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Journal : Molekul: Jurnal Ilmiah Kimia

Direct Extraction and Conversion of Microalgal Lipid from Chlorella vulgaris to Biodiesel Through In Situ Process Assisted by Sonication Wulandari, Melysa; Hadi, Sofijan; Purkan, Purkan; Sumarsih, Sri; Abdulloh, Abdulloh; Wahyuni, Dwi Kusuma; Piluharto, Bambang
Molekul Vol 19 No 1 (2024)
Publisher : Universitas Jenderal Soedirman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20884/1.jm.2024.19.1.10042

Abstract

Direct extraction and conversion of microalgal lipid to biodiesel in one step process is developed to initiate an efficiently method in the biofuel production. The method that called as in-situ process had been applied in the biodiesel production from microalgae Chlorella vulgaris lipid by involving of sonication assisting. Various parameters that affect the in-situ transesterification were investigated to find the optimum conditions including power of sonication, co-solvent use, and biomass amount. The experiment was performed by acidic catalyst The use of sonication in 25kHz/270W yielded the highest biodiesel product. The apply of co-solvent n-hexane significantly increased the yield biodiesel rather than no co-solvent. The biodiesel yield of 10.39 % obtained when the process was accompanied by the n-hexane.as co-solvent with increasing level as 47% rather than without co-solvent. The in situ process in the ratio biomass - methanol 3:50 that assisted by sonication for 60 mins produced the highest biodiesel, which was 20,31 % w/w. The yield was higher than assisting with reflux or combination of reflux-sonication. The component of biodiesel yielded in the process consisting of 7,10,13-hexadecatrienoic methyl ester; pentadecanoic acid, 14-methyl-methyl ester; 9,12,15-octadecatrienoic acid-methyl ester; and eicosanoic acid-methyl ester. Joining of reflux-sonication exhibited a low biodiesel product. Disadvantage method from the combination may inhibit on lipid extraction or FAME transformation, the exact cause needs to be looked for in the future. Keywords : Biodiesel, in-situ transesterification, microalgae Chlorella vulgaris, sonication
Co-Authors A. Budi Prasetyo A.A. Ketut Agung Cahyawan W Abdulloh Abdulloh AFAF BAKTIR Ahlan Riwahyu Habibi Ahmadi Jaya Permana Alfa Akustia Widati Ali Rohman Ami Soewandi J.S. Andi Hamim Zaidan Aning Purwaningsih Antyka Lutfiana Putri Aryati Aryati Ati, Nur Ing Atik Widiyanti Aulianitha Salsabella B. Sulistiyanto Badi’atul Azizah Bambang Piluharto Bambang Sulistiyanto Budi Prasetyo, Antonius Budi Putri Ayu Andina Budi Putri Ayu Andina, Budi Putri Ayu C.I. Sutrisno Cahya Setya Utama Cornelius Imam Sutrisno Dwi Kusuma Wahyuni Dwi Sunarti Edjeng Suprijatna Faiq Nadiatul Mardia Asa Fajrina, Ishmah Tri Faozi, Ahmad Aziz Fatiha Khairunnisa Fatimah Fatimah Fatimah Ganden Supriyanto Gilva Illavi Hamami Handoko Darmokoesoemo Hanny Indrat Wahyuni Harini Nur Hikmah Harsasi Setyawati Hartati Hartati Hartati Hartati Haryanto, Darban Hera Lisna Ginawati Hery Suwito Hwei Voon, Lee Ilham Harlan Amarullah Intan Ayu Pratiwi, Intan Ayu Kariza Makanty Kautsar Ul Haq Kris Cahyo Mulyatno, Kris Cahyo Luthfi Djauhari Mahfudz Masanori Kameoka, Masanori Maylina Ilhami Khurniyati Ma’rifah, Binti Mei Shirli Yasinta Miratul Khasanah Mochamad Zakki Fahmi Mochammad Imron Awalludin Muji Harsini Mulyadi Tanjung Mustofa, Rudian Ni Nyoman Tri Puspaningsih Nira Ambar Arum Ni’matuzahroh Ni’matuzahroh Novia Fajarwati, Novia Nur Cholifah NUR CHOLIFAH One Asmarani Purkan Purkan Purkan Purkan, Purkan Purwaningsih, Aning Qurrota A’yuni Rahayu, E.S Rico Ramadhan, Rico Rike Cahyo Probowati Rina Muryani Rizka Diah Fitri Sarjana, Teysar Adi Sevia Ayuningtyas Shihah, Hanna Dzawish Siti Churrotin, Siti Siti Wafiroh Soegeng Soegijanto Sofijan Hadi Solly Aryza Sri Kismiati, Sri Sri Mukodiningsih Sri Subekti Sulistiyanto, B Tampoebolon, B. I. M. Teguh Hari Sucipto, Teguh Hari Tini Surtiningsih Tokok Adiarto Tokok Ardiarto Tomohiro Kotaki, Tomohiro Ueda, Shuhai Uswatun Chasanah Virgawati, Sari Wahyuni, Nur Maulida Wardhani, Puspa Wulandari, Melysa Yanuardi Raharjo, Yanuardi