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Edi Suharyadi
Universitas Gadjah Mada
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Journal : Empiricism Journal

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Characterization of Crystal Structures and Magnetic Properties of Polyethylene Glycol (PEG-4000) and Silica Encapsulated Mn0.5Zn0.5Fe2O4 Nanoparticles Laisina, Edwin; Suharyadi, Edi
Empiricism Journal Vol. 5 No. 2: December 2024
Publisher : Lembaga Penelitian dan Pemberdayaan Masyarakat (LITPAM)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36312/ej.v5i2.2273

Abstract

In this research has been successfully Mn0.5Zn0.5Fe2O4 nanoparticles synthesis using co-precipitation method and their encapsulation by varying the concentration of polyethylene glycol (PEG-4000) and silica. The result of X-Ray Diffraction (XRD) characterization showed that Mn0.5Zn0.5Fe2O4 nanoparticles was mix spinel crystal structure. There was a phase other than Mn0.5Zn0.5Fe2O4 phase synthesized that a-Fe2O3 phase before and after encapsulated with PEG-4000 and silica. Encapsulation of silica has showed a new diffraction peak (222) because silica was crystal. Mn0.5Zn0.5Fe2O4 particle size before and after encapsulated with PEG-4000 (50% concentration) and silica (50% concentration) was 27.28±0.26 nm; 19.13±0.13 nm and 32.75±0.55 nm, respectively. The result of Transmission Electron Microscopy (TEM) characterization showed that before encapsulated with PEG-4000 and silica, occur agglomeration, meanwhile after encapsulated, the agglomeration was reduced. The result of Fourier Transform Infra Red (FTIR) characterization showed that Mn0.5Zn0.5Fe2O4 nanoparticles encapsulated with PEG-4000 there was shift in the wavenumbers 2878.00 cm-1 to 2885.51 cm-1 in the functional groups C-H and wavenumbers 1103.28 cm-1 to 1111.00 cm-1 in the functional groups C-O-C. Both of those functional groups was a constituent bond PEG-4000. Bonding metal oxide (M-O) was shift the wavenumbers 578.64 cm-1 to 570.93 cm-1, which was an uniform pattern of Mn0.5Zn0.5Fe2O4. Mn0.5Zn0.5Fe2O4 encapsulated with silica was shown in the wavenumbers 1049.28 cm-1; 779.24 cm-1; and 471.00 cm-1, which is the functional groups Si-O-Si (stretching). The characterization result of Mn0.5Zn0.5Fe2O4 magnetic properties with Vibrating Sample Magnetometer (VSM) showed that the values of coercivity, magnetization (at H = 15 kOe) and remnant magnetization was 47.55 Oe, 10.41 emu/g, 1.40 emu/g. After Mn0.5Zn0.5Fe2O4 nanoparticles encapsulated with PEG-4000 and silica was decreased amounting to 45.80 Oe, 45.64 Oe, 10.32 emu/g, 1.34 emu/g, 0.28 emu/g and 0.07 emu/g, respectively.
Co-Authors - Heriansyah, - - Mustawarman, - - Mutmainnah, - A.A. Ketut Agung Cahyawan W Abdul Hakim Prima Yuniarto Abu Khalid Rivai Ade Iriani Adriyanto Juliastomo Gundo Agnesia, Wega Dhea Agustin, Ayu Chandra Agusutrisno Agusutrisno, Agusutrisno Alfiazh, Andini Tria Anik Nunuk Wulyani Arditya Prayogi Armitasari, Linda Asep Awaludin, Asep BUDI SETIADI DARYONO Chairani, Nur Julianti Dwi Damanik, Lina Aftiani DEWI SARTIKA Dewi, Priyantini Dhel Prisca Daro Kowe Ekaning Dewanti Laksmi El Khoiri, Niamika Erni Marlina, Erni Evi Maria Evynurul Laily Zen Fakhrillah, Agvy Rena Farkan, Mochammad Ferni Malega Flora Rosdiana Lumbansiantar Gunadi Harry Sulistyo Hafied Cangara, Hafied Harianto, Muhammad Bayu Aji Putra Heri Kiswanto Heri Kiswanto Hidayati, Yustina I Putu Tedy Indrayana Ihsan, Iif Miftahul Ilham Ilham Imam Prayogo Pujiono Indrawati, Dewi Miska Irwan Sembiring Istiqomah, Nurul Imani Ivone, Fransisca Maria Kamsul Abraha Karenia Jannah Dewi Prayogo Kristiany, Maria Gorety Eny Kuat Ismanto Kusumamawarni, Deaseptia Nirmala Laisina, Edwin Mahardika Yoga Darmawan Malega, Ferni Malega, Ferni Mangalla, Bileam Mardiyanto Mardiyanto Margono Margono Mirjam Anugerahwati Mudasir Mudasir Muhammad Hanif Mulyono, Mugi Nasirin, Nasirin Nasrullah Nasrullah Novela, Monica Nugraha, Bayu Adi Nur Aji Wibowo Nurul Imani Istiqomah Nurwadi, Nurul Fadilah Parlina, Iin Posman Manurung Prabandaru, Lila Prabowo, Guntur Prima Widayani Putra, Angkasa Rahardian, Renaldy Baptista Rahayu, Dwi Indah Raihana Binti Romly Ramadiansyah, Febry Rheido, Gestar Riyanto, Didik Rohmah, Syifa Romi Novriadi Rony, Zahara Tussoleha Rosyidah, Umniyah Juman Safitri, Mega Said, Dian Riani Samsu Harapan, Sri Budiani Samsuardi Samsuardi, Samsuardi Samsuharapan, Sri Budiani Sari, Emi Kurnia Satoshi Iwata Sektiana, Sinar Pagi Shirly Rizki Kusumaningrum Sintha Tresnadewi Siti Muniroh Sri Andreani Sri Budiani Stephanie Gabriella Wijaya Suhardi, Muhammad Tegar Alif Suprihatin Susilo, Dinantari Susilo, Sandy Pria Nanda Syahirul Alim Syahrul R, Syahrul Syamsul Arifin Syaputra, Affandi Syukron, Akhmad Aufa Tahir, Asman Bin Mohd Takeshi Kato Theopillus J. H. Wellem Tintien Koerniawati Tjoa, Stanley Evander Emeltan Tresnadewi, Shinta Tyas Adi Novianto Utami, Revita Putri Utari Praba Astuti Wake, Yohana Dhoe Yani, Achmad Yazid Basthomi Yessica Nataliani Yulizar Yulizar Yumna, Asy Syafa’