Claim Missing Document
Check
Articles

Optimization of Titanium Recovery from Tin Tailings Using Flotation Route Subandrio, Subandrio; Dahani, Wiwik; Sundari, Rita; Kurniawati, Riskaviana; Marwanza, Irfan; Darren, Franko Sajow
International Journal of Innovation in Mechanical Engineering and Advanced Materials Vol 6, No 3 (2024)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/ijimeam.v6i3.28891

Abstract

Titanium has found widespread application across various industries due to its high corrosion resistance. It is commonly used in dental equipment, surgical instruments, bone implants, and marine components, and serves as an engine material in high-temperature environments. Because of its lighter weight compared to steel, titanium has also replaced stainless steel in many construction materials. In Bangka Island, Indonesia, tin tailings have been identified as a potential source of titanium, making the analysis of titanium in these tailings highly significant. This study employed the froth flotation method, known for its simplicity, speed, and cost-effectiveness, to analyze titanium content from tin tailings. Sodium oleate was used as the frother and collector, while sodium chlorate acted as the depressant. The mass ratios of depressant to collector were varied at fixed collector amounts (1:10, 5:10, 10:10, and 15:10) and fixed depressant amounts (10:3, 10:6, 10:9, and 10:12). The highest titanium concentration (2.03%) was achieved with a mass ratio of 10:12, while the optimal titanium recovery (45.51%) in the concentrate occurred with equal amounts (3.75 g) of depressant and collector, or at a mass ratio of 10:10, at 15 minutes of flotation time and neutral pH. X-ray fluorescence (XRF) and X-ray diffraction (XRD) analyses indicated that the tin tailings primarily contained silicate and zircon minerals, with traces of titanium in the form of rutile, ilmenite, and titanate. These findings contribute valuable insights for future titanium extraction and processing industries.
PYROMETALLURGICAL PROCESS FOR ZINC ANALYSIS IN SPHALERITE APPLYING XRD AND XRF Dahani, Wiwik; Kurniawati, Riskaviana; Sundari, Rita; Marwanza, Irfan; Rachman, Faisal
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1525

Abstract

This paper has analyzed dominant zinc element in sphalerite naturally found together with galena in mineral ore. Since pyrometallurgical route related to roasting process is very common to mineral dressing, therefore, this investigation has studied the effect of varied roasting time (30 min, 60 min, and 90 min) and temperature (500oC, 600oC, and 700oC) on zinc mineral examination using XRD (X-Ray Diffraction) and zinc element using XRF (X-Ray Fluorescence) analyses. Previous studies usually applied cheaper AAS (Atomic Absorption Spectrometer) for zinc analysis in aqueous solution, however, sphalerite is a solid matrix and therefore, this study has applied XRF to analyze zinc. Pyrometallurgical process of zinc mineral in sphalerite is related to mineral transformation in the form of ZnSO4, ZnS, and ZnO that cannot be detected by XRF. Therefore, this study has used XRD that can observe mineral transformation.   The XRD pattern shows four intense peaks at 2θ (28o, 47o, 56o, and 76o) justified sphalerite (ZnS) sample with little amount of pyrite (FeS2) and galena (PbS) as impurities. The XRF analysis shows from 30 min to 90 min, the Zn content has increased remarkably at 700oC and Zn content looked stagnant at 500oC, while Zn content increased dramatically from 60 min to 90 min at 600oC. During roasting process at high temperature, ZnS mineral converted to ZnO and expelled SO2 gas due to oxidation reaction causing weight reduction. The study is valuable for mineral processing in searching for optimization.
Co-Authors Adhitia, Iit Aditya Saputra Afiat Anugrahadi Afiat Anugrahadi Afiat Anugrahadi Afiat Anugrahadi, Afiat Ahmad Helman Hamdani Alvando Alone, Marcel Samuel Anak Agung Istri Sri Wiadnyani Andriyani Andriyani Andry Prima Ardiansyah Ardiansyah Arinda Ristawati Arkaan, Muhammad Dzaki Aryanto, Reza Azizi, Masagus Ahmad Bani Nugroho Bani Nugroho Bani Nugroho Chairul Nas Chairul Nas Chairul Nas Chairul Nas Christin Palit Damarizky, Rico Danu Putra Danu Putra Darren, Franko Sajow Dewi Kumala Salim Djoko Hartanto Emmy Fatmi B. I. Emmy Fatmi Budhya Fadliah Fadliah Faisal Rachman Fitra Yuda, Himmes Gumay, Rhazes Eesha Hadi, Singgih Irianto Trisilo Havidh Pramadika Himmes Fitra Yuda Idris Juradi, Muhammad IIT ADHITIA iputu rama aryawan Ivetta Ivetta Iyan Haryanto Jeremy Gerald Puglisi Kamardi, Muhammad Agus Karim, Razak Karmadi, Muhammad Agus Khuzaimah Arifin Korra Herdyanti, Mixsindo Kurniawati, Riskaviana M Kemal Ghifari M. A. Azizi M. Puspita Maulida, Fajri Mixsindo Korra Herdyanti Mohamad Nur Hariawan Muhammad Agus Kamardi Muhammad K. Ghifari Muhammad Kemal Ghifari Muhammad Napis Fikri Muhammad Rahthin Qinthara Muhammad Taufiq Fathaddin, Muhammad Taufiq Nadya A. Hartanti Nadya A. Hartanti Nas, Chairul Nas, Chairul Nugraheni, Rosmalia Palit, Christin Pandiangan, Violeta Apriani Panjaitan Novi Hartami Patian, Syamidi Permatasari, Claudia Intan Prapansya, Onnie Ridaliani Prasta Kumarana Garnika Purwiyono, Taat Tri Putra, Danu Ratna Ediati Reza Aryanto Ririn Yulianti Rita Sundari Rita Sundari Rosmalia Nugraheni Rully Naufal Falih Safitri, Diah Utami Sahetapy, Silvia Immanuela Sekar Tika Sari Simon Fides Singgih Irianto Trisilo Hadi Solihin Solihin Subandrio Subandrio Subandrio, Subandrio Suherman Dwi Nuriana Suherman Dwi Nuryana Suliestyah Sumotarto, Untung Sundari, Rita Susanti, Chiesa Artamevia Diva Syamidi Patian Syamidi Patian Taat Tri Purwiyono Theresa Naomi Putri Tuheteru, Edy Jamal Untung Sumotarto W. Dahani Wahyu Gendam Prakoso Wahyu Gendam Prakoso, Wahyu Gendam Wiwik Dahani Wiwik Dahani Wiwik Dahani Wiwik Dahani Wiwik Dahani wiwik dahani, wiwik Y. Maulana Yansen Barus Yuga Maulana Yulianti, Ririn Ziad S Zulfahmi Zulfahmi