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All Journal International Journal of Renewable Energy Development Bulletin of Chemical Reaction Engineering & Catalysis Journal of Degraded and Mining Lands Management The Journal of Pure and Applied Chemistry Research IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Biomedical Journal of Indonesia Science and Technology Indonesia Jurnal Penelitian Sains Indonesian Journal of Chemistry Communications in Science and Technology Molekul: Jurnal Ilmiah Kimia Jurnal Gema Ngabdi Jurnal Abdi Insani Jurnal Pengendalian Pencemaran Lingkungan (JPPL) Budapest International Research and Critics Institute-Journal (BIRCI-Journal): Humanities and Social Sciences Jurnal Altifani Penelitian dan Pengabdian kepada Masyarakat SRIWIJAYA JOURNAL OF ENVIRONMENT Makara Journal of Science Jurnal Pepadu Jurnal Ruaya : Jurnal Penelitian dan Kajian Ilmu Perikanan dan Kelautan Aceh International Journal of Science and Technology Molekul: Jurnal Ilmiah Kimia Bulletin of Chemical Reaction Engineering & Catalysis Analit: Analytical And Environmental Chemistry
Poedji Loekitowati Hariani
Department Of Chemistry, Universitas Sriwijaya
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Photocatalytic degradation of methylene blue and Congo red dyes from aqueous solutions by bentonite-Fe3O4 magnetic Riyanti, Fahma; Hasanudin, Hasanudin; Rachmat, Addy; Purwaningrum, Widia; Hariani, Poedji Loekitowati
Communications in Science and Technology Vol 8 No 1 (2023)
Publisher : Komunitas Ilmuwan dan Profesional Muslim Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21924/cst.8.1.2023.1007

Abstract

This study describes the co-precipitation synthesis of magnetic bentonite-Fe3O4 for photocatalytic degradation of methylene blue and Congo red pigments under visible light. Bentonite-Fe3O4 composites were produced using the mass ratio of 2:1 and 1:1 for bentonite to Fe3O4, respectively. X-ray Powder Diffraction (XRD), Fourier Transform Infra-Red (FTIR), BET surface area, Vibrating-Sample Magnetometer (VSM), Scanning Electron Microscopy with Energy Dispersive Spectroscopy (SEM-EDS), and Ultraviolet–Visible Diffuse Reflectance Spectroscopy (UV DRS) were used to characterize the materials. The bentonite-Fe3O4 (1:1) composite exhibited a greater surface area in comparison to the bentonite-Fe3O4 (2:1) composite with a measured value of 106.6 m2/g. It is a superparamagnetic material with a band gap of 2.25 eV and a saturation magnetization of 69.64 emu/g. The photocatalytic degradation of dye using bentonite-Fe3O4 (1:1) with the initial dye concentration of 25 mg/L, volume of 50 mL, catalyst dose of 0.05 g/L, addition of 3 mL H2O2, and 90 minutes of visible irradiation resulted in 94.34% and 98.45% degradation efficiency of methylene blue and Congo red dyes, respectively. The study determined that the most favorable pH for the photocatalytic degradation of methylene blue was pH 11, whereas the optimal pH for Congo red was found at pH 5. For methylene blue and Congo red dyes, photocatalytic degradation followed pseudo-first-order with the constant rates of 0.0356 min-1 and 0.0348 min-1, respectively. After five cycles of use in the photocatalytic process, the catalyst's degradation efficiency fell into below 5%. This research demonstrated that catalysts could be utilized in wastewater treatment technology.
Optimization Photodegradation of Methylene Blue Dye using Bentonite/PDA/Fe3O4@CuO Composite by Response Surface Methodology Riyanti, Fahma; Hariani, Poedji Loekitowati; Hasanudin, Hasanudin; Rachmat, Addy; Purwaningrum, Widia
Bulletin of Chemical Reaction Engineering & Catalysis 2024: BCREC Volume 19 Issue 2 Year 2024 (August 2024)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20132

Abstract

This study aims to synthesize bentonite/PDA/Fe3O4@CuO composites as a catalyst for the photodegradation of Methylene blue dye. Composite characterization involves X-ray Diffractometry (XRD), Scanning Electron Microscopy (SEM) with X-ray Energy Dispersion Spectrometry (EDS), UV-Vis Diffuse Reflectance Spectroscopy (UV-Vis DRS), and Vibrating Sample Magnetometer (VSM). Response Surface Methodology (RSM) employs Central Composite Design (CCD) to optimize photodegradation by varying dye concentration, irradiation time, and catalyst dose. The bentonite/PDA/Fe3O4@CuO composites exhibit a saturation magnetization value of 54.82 emu/g and a band gap of 2.1 eV. The optimization revealed that concentration and dose significantly impact the photodegradation efficiency. A quadratic model is suitable for modeling the photodegradation of Methylene blue dye using bentonite/PDA/Fe3O4@CuO composites, as determined by analysis of variance (ANOVA). The optimal conditions for achieving maximum photodegradation efficiency were identified as a dye concentration of 10 mg/L, an exposure time of 90 min, and a catalyst dose of 1.67 g/L. Under these parameters, the photodegradation process exhibited a remarkable efficiency of 100%. The Bentonite/PDA/Fe3O4@CuO composites exhibited strong stability, efficiency, and recyclability. After six photodegradation cycles, there was a 5.18% decrease in photodegradation efficiency. Copyright © 2024 by Authors, Published by BCREC Publishing Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Synthesis and Characterization of Nanoparticle Composite CaO/Fe3O4 from Duck Egg Shells and Its Application for Congo Red and Procion Red MX-5b Dyes Adsorption Purwaningrum, Widia; Riyanti, Fahma; Julinar, Julinar; Hariani, Poedji Loekitowati; Ahadito, Bijak Riyandi; Chodijah, Siti; Safira, Vika Putri
IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Vol 9, No 2 (2024): June 2024
Publisher : IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24845/ijfac.v9.i2.103

Abstract

In order to improve the adsorption performance of CaO prepared from duck egg shells, a 1:1 composite of CaO/Fe3O4 were synthesized using a coprecipitation method. This composite was then used to adsorb Congo red and Procion red MX-5b dyes from an aqueous solution. The adsorption process was studied by investigating the effects of contact time, temperature, and initial concentration of dye. It was found that the optimum conditions for Congo red adsorption are 50 minutes of contact, 50 °C, and 225 mg/L of dye, while for Procion red MX-5b the conditions are 50 minutes of contact, 60 °C, and 250 mg/L of dye. The behavior of both adsorbents at equilibria follows a pseudo-second-order kinetic model and Langmuir isotherm, with the adsorption capacity at optimum condition for Congo red and Procion red MX-5b 46.95 mg/g and 47.39 mg/g, respectively. Thermodynamics studies showed that the adsorption process of Congo red was endothermic, while Procion red MX-5b was exothermic, yet both were found to happen spontaneously.
Comparison of Alum and Coal-Based Activated Carbon for the Treatment of Raw Water Subroto, Subroto; Said, Muhammad; Ibrahim, Eddy; Hariani, Poedji Loekitowati
IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Vol 10, No 1 (2025): February 2025
Publisher : IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24845/ijfac.v10.i1.23

Abstract

The availability of clean water is an essential element for supporting the life cycle and sustainable development. The efficiency of providing raw water sources is an important factor for adequate water quantity and quality. This study examines the effectiveness of alum compared with coal-based activated carbon in the removal of Fe, Mn, and turbidity in raw water from the Lematang River, Muara Enim Regency. Activated carbon in this study was produced using a KOH activator with varying activation temperatures (700 °C, 800 °C, and 900 °C). The research results showed that the quality of the third activated carbon met the active carbon quality standards (moisture, ash content, Methylene blue dye and iodine adsorption capacity), but the activated carbon with activation at a temperature of 800 °C had the largest surface area. Activated carbon was proven more effective in reducing Fe and Mn concentrations than alum, while alum was superior in reducing turbidity. After three cycles of activated carbon regeneration, the reduction in Fe and Mn remained below 5%. These results show that activated carbon is a cost-effective and eco-friendly option for raw water treatment.Keywords: Coal, activated carbon, alum, raw water, regeneration
Study of Mangan Peroxidase (Mnp) Enzymes from Pleurotus Ostreatus Produced using Coffee Grounds and Rice Bran as Substrates through Response Surface Methodology Jannah, Mifthahul; Hermansyah, Hermansyah; Hariani, Poedji Loekitowati
IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Vol 10, No 1 (2025): February 2025
Publisher : IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24845/ijfac.v10.i1.68

Abstract

This study aimed to optimize the production of Manganese Peroxidase (MnP) enzyme from Pleurotus ostreatus using agricultural waste substrates such as coffee grounds (CG) and rice bran (RB) through Response Surface Methodology (RSM) approach. Optimization was conducted using a Central Composite Design (CCD) with three main variables, namely MnSO₄ concentration (0.5-1.5) mM, incubation temperature (25-35) °C, and reaction time (20-30) min. The enzyme fractionation process was carried out by ammonium sulfate saturation (0-20%), (20-40%), (40-60%), followed by dialysis, and SDS-PAGE analysis. The results showed that the 0-20% fraction of CG:RB (50:50) substrate had the highest enzyme activity, which was 20.588 ± 0.141 U/mL, with the highest specific activity of 76.967 ± 0.325 U/mg. The highest protein content was found in CG:RB (0:100) substrate at 0.825 ± 0.016 mg/mL. However, the enzyme activity was lower due to the presence of non-enzymatic proteins and natural inhibitors. This study successfully demonstrated that the substrate combination of CG:RB (50:50) provided optimal results for MnP production. The Response Surface Methodology proved effective in optimizing process variables, providing great potential for biotechnology applications using agricultural waste as an environmentally friendly raw material.Keywords: Pleurotus ostreatus, Manganese Peroxidase, Coffee Dregs, Rice Bran, RSM, SDS-PAGE
Fabrication of NiFe2O4/SiO2/TiO2 Magnetic Composite for Effective Photodegradation of Congo Red Dye Hariani, Poedji Loekitowati; Salni, Salni; Kimur, Melviana Violetta; Hidayati, Nurlisa; Elfita, Elfita
Indonesian Journal of Chemistry Vol 25, No 3 (2025)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.94143

Abstract

This study aims to fabricate a NiFe2O4/SiO2/TiO2 magnetic composite to serve as a photocatalyst for the degradation of Congo red dye. The catalyst characterization involved XRD, FTIR, UV-vis DRS, BET, VSM, SEM-EDS, and pHpzc analyses. The performance in degradation was determined by the effect of various variables, including solution pH, dye concentration, and irradiation time. Results revealed that the NiFe2O4/SiO2/TiO2 composite exhibited a crystallite size of 24.56 nm and a bandgap of 2.1 eV. The surface area of NiFe2O4/SiO2/TiO2 was measured at 154 m2/g, exceeding that of NiFe2O4/SiO2 and NiFe2O4, which were observed at 122 and 51 m2/g, respectively. NiFe2O4/SiO2/TiO2 exhibited magnetic properties with a magnetic saturation of 18.55 emu/g. Under optimal conditions (pH 5, initial dye concentration of 20 mg/L, and 90 min of visible irradiation), the degradation efficiency reached 96.86%. It was concluded that the photodegradation was effective, as its efficiency decreased from 96.86 to 92.45% after five reuse cycles. The presence of mineralization was evaluated using total organic carbon analysis, which revealed an 84.60% reduction in carbon content.
Pelatihan Pembuatan Sabun Transparan Antibakteri Berbahan Ekstrak Daun Mengkudu (Morinda Citrifolia L.) sebagai Upaya Pemberdayaan Masyarakat di Desa Tanjung Atap, Ogan Ilir Harmida, Harmida; Tanzerina, Nina; Lamin, Safrina; Salni, Salni; Aminasih, Nita; Hariani, Poedji Loekitowati
Jurnal Altifani Penelitian dan Pengabdian kepada Masyarakat Vol. 5 No. 3 (2025): Mei 2025 - Jurnal Altifani Penelitian dan Pengabdian kepada Masyarakat
Publisher : Indonesian Scientific Journal

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.59395/altifani.v5i3.679

Abstract

Tanaman mengkudu (Morinda Citrifolia L.) telah dikenal masyarakat sebagai salah satu tanaman sebagai sumber obat tradisional. Ekstrak daun mengkudu mengandung senyawa bioaktif seperti fenolik, flavonoid dan antrakuinon yang bersifat antibakteri dan antioksidan. Pemanfaatan ekstrak daun mengkudu sebagai bahan sabun padat transparan antibakteri untuk mendukung pengembangan produk alami, aman digunakan, dan yang paling utama adalah meningkatkan kebersihan dan kesehatan masyarakat. Kegiatan pengabdian masyarakat ini bertujuan memberikan pelatihan pembuatan sabun transparan antibakteri dari ekstrak daun mengkudu yang dilakukan di desa Tanjung Atap, kecamatan Tanjung Batu, kabupaten Ogan Ilir. Kegiatan diikuti oleh ibu-ibu dan remaja putri sebanyak 30 orang. Metode kegiatan meliputi penyuluhan, pelatihan dan evaluasi hasil kegiatan. Hasil pre-test dan pos-test menunjukkan terjadinya peningkatkan pengetahuan peserta tentang sabun transparan antibakteri yang dari ekstrak daun mengkudu. Peserta yang menjawab pertanyaan dengan tepat dari sebelum pelatihan sebanyak 18,75% meningkat menjadi 76,67% setelah pelatihan. Selain itu masyarakat juga menyukai produk sabun yang dihasilkan. Hal ini mengindikasikan keberhasilan kegiatan pelatihan yang diberikan.
PELATIHAN PEMBUATAN LULUR WAJAH DARI DAUN SIRSAK (Annona Muricata L) UNTUK MENDAPATKAN KULIT SEHAT DI DESA TANJUNG ATAP Hariani, Poedji Loekitowati; Fatma, Fatma; Said, Muhammad; Ahadito, Bijak Riyandi; Rohendi, Dedi
Jurnal Pepadu Vol 6 No 1 (2025): Jurnal Pepadu
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/pepadu.v6i1.6149

Abstract

Facial scrubs are a part of skin care that is often done by mothers and young women. In line with back to nature awareness, body scrubs use ingredients from natural sources. This community service activity aims to provide counseling and training on the importance of skin care and making facial scrubs from soursop leaves. Soursop leaves contain bioactive ingredients which are antioxidant and antibacterial. The activity was carried out in Tanjung Atap village, Tanjung Batu sub-district, Ogan Ilir district and was attended by 26 participants. The soursop plant is easy to find in the village growing in the yard. Activity participants play an active role in activities both in counseling and training. Evaluations are carried out before and after the activity to determine the level of participants' understanding of the counseling and training provided. Apart from that, an organoleptic test was carried out to determine the level of acceptance of the body scrub product. The results of the activity showed that there was an increase in public understanding of the importance of maintaining healthy skin and making body scrubs from soursop leaves. The increase in participants' understanding was 93.03% from not understanding or not understanding. The organoleptic test results showed that 85.36% of participants said they really liked it and 14.64% said they liked the facial scrub product made from soursop leaves. With this service activity, people are increasingly aware of the importance of skin care using natural resources. Scrubs made from natural ingredients are safe, cheap and avoid the side effects of chemicals.
Synthesis of Ag/CeO2 Nanocomposites with Noni Leaf Extract and Its Potential Antibacterial Properties Denada, Laellia; Hariani, Poedji Loekitowati; Aprianti, Nabila
IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Vol 10, No 3 (2025): October 2025
Publisher : IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

This study aims to perform green synthesis of Ag/CeO2 nanocomposites using noni leaf extract and to test their potential antibacterial activity. The synthesis results were characterised using X-ray Diffraction (XRD) to determine crystallite size, Scanning Electron Microscope-Energy Dispersive Spectroscopy (SEM-EDX) to observe morphology and elemental composition, and Fourier Transform Infrared Spectroscopy (FTIR) to identify functional groups. The XRD characterization results showed the formation of typical Ag/CeO2 peaks with an average crystallite size of 15,28 nm. SEM analysis revealed morphology in the form of aggregates with varying sizes. EDX results confirmed the presence of Ag, Ce, and O elements. FTIR analysis showed the presence of typical Ce–O group absorption bands, which supports the successful synthesis of Ag/CeO2. The synthesized nanocomposites were then tested for their antibacterial activity against Escherichia coli and Staphylococcus aureus bacteria. Antibacterial activity tests showed the formation of an 8 mm zone of inhibition (ZOI) at a concentration of 5000 ppm, demonstrating the potential of the synthesized green Ag/CeO2 as an antibacterial agent. This study confirms that the use of noni leaf extract as a reducing and stabilizing agent is an environmentally friendly approach and has potential for environmental applications.
Modification of Activated Carbon from Palm Kernel Shells with Fe₃O₄ Magnetic for Water Treatment of Enim River Damayanti, Damayanti; Arita, Susila; Hariani, Poedji Loekitowati
IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Vol 10, No 3 (2025): October 2025
Publisher : IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

The economical, easy-to-implement, and regenerative treatment methods are essential to obtain clean water. In this study, activated carbon was synthesized from palm kernel shells using ZnCl₂ as an activator. The activated carbon was then modified with Fe₃O₄. The resulting activated carbon and activated carbon-Fe₃O₄ product were characterized using XRD, SEM-EDX, VSM, and BET surface area analysis. Furthermore, activated carbon-Fe3O4 was applied to reduce Fe ions, turbidity, and total suspended solids (TSS) and increase the pH value in Enim river water. The resulting activated carbon has met SNI standards, with a moisture content of 8.81%, ash content of 5.475%, and an iodine adsorption capacity of 1763.86 mg/L. The synthesized activated carbon-Fe₃O₄ exhibits strong magnetic properties, with a saturation magnetization value of 68.82 emu/g and a surface area of 355.42 m²/g. Optimal conditions for the treatment of Enim river water were obtained at an adsorbent dose of 40 mg/L, a stirring rate of 120 rpm, and a stirring time of 120 minutes. Under these conditions, the Fe ion reduction efficiency reached 96.95%, turbidity 89.83%, and TSS 80.74%, while the pH increased from 6.23 to 6.74. FTIR analysis showed a change in peak intensity in the activated carbon-Fe₃O₄ after the adsorption process, indicating interaction with contaminants. The adsorption process of Fe ions by activated carbon-Fe₃O₄ follows a pseudo-second-order kinetic model.
Co-Authors Abdullah Abdullah Addy Rachmat Addy Rachmat Ahmad Fatoni Ahmad Fatoni Ahyati Fadilah Aldes Lesbani Aldi Herbanu Amallia, RA Hoetary Tirta Amri, Nanda Hasanul Annisa Filantropie Aria Septi Handayani Aroef, Hukmanan Rais Asia Asia Afriyani Astri Nurmayansih Bijak Riyandi Ahadito Damayanti Damayanti Dedi Rohendi Denada, Laellia Desneli Desneli Desnelli Desnelli Eddy Ibrahim Elfita Elfita Elfita Elfita Endri Junaidi Evi Yuliana, Evi Fahma Riyanti Fatma Fatma Febrina Sari Ferlinahayati Ferlinahayati Handayani Citra Pratiwi Hanifa, Hanifa Marisa Harmida Harmida Hasanudin Hasanudin Heni Oktaviani Heni Yohandini Hermansyah Hermansyah Hermansyah Hermansyah Hermansyah Hermansyah Hermansyah Herpandi . Hery Widijanto Hesti Ratnasari, Hesti Hidayat, Bachtari Alam Hilda Zulkifli Indah Hamida Iqlima Amelia Irfannuddin Irfannuddin Izzati Izzati Julinar Julinar Juswardi Juswardi Kasmiarti, Getari Kimur, Melviana Violetta Lamin, Safrina Leily Nurul Komariah Lilian Novarika M. B. Prayitno Maulana Yusuf Melly Oktaria Mgs. Irsan Saleh Mifthahul Jannah Muhammad Faizal Muhammad Faizal Muhammad Irsan Saleh Muhammad Ramdan Abdul Mannan Muhammad Said Muhammad Said Muhammad Said Muhammad Said MUHAMMAD SAID Muhammad Said Muryati Muryati Mustafa Kamal Nabila Aprianti Nina Tanzerina Nirmalasary, Try Nensy Nita Aminasih Novia Novia Nur Hanis Hayati Hairom Nurlisa Hidayati Nurlisa Hidayati Purwitasari, Listiyani Putri Erlyn Rani Nawang Sari Ratu Wulandari Permatasari Putri Risfidian Mohadi Risfidian Mohadi Riski Dita Asmara Rizki Indah Putri Rizki, Widya Twiny Robert Sibarani, Robert Robiyanto Hendro Susanto Sabila Yunita Safira, Vika Putri Safitri, Bella Salni Salni Salni Salni Salni Salni Salni Salni Salni Salni Sari, Febrina Setiyawan, Bambang Dwi Shella Santika Damarril Singgih Tri Wardana Sisca, Vivi Siti Chodijah Siti Nuraini Sri Hartika Subroto Subroto Suheyanto Suheryanto Susila Arita Vilantina, Vilantina Widia Purwaningrum Wiwin Sepriani Yogi Astrada Zainal Arifin Zazili Hanafiah Zulfikar Zulfikar