The low level of organic matter in alluvial soil requires amendments to improve soil structure by adding liquid palm oil waste as organic fertilizer which can improve soil structure and enrich organic carbon in the soil and increase soil pH. This research aims to find the interaction effect of BOD (Biological Oxygen Demand) concentration of liquid palm oil waste from anaerobic ponds and NPK fertilizer on soil N, P, K nutrient content, growth and yield of sweet corn plants on alluvial soil. The research was conducted at the experimental garden of the Faculty of Agriculture, Tanjungpura University. Analysis of BOD, N, P and K levels of liquid waste was carried out at the Land Quality and Health Laboratory, Faculty of Agriculture, Tanjungpura University. Analysis of the N, P, K elements of liquid waste was carried out at the Chemistry and Soil Fertility Laboratory, Faculty of Agriculture, Tanjungpura University. The research took place from August to December 2023. This research method was a field experiment with a two-factorial Completely Randomized Design. The first factor consists of three levels, namely: N0 (0 g Urea, 0 g SP-36, and 0 g KCl), N1 (4.5 g Urea, 3.75 g SP-36, 2.8 g KCl), N2 (9 g Urea, 7.50 g SP-36, 5.6 g KCl) and the second factor consists of four levels, namely: L0 (Palm Oil Liquid Waste/LCKS 100%), L1 (LCKS 75%), L2 (LCKS 50%), L3 (LCKS 25%), each treatment was repeated three times to obtain 36 plant samples. Variables observed: soil reaction (pH H2O), C-organic, N-total, P-available, K-available, plant height, stem diameter, number of leaves, and weight of cobs with husks and weight of cobs without husks. The results showed that the anaerobic pond LCKS treatment had a real influence on soil pH, available K, and plant height, while the NPK fertilizer treatment had a real influence on soil pH, total N, available K, plant height, stem diameter, number of leaves, and results of cob weight with husk and husk weight without husk. Keywords: alluvial, sweet corn, palm oil liquid waste, NPK fertilizerINTISARIRendahnya bahan organik pada tanah aluvial membutuhkan bahan pembenah untuk memperbaiki struktur tanah dengan penambahan limbah cair kelapa sawit sebagai pupuk organik yang dapat memperbaiki struktur tanah dan memperkaya karbon organik dalam tanah dan meningkatkan pH tanah. Penelitian ini bertujuan untuk mencari interaksi pengaruh konsentrasi BOD (Biological Oxygen Demand) limbah cair kelapa sawit kolam anaerobik dan pupuk NPK terhadap kandungan hara N, P, K tanah, pertumbuhan serta hasil tanaman jagung manis pada tanah aluvial. Penelitian dilakukan di kebun percobaan Fakultas Pertanian Universitas Tanjungpura. Analisis kadar BOD, N, P, dan K limbah cair dilakukan di Laboratorium Kualitas dan Kesehatan Lahan Fakultas Pertanian Universitas Tanjungpura. Analisis unsur N, P, K limbah cair dilakukan di Laboratorium Kimia dan Kesuburan Tanah Fakultas Pertanian Universitas Tanjungpura. Penelitian berlangsung pada Agustus hingga Desember 2023. Metode penelitian ini adalah eksperimen lapangan dengan Rancangan Acak Lengkap dua faktorial. Faktor pertama terdiri dari tiga taraf, yaitu: N0 (0 g Urea, 0 g SP-36, dan 0 g KCl), N1 (4,5 g Urea, 3,75 g SP-36, 2,8 g KCl), N2 (9 g Urea, 7,50 g SP-36, 5,6 g KCl) dan faktor kedua terdiri dari empat taraf, yaitu: L0 (Limbah Cair Kelapa Sawit/LCKS 100%), L1 (LCKS 75%), L2 (LCKS 50%), L3 (LCKS 25%), masing-masing perlakuan diulang tiga kali sehingga didapatkan 36 sampel tanaman. Variabel yang diamati: reaksi tanah (pH H2O), C-organik, N-total, P-tersedia, K-tersedia, tinggi tanaman, diameter batang, jumlah daun, dan berat tongkol dengan klobot serta berat tongkol tanpa klobot. Hasil penelitian menunjukkan bahwa perlakuan LCKS kolam anaerobik memberikan pengaruh nyata terhadap pH tanah, K-tersedia, dan tinggi tanaman, sedangkan pada perlakuan pemberian pupuk NPK memberikan pengaruh nyata terhadap pH tanah, N-total, K-tersedia, tinggi tanaman, diameter batang, jumlah daun, dan hasil berat tongkol dengan klobot serta berat klobot tanpa klobot. Kata kunci: aluvial, jagung manis, limbah cair kelapa sawit, pupuk NPK