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All Journal Pharmaciana: Jurnal Kefarmasian JKPK (Jurnal Kimia dan Pendidikan Kimia) ALKIMIA : Jurnal Ilmu Kimia dan Terapan Jurnal Keperawatan dan Fisioterapi (JKF) Jurnal Kesmas dan Gizi (JKG) JURNAL FARMASIMED (JFM) Jurnal Dunia Farmasi Jurnal Keperawatan Priority JURNAL PENELITIAN PERAWAT PROFESIONAL Jurnal Ilmiah Wahana Pendidikan Jurnal Indah Sains dan Klinis FORTE JOURNAL All Fields of Science Journal Liaison Academia and Sosiety Journal Liaison Academia and Society Jurnal Pengmas Kestra (JPK) Analit: Analytical and Environmental Chemistry Medistra Medical Journal (MMJ) Analit: Analytical And Environmental Chemistry
Herlina H
Institut Kesehatan Medistra Lubuk Pakam
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Journal : Analit: Analytical And Environmental Chemistry

 1 
PENGEMBANGAN ANALISA GLIBENKLMID MENGGUNAKAN SORBEN POLIMER BERCETAKAN MOLEKUL Sirumapea, Lasmaryna; Herlina, Herlina; Hilma, Hilma; Mellinda, Mellinda
Analit : Analytical and Environmental Chemistry Vol. 8, No. 02 October (2023) Analit: Analytical and Enviromental Chemistry
Publisher : Jurusan Kimia FMIPA Universitas Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/aec.v8i2.2023.p24-33

Abstract

Research on the development of glibenclamide analysis has been carried out using molecularly printed polymeric sorbents. This study aims to prepare a selective and accurate method of determining glibenclamide, through the molecular imprint method. Glibenclamide imprinted polymers have been successfully synthesized. Methyl methacrylic acid, ethyleneglycodimethacrylate, benzoyl peroxide were dissolved in acetonitrile and chloroform at a controlled temperature of 70°C. Extraction was carried out with methanol: acetic acid (8.5:1.5). Physical functional group analysis was carried out with FTIR spectrophotometer which showed specific peaks of glibenclamide, amine and amide groups at 3405 cm-1. The selectivity test gave the following results: imprinting factor (IF) = 2.45 and the selectivity coefficient (?) for ramipril = 1.21 and against metformin = 2.28. The results showed that the polymer had a good impression and was selective for glibenclamide analysis Keywords: glibenklamid, molecularly imprinted polymer, metformin, ramipril.
Co-Authors AGNES OCTAVIA DAMANIK Ahmad Hafizullah Ritonga Alinur, Alinur Alwi Fahruzy Nasution ANGELIKA SINAGA Ardi Ardi Aritonang, Barita Asvia Rahayu Asvia Rahayu Barus, Ester Julianti Karolina Buchari Buchari Buchari Buchari Buchari Buchari Buchari Buchari Daulay, Dicky Edwar Desi Paramita Dewi Sartika Munthe Dicky Yuswardi Wiratma Efrizah, Doni Felix Kasim Fransiskus Gultom, Fransiskus Hani, Sheila Harahap, Fitri Ramadani Harahap, Mutiara Hatni Hasni Yaturramadhan Harahap Helman Helman, Helman Hetty Elfina Hilma Hilma, Hilma julian, julian Karnirius Harefa Lasmaryna Sirumapea Lasmaryna Sirumapea Lubis, Basyariah Lumban Batu, Fider Maryani Maryani Masitah, Tina Herianty Melda Astrika Sianipar Mellinda, Mellinda Misdawati, Misdawati Muhammad Ali Zulfikar Muhammad Ali Zulfikar Muhammad Razali Muthawali, Dede Ibrahim Napitupulu, Erni Malinda Nasution, M.Dandy Resafahlevi Novi Yanti Nurlela Petra Saragih Nursaputri, Ika Pitriani Pranata, Chandra Razali, Muhammad RINI RINI Rizqa Hafizhah Harahap Rotua Sumihar Sitorus Samah, Eri Shofian Syarifuddin Sibuea, Nurhalimah Sinambela, Megawati Sirait, Reni Aprinawaty Siregar, Imanuddin Sirumapea Sirumapea Suprianto Suprianto Supriono Supriono Suwianto, Suwianto Tarigan, Purnaya Sari Teja Rinanda Widyaningsih, Fadlilah Yana, Sri Nur Yaturramadhan Harahap, Hasni Yosi Darmirani Yusri Yusri