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All Journal Jurnal Ilmu Pertanian Indonesia ACTA VETERINARIA INDONESIANA Jurnal Pengolahan Hasil Perikanan Indonesia Buletin Kimia VALENSI Jurnal Natur Indonesia JURNAL SAINS DAN TEKNOLOGI INDONESIA JURNAL TEKNOLOGI LINGKUNGAN Jurnal Penelitian Hasil Hutan The Journal of Pure and Applied Chemistry Research EduChemia: Jurnal Kimia dan Pendidikan Indonesian Journal of Chemistry Marinade Chemistry Indonesian Journal of Chemical Research EKOLOGIA : Jurnal Ilmiah Ilmu Dasar dan Lingkungan Hidup Molekul: Jurnal Ilmiah Kimia Jurnal Jamu Indonesia Asian Journal of Aquatic Sciences Jurnal Penelitian Hasil Hutan Makara Journal of Science Jurnal Kedokteran Hewan Indonesian Journal of Jamu Jurnal Penelitian Hasil Hutan
Purwantiningsih Sugita
Departemen Kimia, Fakultas MIPA, IPB University
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Decision Sciences, Operations Research & Management Education Energy Engineering Environmental Science Health Professions Immunology & microbiology Materials Science & Nanotechnology Mathematics Medicine & Pharmacology Veterinary Other

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AKTIVITAS ANTIOKSIDAN DAN FLAVONOID EKSTRAK BIJI KURMA Siti Warnasih; Diana Widiastuti; Uswatun Hasanah; Laksmi Ambarsari; Purwantiningsih Sugita
Ekologia: Jurnal Ilmiah Ilmu Dasar dan Lingkungan Hidup Vol 19, No 1 (2019): Ekologia : Jurnal Ilmiah Ilmu Dasar dan Lingkungan Hidup
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33751/ekol.v19i1.1660

Abstract

Date seeds are waste from palm fruit processing that has not been utilized optimally. Date seeds contain flavonoids which are known to act as antioxidants. The aim of this study was to determine the antioxidant activity and flavonoid of methanol extract which was carried out by soxhletation and its fractionation results. Date seeds are made into simplicia, soxhlet extraction with methanol, then the methanol extract is fractionated in stages by liquid-liquid partition with n-hexane, ethyl acetate, and n-butanol. Each fraction and extract was determined by its antioxidant activity with the DPPH method and its flavonoid was determined by spectrophotometry. Ethyl acetate fraction has the strongest antioxidant activity with the lowest IC50 value, that is equal to 5.74 ± 0.05μg/mL, followed by methanol extract of 9.55±0.53 μg/mL, n-butanol fraction 19.73±0,58 μg/mL, and n-hexane fraction of 289.59±10.52 μg/mL, while the IC50 value for vitamin C as a positive control was 4.29±0.74 μg/mL. The highest flavonoids were produced from ethyl acetate fractions which amounted to 1484.33 ± 161.47 mg Quercetin Equivalent (QE) / 100 g, followed respectively by methanol extract of 282.84±13.72 mg QE/100 g.
PVA-Sansevieria trifasciata Fraction Films as Absorbers of Electromagnetic and Thermal Radiation on Smartphones Rahmani, Nabiila; Syahbirin, Gustini; Maddu, Akhiruddin; Sugita, Purwantiningsih; Ilmiawati, Auliya
Makara Journal of Science Vol. 27, No. 1
Publisher : UI Scholars Hub

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Abstract

Technological developments have prompted the production of highly advanced smartphones. However, various advanced features cause smartphones to heat up quickly and emit more electromagnetic radiation, which harms human health. Smartphone protection is needed to solve these issues. This study aims to create a film from the S. trifasciata plant based on polyvinyl alcohol (PVA) to reduce electromagnetic and thermal radiation on smartphones. S. trifasciata plants were macerated with acetone and partitioned with n-hexane, dichloromethane, ethyl acetate, and water. The films were made by mixing PVA with the four fractions. Among the four layers of film, the PVA + water and PVA + ethyl acetate fractions reduced electromagnetic radiation by 25.34% and 2.64%, respectively, and smartphone heat by 3.82 °C and 2.8 °C, respectively, the largest reductions. The results of an LC–MS/MS analysis show that the compounds thought to be contained in both fractions and play a major role in reducing electromagnetic and thermal radiation in smartphones are di-(2-ethylhexyl) phthalate, diisononyl phthalate, and two steroidal compounds, namely, stigmasterol and ergosterol peroxide.
Suspension Stability and Characterization of Chitosan Nanoparticle–Coated Ketoprofen Based on Surfactants Oleic Acid and Poloxamer 188 Rasyid, Nur Qadri; Sugita, Purwantiningsih; Ambarsari, Laksmi; Syahbirin, Gustini
Makara Journal of Science Vol. 18, No. 3
Publisher : UI Scholars Hub

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Abstract

In this research, ketoprofen was used as a drug model in the preparation of chitosan nanoparticles as a potential drug delivery system through the ionic gelation process with tripolyphosphate (TPP). The particle size analysis (PSA) revealed that the average particle size, polydispersity index (PI), and entrapment efficiency of chitosan nanoparticles prepared with oleic acid were 253.7 nm and 0.375 with drug entrapment efficiency of 73.30%. Those prepared with poloxamer 188 were 242.94 nm and 0.302 with drug entrapment efficiency of 87.89%. Scanning electron microscopy (SEM) analysis showed that the shapes of the nanoparticles, both prepared with oleic acid and poloxamer 188, were intact and spherical. Fourier transform infrared spectroscopy (FTIR) indicated several differences between the spectra of chitosan- and ketoprofen-loaded chitosan nanoparticles; for example, a new peak at the wavenumber 1409/cm indicated the presence of electrostatic interaction between the carboxyl group of ketoprofen and the amino group of chitosan. The chitosan nanoparticle suspension prepared with poloxamer 188 showed smaller increases in turbidity and viscosity than that prepared with oleic acid after 34 d of storage.
Adsorption of Waste Metal Cr(VI) with Composite Membranes (Chitosan-Silica Rice Husks) Zulti, Fifia; Dahlan, Kiagus; Sugita, Purwantiningsih
Makara Journal of Science Vol. 16, No. 3
Publisher : UI Scholars Hub

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Abstract

Chromium compounds are widely used in modern industry. Many of these compounds are dumped into the surrounding environment. Membrane technology is more efficient and effective than conventional methods for waste treatment. The research objective was to make a membrane separation process that can be applied to Cr(VI). Membranes were made from chitosan and silica rice husks. Variations of chitosan and silica rice husk used (g) are 2:1 (A1), 2:2 (A2), 3:1 (B1), and 3:2 (B2). The membrane was made by using an inverted phase technique. Results of SEM characterization of membranes showed that B2 has the largest pores at 2.58 μm. The FTIR characterization results indicate the presence of crosslinking between chitosan with silica rice husk with the appearance of Si-O adsorption band at wavelength 1122- 980/cm. A1 membrane, with the smallest pore size has the greatest rejection value towards Cr(VI) which is 70%. The result of this research showed that the composite membrane of silica rice husk was effective enough to adsorb metal Cr(VI) with an average adsorption capacity of 1665.85 mg/g.
Synthesis and Application of Jatropha Oil based Polyurethane as Paint Coating Material Harjono, Harjono; Sugita, Purwantiningsih; Mas’ud, Zainal Alim
Makara Journal of Science Vol. 16, No. 2
Publisher : UI Scholars Hub

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Abstract

Recently, the use of renewable sources in the preparation of various industrial materials has been revitalized in response to environmental concerns. Natural oils are considered to be the most important genre of renewable sources. Jatropha curcas oil (JPO) based polyol is an alternative material that may possibly replace petrochemical-based polyol for polyurethane coating material. Polyurethane was synthesized by reacting JPO-based polyol with isocyanate. To produce JPO-based polyol, JPO was first epoxidized to form epoxidized J. curcas oil (EJP), subsequently it was converted to polyol by the opening ring reaction with acrylic acid (AA) using triethylamine (TEA) as a catalyst. The JPO-based polyurethane film resulting from this study is compared with polyurethane film from commercial polyol for gloss, hardness, and adhesion quality. The result showed that the source of polyol has an influence on gloss, hardness, and adhesion of polyurethane film, but the differences with using isocyanate has less influence. Using visual observation, polyurethane film produced from L.OHV polyol, H.OHV polyol and commercial polyol have similar quality.
ENKAPSULASI KETOPROFEN DENGAN KITOSAN-ALGINAT BERDASARKAN JENIS DAN RAGAM KONSENTRASI TWEEN 80 DAN SPAN 80 Sugita, Purwantiningsih; Napthaleni, Napthaleni; Kurniati, Mersi; Wukirsari, Tuti
Makara Journal of Science Vol. 14, No. 2
Publisher : UI Scholars Hub

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Abstract

Encapsulated Ketoprofen by Chitosan-Alginat based on Type and Variation of Tween 80 and Span 80 Concentration. Ketoprofen has been encapsulated by chitosan-alginate based on types of surfactant and it’s concentration. The variations of concentration either Tween 80 (polietilena sorbitanmonooleat) or Span 80 (sorbitanmonooleat) that used were around (1- 3)% concentrations with stirring around (15-60) minutes. The using of Tween 80 resulted efficiency of encapsulated ketoprofen and nano particle size (100-1000) nm are higher than Span 80.
DISOLUSI MIKROENKAPSULASI KURKUMIN TERSALUT GEL KITOSAN-ALGINAT-GLUTARALDEHIDA Herdini, Herdini; Darusman, Latifah K; Sugita, Purwantiningsih
Makara Journal of Science Vol. 14, No. 1
Publisher : UI Scholars Hub

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Abstract

Dissolution of Curcumin Microencapsulation Coated by Chitosan-Alginate-Glutaraldehide. In vitro dissolution of curcumin coated by chitosan-alginate gel in its optimum condition was studied. The maceration process using 17.08% ethanol yields and the content of the curcumin in the extract detected by visible spectrophotometry λ 430 nm is found to be 10.30 %. Its optimum condition was obtained using response surface method at concentrations ratio of alginate 0.62% (b/v) and glutaraldehide 4.63% (v/v) , respectively, where the chitosan concentration was fixed (1.75% [b/v]). The dissolution assay was done at 37 o C, at 100 rpm of stirring rate in 8 hours. Aliquots were taken at 15, 30, 45, 60, 90, 120, 150, 180, 240, 300, 360, 420, 480 minutes. Absorbance of the Aliquots was measured at λ 430 nm. The curcumin released has the best linear correlation to the first order reaction with released constant, k = 2.24 10-3 minute-1 while it’s half live is t1/2 = 5.16 hours. Release curcumin was determined mainly by diffusion mechanism. Compared to the result based on Fick model, the one of Higuchi model is better in agreement in reproducing the released data.
Antioxidant Activity, Cytotoxicity, and Identification of Secondary Metabolites of Kigelia africana from Waterpark Platinum Riau Fitri, Iis Yusma; Kurniawanti, Kurniawanti; Syahbirin, Gustini; Sugita, Purwantiningsih
Indonesian Journal of Chemical Research Vol 11 No 2 (2023): Edition for September 2023
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598//ijcr.2023.11-iis

Abstract

Antioxidants can prevent reactive oxygen-associated diseases, which trigger carcinogenesis, cardiovascular disease, and premature aging. India and Africa have mostly practiced sausage trees (Kigelia africana) as traditional medicine, whereas Indonesia is still limited. The research aims to determine the phytochemistry and bioactivity of the n-hexane fractions from crude methanol extract of the leaves and bark of the sausage tree as antioxidants and their toxicity. The sausage tree is derived from Waterpark Platinum Riau. The sausage trees were macerated with methanol and fractionated by n-hexane and ethyl acetate. All samples were tested for their antioxidant to 1,1-diphenyl-2-picrylhydrazyl (DPPH) and cytotoxicity to Artemia salina Leach larvae. Phytochemical results of methanol crude extract, n-hexane, and ethyl acetate fractions of leaves and sausage bark showed the presence of all secondary metabolites except alkaloids in the n-hexane fraction. Antioxidant and cytotoxic activity of stem and leaf bark ethyl acetate fraction was stronger than crude methanol extract and n-hexane fraction. Based on LC-MS/MS data, the secondary metabolite components that have contributed strongly antioxidant activity of this study are flavonoid compounds such as kaempferol and the derivatives, lignans (cubebin), and steroids (pregnant).
Synthesis of Green Diesel from Palm Oil Using Nickel-based Catalyst: A Review Aziz, Isalmi; Sugita, Purwantiningsih; Darmawan, Noviyan; Dwiatmoko, Adid Adep
Jurnal Kimia Valensi Jurnal Kimia VALENSI Volume 9, No. 1, May 2023
Publisher : Syarif Hidayatullah State Islamic University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15408/jkv.v9i1.26488

Abstract

Petroleum is the primary energy that is generally used throughout the world. Its non-renewable nature and exhaust gas emissions that can damage the environment are a concern for developing environmentally friendly renewable energy. Green diesel is an alternative energy to replace diesel fuel (diesel) from petroleum which has the potential to be developed. The raw material in palm oil has great potential for development due to its relatively high production. Green diesel synthesis can be carried out using the catalytic deoxygenation method. The type of raw material, catalyst, and process conditions influences this method. The catalyst is the most influential factor in catalytic deoxygenation. Transition metal catalysts like nickel are inexpensive and have good catalytic activity like precious metals. Catalytic activity can be increased by modifying the catalyst components and optimizing the process. Modification of the catalyst can increase the surface area, Lewis and Bronsted sites, and crystal size so that the resulting green diesel can be maximized, such as Ni-Co, Ni-Zn, and Ni-Mo bimetallic catalysts.
ACUTE TOXICITY WATER EXTRACT OF Meretrix meretrix Linnaeus IN VIVO ON SPRAGUE DAWLEY RATS Apriandi, Azwin; Tarman, Kustiariyah; Sugita, Purwantiningsih
Asian Journal of Aquatic Sciences Vol. 4 No. 3 (2021): December
Publisher : Lembaga Penelitian dan Pengabdian Kepada Masyarakat Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31258/

Abstract

Meretrix meretrix empirically has been widely believed by the public to a wide variety of health benefits. It is necessary to do an analysis of the level of toxicity of Meretrix meretrix extract. The experiment was carried out extraction sample with water (1;4) (w/v), analysis of acute toxicity Meretrix meretrix extract with the OECD method 403:2009. Based on the results of water extract of Meretrix meretrix no effect on physical observations of test animals with LD50> 15 g/kg BW. Histopathological observation on the liver and kidneys, there is necrosis of the liver cells and some cell degeneration in the kidneys, but on the whole network under normal conditions appropriate control group.
Co-Authors Achmad Sjachriza Achmad Sjahriza Ade Heri Mulyati Adi Cifriadi, Adi Adi Santoso Adi Santoso ADI SANTOSO Agusta, Dhea Demitri Akhiruddin Maddu Apriandi, Azwin Asep Hidayat Asep Hidayat Asep Saefurohman Asron Ferdian Falaah, Asron Ferdian Auliya Ilmiawati Azkiyah, Dina Bambang Srijanto Bambang Srijanto Bambang Srijanto Budi Arifin Cece Sumantri Dedi Duryadi Solihin Dian Susanthy Diana Widiastuti Dita Ariyanti dwi wahyono Dwiatmoko, Adid Adep Dyah Iswantini Ellin Vina Setyowati Epi Taufik Ermin Katrin Winarno Ermin Katrin Winarno Fifia Zulti Firdayani, Firdayani fithri amelia Fitri, Iis Yusma Ghozali, Ali Aulia Gustini Syahbirin Hanhan Dianhar Harjono - Harjono Harjono Hefni Effendi Henny Purwaningsih Herdini , Herdini Herdini . Ida Ayu Putu Sri Widnyani Irmanida Batubara Isalmi Aziz Jaya Hardi Kiagus Dahlan Kiagus Dahlan Kurniawan, Yehezkiel Steven Kurniawanti, Kurniawanti Kustiariyah Tarman LAKSMI AMBARSARI latifah K Darusman Latifah K. Darusman Lia Anriani Luthfan Irfana mahdi mubarok Mas’ud, Zainal Alim Mela Faradika Mersi Kurniati Muhamad Rifai Muhamad Rifai Muhammad Fathurrahman Napthaleni , Napthaleni, Napthaleni Ningtias, Widya Sekar Ayu Novik Nurhidayat Noviyan Darmawan Nur Qadri Rasyid Okti Rachmawati Okti Rachmawati Okti Rachmawati Priandanda, Rafi Chandra Pujiyati Pujiyati Pujiyati, Puspita Sari Puspita Sari Rahayu, Dyah Utami Cahyaning Rahmani, Nabiila Rarah Ratih Adjie Maheswari Rasyid, Nur Qadri Rini Siswati Asnel Santi Puspitasari Siti Nikmatin Siti Warnasih Suminar S Achmadi SUMINAR SETIATI ACHMADI Taher, Dharmawaty M. Tetty Kemala Tiltje Andretha Ransaleleh Tuti Wukirsari Umi Cahyaningsih Uswatun Hasanah Wasmen Manalu Yuyu Yundhana Zainal Alim Mas’ud Zulti, Fifia Zuniar Subastian Zuraida Hanum Zuraida Hanum Zuraida Hanum