga, Fitra Wahyuni Lora Vitanesa Lucyanti . Lucyanti Lucyanti Lusi Teresia Mardianto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto Mardiyanto, Marieska Verawaty Mariska Verawaty Melantina Melan Oktriyanti Melwita, Elda Menik Setyowati Mikha Meilinda Christina Miksusanti Miksusanti Muhammad Imron MUHAMMAD SAID Muhammad Said Muhammad Said Muhammad Said Najma Annuria Fithri Najma Annuria Fithri Najma Annuria Fithri Najma Annuria Fithri, Najma Annuria Narsito Narsito Neza Rahayu Niken Oktora Niken Oktora Nirwan Syarif Normah Normah Normah Normah, Normah Nova Yuliasari Novie Juleanti Novie Juleanti Novie Juleanti Nur Ahmad Nur Ahmad, Nur Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nurlisa Hidayati Nur’aini, Siti Nyanyu Ummu Hani Palita Tamba Patimah Mega Syah Bahar Nur Siregar Patimah Mega Syah Bahar Nur Siregar Patimah Mega Syah Bahar Nur Siregar Poedji Loekitowati Hariani Putri Erlyn Putri, Bunga Indah R.A. Mika Melviana Rabelia Juladika Sayeri Radja Nardo Purba Rakhmawati Farma Ramadhan, Jeri Rananda Vinsiah Randi O. Saragih Ratna, L.P Ratna, L.P Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risfidian Mohadi Risma Kurniawati M Rohmatullaili Rohmatullaili, Rohmatullaili Roy Andreas Sabat Okta Ceria Sitompul, Sabat Okta Ceria Samat Samat Savira, Dila Setiawan Yusuf Setiawati Yusuf Setiawati Yusuf Sherly Agustina, Sherly Siregar, Patimah Mega Syah Bahar Nur Sitanggang, Jonra P. Soerya, Balada Sri Juari Santosa Suheryanto Suheyanto Suheryanto Sumiati Sumiati SUMIATI, Susila Arita Syaflina Lamin Syafrina Lamin, Syafrina Tamizi Taher Tarmizi Taher Welinda Me Wibiyan, Sahrul Wijaya, Alfan Winda Fitriana Yeni Iswanti Yoshinori Yamanoi Yosi Saria Yosi Saria Yosi Saria Yosine Susi Yosine Susie Yunita Irianty Zahara, Zaqiya Artha Zazili Hanafiah Zultriana