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Sutiyono
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Journal : Biomedical and Mechanical Engineering Journal

 1 
Analysis of effect Magnesium Ammonium Phospate (MAP) Concentration on Struvite Morphology in A Vertical Reactor Luluk Edahwati; Sutiyono; Atika Andini; Wahyu Dwi Lestari; Tria Puspa Sari; Ndaru Adyono; Novel Karaman
Biomedical and Mechanical Engineering Journal (BIOMEJ) Vol. 1 No. 1 (2021): BIOMEJ
Publisher : Mechanical Engineering Department at Universitas Pembangunan Nasional "Veteran" Jawa Timur

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Abstract

Struvite was a white crystal known as Magnesium Ammonium Phosphate Hexahydrate (MgNH4PO4.6H2O). In industry, struvite was found in the pipes crust which the hot fluid through passes. Struvite is often used as fertilizer because it contains phosphate content. The one of benefits of struvite crystals is slow release fertilizer, so it can be more durable, which is good for the growth of the plants. The Precipitation technology is currently one of the most widely applied technologies in struvite formation. The process of forming struvite is carried out by using a vertical reactor. The process started by mixing the equimolar solutions of MgCl2, NH4OH, and H3PO4 with a concentration ratio of 1: 1: 1 and 1: 1: 2. The process was carried out with the condition at the 30°C while the air inlet rate was 1.25 liters/min. The pH of the solution is pH 9 and controlled using NaOH solution. The process was carried out in the steady state condition. Then the solution was filtered and solid was dried at room temperature for 48 hours. From this study, the concentration ratio of 1:1:2 was obtained the best composition of struvite compared to the others ratio. The solid was analyzed by using the SEM-EDX instrument. The morphology of struvite was formed an irregular pyramid-like crystal or commonly referred to as an authorhombic shape.
Analysis of effect Magnesium Ammonium Phospate (MAP) Concentration on Struvite Morphology in A Vertical Reactor Luluk Edahwati; Sutiyono; Atika Andini; Wahyu Dwi Lestari; Tria Puspa Sari; Ndaru Adyono; Novel Karaman
BIOMEJ Vol. 1 No. 1 (2021): BIOMEJ
Publisher : UPN 'Veteran" Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Struvite was a white crystal known as Magnesium Ammonium Phosphate Hexahydrate (MgNH4PO4.6H2O). In industry, struvite was found in the pipes crust which the hot fluid through passes. Struvite is often used as fertilizer because it contains phosphate content. The one of benefits of struvite crystals is slow release fertilizer, so it can be more durable, which is good for the growth of the plants. The Precipitation technology is currently one of the most widely applied technologies in struvite formation. The process of forming struvite is carried out by using a vertical reactor. The process started by mixing the equimolar solutions of MgCl2, NH4OH, and H3PO4 with a concentration ratio of 1: 1: 1 and 1: 1: 2. Theprocess was carried out with the condition at the 30°C while the air inlet rate was 1.25 liters/min. The pH of the solution is pH 9 and controlled using NaOH solution. The process was carried out in the steady state condition. Then the solution was filtered and solid was dried at room temperature for 48 hours. From this study, the concentration ratio of 1:1:2 was obtained the best of struvite compared to the others ratio. The solid was analyzed by using the SEM-EDX instrument. The morphology of struvite was formed an irregular pyramid like crystal or commonly referred to as an authorhombic shape.
Mini Factory Laboratory from Technology Reverse Engineering Ballet Reactors in Struvite Formation Luluk Edahwati; Sutiyono; Wahyu Dwi Lestari Edahwati; Radissa Dzaky Issafira; Wiliandi Saputro; Ahmad Khairul Faizin; Ndaru Adyono; Tria Puspa Sari
BIOMEJ Vol. 1 No. 2 (2021): BIOMEJ
Publisher : UPN 'Veteran" Jawa Timur

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Abstract

Reverse Engineering (RE) can be interpreted as procedures and processes in dismantling an object to find out the materials, working methods, or technology used so that the object can function properly. Design activities using the reverse engineering concept make it easier for students to understand product specifications, product advantages and disadvantages, product production processes and production cost estimates before designing new products. The laboratory is one place that can be used to carry out the reverse engineering process. The bulkhead reactor is an alternative to the stirred tank reactor with the aim that the resulting product is maximized both in terms of quantity and morphology or shape of the material. The benefit of disassembling this product is as a first step in understanding the concept of reverse engineering in the task of designing machines or tools. From the results of the study, it was found that the formation of struvite occurred at pH 9 using an air flow rate of 1 l/minute.
Analysis of effect Magnesium Ammonium Phospate (MAP) Concentration on Struvite Morphology in A Vertical Reactor Edahwati, Luluk; Sutiyono; Andini, Atika; Dwi Lestari, Wahyu; Puspa Sari, Tria; Adyono, Ndaru; Karaman, Novel
BIOMEJ Vol. 1 No. 1 (2021): BIOMEJ
Publisher : UPN 'Veteran" Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/biomej.v1i1.22

Abstract

Struvite was a white crystal known as Magnesium Ammonium Phosphate Hexahydrate (MgNH4PO4.6H2O). In industry, struvite was found in the pipes crust which the hot fluid through passes. Struvite is often used as fertilizer because it contains phosphate content. The one of benefits of struvite crystals is slow release fertilizer, so it can be more durable, which is good for the growth of the plants. The Precipitation technology is currently one of the most widely applied technologies in struvite formation. The process of forming struvite is carried out by using a vertical reactor. The process started by mixing the equimolar solutions of MgCl2, NH4OH, and H3PO4 with a concentration ratio of 1: 1: 1 and 1: 1: 2. Theprocess was carried out with the condition at the 30°C while the air inlet rate was 1.25 liters/min. The pH of the solution is pH 9 and controlled using NaOH solution. The process was carried out in the steady state condition. Then the solution was filtered and solid was dried at room temperature for 48 hours. From this study, the concentration ratio of 1:1:2 was obtained the best of struvite compared to the others ratio. The solid was analyzed by using the SEM-EDX instrument. The morphology of struvite was formed an irregular pyramid like crystal or commonly referred to as an authorhombic shape.
Analysis of pH Regulation on the Ca/P Ratio of Green Mussel Shell Hydroxyapatite using the Sol-Gel Method Edahwati, Luluk; Sutiyono; Suprihatin; Titi Susilowati; Sri Muljani
BIOMEJ Vol. 3 No. 2 (2023): BIOMEJ
Publisher : UPN 'Veteran" Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/biomej.v3i2.83

Abstract

Kandungan kalsium karbonat dari cangkang kerang hijau dapat dimanfaatkan sebagai salah satu material. Hidroksiapatit merupakan mineral utama yang menyusun tulang dan gigi sehingga memiliki kemiripan dengan bagian mineral pada tulang. Penelitian dilakukan untuk Konsentrasi reagen asam fosfat yang digunakan dan pH reaksi pada perolehan rasio Ca/P dari Hidroksiapatit yang didapatkan melalui proses sintesis dengan menggunakan metode sol-gel. Proses presipitasi calsium carbonat dilakukan dengan menambahkan air sebanyak 50 ml kedalam larutan H3PO4 dengan konsentrasi 1M kemudian diaduk selama 3 jam menggunakan magnetic stirrer dengan kecepatan pengadukan sebesar 300 rpm, pH dijaga 8 – 12 ( variabel ) menggunakan bantuan NaOH. Selanjutnya larutan dilakukan penuaan (waktu aging) pada suhu kamar selama 20 jam sampai terbentuk gel. Gel yang telah terbentuk disaring menggunakan kertas saring watman. Selanjutnya gel dipanaskan dalam oven dengan suhu 105 selama 2 jam. Serbuk yang dihasilkan kemudian difurnace pada temperatur 600oC selama kurang lebih 6 jam supaya membentuk serbuk kering Hidroksiapatit. Rasio Ca/P terbaik sebesar 1,6708 dengan penggunaan H3PO4 sebesar 1M serta pH sebesar 11.
Struvite Mineral Synthesis from Laundry Waste Water Sutiyono; Edahwati, Luluk; Indah Nur Fauziyah; Lusy Larasati A
BIOMEJ Vol. 3 No. 2 (2023): BIOMEJ
Publisher : UPN 'Veteran" Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/biomej.v3i2.87

Abstract

Struvite is a white crystal chemically known as magnesium ammonium phosphorus hexahydrate (MgNH4PO4.6H2O). This mineral has a hardness of 1.5 to 2 Mohs. Struvite is easily soluble under acidic conditions and slightly soluble under neutral and alkaline conditions. In industry, struvite is found in the crust of pipes through which hot fluids pass. Struvite is often used as fertilizer because of its phosphate content. The formation of struvite minerals (hereinafter MAP) from laundry waste water is carried out using an aeration tank. MAP solution is made by reacting laundry waste water with Phosphoric Acid (H3PO4) and Ammonium Hydroxide (NH4OH). The MAP ratio was set at 1:1:1 with a temperature of 20 - 40 oC and an air flow rate of 0.5 - 1.5 liters per minute. The best results were at a temperature of 25oC with an air flow rate of 1 (Liter / minute) with a magnesium content of 10% and phosphorus of 42%.
A Performance of Baffled Stirred Tank Reactor in Map Mineral Recovery Luluk Edahwati; Sutiyono; Suprihatin
BIOMEJ Vol. 4 No. 1 (2024): BIOMEJ
Publisher : UPN 'Veteran" Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/biomej.v4i1.101

Abstract

In the agricultural and wastewater treatment industries, the formation of Magnesium Ammonium Phosphate (MAP), also known as struvite, is an important process to utilize organic waste and produce value-added phosphate fertilizers. In this context, the use of a stirred tank reactor equipped with baffles is a major concern. This study aims to evaluate the performance of a stirred tank reactor with baffles in the recovery of MAP. Analysis of the experimental results shows that the use of baffles has a significant impact on process efficiency and the quality of the MAP product produced. This study provides a deeper understanding of the role of baffles in maintaining the flow pattern and mixing of raw materials in the reactor tank, thus making an important contribution to the development of more efficient and environmentally friendly phosphate fertilizer manufacturing technology. best phosphate obtained 27%, ph 10, temperature 30oC and molar ratio 1:1:2 Keywords: molar ratio, pH, precipitation, RTB, temperature, struvite
Co-Authors Agus Zaenul Fitri Ahmad Khairul Faizin Alfira Triska Maharani Andini, Atika Anggriawan, Rizqi Rendri Ani Wahyuni Anik Wahyunita Anita Nanda Fatanaila Aripin As’aril Muhajir Atika Andini Aulia Sholichah Iman Nurchotimah Ayu, Sukma Defyan Ahmad Muflizar Denny Rusdianto Deny Rahmat DHIYAN NANY WIGATI Diana Salendra DWI LESTARI, WAHYU Eko Pramono Erni Pustikha Sari Febriana Tri Kusumawati Fiana Khayu Maftuhah Fikri Salman Ramadan Hanny Novita Sari Indah Nur Fauziyah INFORMATIKA, COMPUTING Irpan, Ade Irsa Riswanda j-sika j-sika Jayanti JULIANTI, MEGA Khaerunnisa, Novita Khilda Nistrina Kumalasari , Nurya L.Urip Widodo, Yohandrik Novel Karaman Latifatu Siyadah Ludi Zaelani Luluk Edahwati Luluk edahwati Lusy Larasati A M. Zulfa Chusni Mubarok Meila Cindy Putri Lestari Meity Mulya Susanti Mika Agustiana Mingle A Pistanty Mubin , Kholifatul Muhammad Athallah Rifqi Shafwan Muhammad Makmun Muhammad Makmun, Muhammad Muhammad Mufti Wibawa Nalfriza Alfianti Nandini, Atika Ndaru Adyono Ndaru Adyono, Ndaru Nieken Luh putu Nur Intan Permatasari Nurlia Fitrianingrum Nurul Kodiyah Nurya Kumalasari Pandu Cahyono, Sigit Puspa Sari, Tria Putri Melli Anjani Putri Syifa Ratu Ayu Jelita Radissa Dzaky Issafira Rahmania Isabel Rahmawati Rangga kurniawan Ria Naf'ana Ricard Janottama Riniasih , Wahyu Riniasih, Wahyu Riska Indrayati Risma Aisya Risti Linta Chumaira Rizki Sahara Rosandra Firdi Silvian Rosmalina Saddhadika, Adhi Khumara Santi Sarah Wahyu Agustini Satriya Hendi Rega Dani Shinta Amalia Silvi Nur Hakiki siti aena Siti Avitasari Sri Muljani Sri Temu Sri Untari Sukiman Supirdan Suprihatin SURYANI SUTOMO Temu, Sri Titi Susilowati Tria Puspa Sari Wahyu Dewi Hapsari Wahyu Dwi Lestari Wahyu Dwi Lestari Edahwati Wiliandi Saputro Yulianasari Yuliyant Yusuf Muharam Zulfian , Firhan Adam