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All Journal VALENSI Jurnal Teknik ITS IPTEK Journal of Proceedings Series IPTEK The Journal for Technology and Science Ulul Albab: Jurnal Studi Islam Jurnal Bahan Alam Terbarukan Bulletin of Chemical Reaction Engineering & Catalysis Journal of Engineering and Technological Sciences I-Finance Journal Dinar: Jurnal Ekonomi dan Keuangan Islam Science and Technology Indonesia Journal Of Chemical Process Engineering (JCPE) BERDIKARI : Jurnal Inovasi dan Penerapan Ipteks Indonesian Journal of Chemistry At-Tafkir ILTIZAM Journal of Sharia Economic Research Journal of Economic, Management, Accounting and Technology (JEMATech) Management Studies and Entrepreneurship Journal (MSEJ) ASEAN Journal of Chemical Engineering Al-Kharaj: Jurnal Ekonomi, Keuangan & Bisnis Syariah JOURNAL OF BUSINESS AND ECONOMICS RESEARCH (JBE) Indonesian Journal of Islamic Economics and Business Jurnal Ahsana Media : Jurnal Pemikiran, Pendidikan dan Penelitian ke-Islaman Jurnal Iqtisaduna Share: Jurnal Ekonomi dan Keuangan Islam Islamiconomic: Jurnal Ekonomi Islam Prosiding Seminar Nasional Teknologi Industri Berkelanjutan Reflection Journal Jurnal Yustitia Sewagati Bukhori: Kajian Ekonomi dan Keuangan Islam Jurnal Informatika Ekonomi Bisnis PARADUTA : Jurnal Ekonomi dan Ilmu-Ilmu Sosial SAINTEK Qanuni : Jurnal of Indonesian Islamic Family Law Bulletin of Chemical Reaction Engineering & Catalysis Journal of Fundamentals and Applications of Chemical Engineering Journal Of Chemical Process Engineering PANDALUNGAN : Jurnal Pengabdian kepada Masyarakat
Lailatul Qadariyah
Departemen Teknik Kimia Institut Teknologi Sepuluh Nopember
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Journal : ASEAN Journal of Chemical Engineering

 1 
Biodiesel Production From Calophyllum Inophyllum Using Base Lewis Catalyst Lailatul Qadariyah; Donny Satria Bhuana; Raka Selaksa; Ja'far As Shodiq; Mahfud Mahfud
ASEAN Journal of Chemical Engineering Vol 18, No 1 (2018)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1030.048 KB) | DOI: 10.22146/ajche.49547

Abstract

The search for renewable alternative energy must be developed, one of which is biodiesel. Seed Calophyllum inophyllum has a fairly high oil content of about 71.4% by weight, has great potential when used as raw material for making biodiesel. The purpose of this research was to synthesize biodiesel from Calophyllum inophyllum oil through the transesterification process using base lewis catalyst with microwave assisted, comparing the performance of sodium acetate to potassium hydroxide, knowing the amount of catalyst required to obtain the best biodiesel, and knowing the optimum power in the manufacture of biodiesel, The first step of making Calophyllum inophyllum biodiesel is degumming process, then continued with esterification. The next process is transesterification, followed by purification of biodiesel. The catalysts used are CH3COONa, and KOH. From the results, Calophyllum inophyllum oil can be used as biodiesel feedstock, the best operating conditions for base catalyst at 300 W power, 1% (w/w) concentration, produced the best yield is 96% (for KOH catalyst) and 87% (for CH3COONa catalyst).
The Effect of Reaction Time and Temperature on the Synthesis of Methyl Ester Sulfonate Surfactant from Palm Oil as a Feedstock using Microwave-Assisted Heating Lailatul Qadariyah; Sahiba Sahila; Mahfud Mahfud
ASEAN Journal of Chemical Engineering Vol 21, No 1 (2021)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ajche.63786

Abstract

Methyl ester sulfonate is an anionic surfactant that can be synthesized from palm oil as a raw material with the addition of sodium bisulfite and calcium oxide catalyst through transesterification and sulfonation process using microwave-assisted heating. The effect of microwave-assisted heating in the transesterification-sulfonation process was investigated in this study. The transesterification process was carried out using a microwave power of 300 watts for 10 minutes with an addition of a KOH catalyst of 1%. The transesterification process gave a result of palm oil methyl ester with a yield of up to 98% and density of 0.8546 gr/ml, and kinematic viscosity of 3.19 cSt. The sulfonation process is carried out using palm oil methyl ester and sodium bisulfite with a mole ratio of 1:3 and calcium oxide catalyst of 1.5% with the microwave power of 300 watts while varying the sulfonation time and temperature. The physicochemical properties of methyl ester sulfonate were analyzed, and the sulfonate group was characterized using FTIR. The optimum condition gave a yield of up to 98.68%, the density of 0.8657 gr/ml, viscosity of 3.75 cSt, pH of 2.12, and surface tension of up to 27.34 dyne/cm at a temperature of 100oC and sulfonation time of 40 minutes.
Parametric Study and Characterization of Sappan Wood (Caesalpinia Sappan Linn) Natural Red Colorant Extract with Ultrasonic Assisted Extraction Method Yuyun Yuniati; Dhiya Dini Azmi; Eric Nurandriea; Lailatul Qadariyah; Mahfud Mahfud
ASEAN Journal of Chemical Engineering Vol 23, No 1 (2023)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ajche.77249

Abstract

In this study, the optimization and characterization of the colorant extraction process from sappan wood were carried out using the ultrasound-assisted extraction method. Sappan is proposed as a source of natural material wealth, producing a natural red colorant that is being needed by the community in the food sector. Based on this research, the optimum operating conditions for the extraction of sappan wood were obtained using a frequency of 40 kHz, a temperature of 60 °C, a ratio of 0.0050 g mL-1, an extraction time of 20 min, and the use of 60% ethanol solvent. Sappan wood extract created a yellow to reddish orange color at acidic pH (2-6), red at neutral pH (7) and shifted towards purplish red with increasing pH. The extract was qualitatively positive containing quinone, flavonoid, quinone, and tannin compounds, as well as several phenolic compounds detected in the Gas Chromatography Mass Spectroscopy qualitative test.
Co-Authors Achmad Fajrul Akbar Achmad Qodim Syafa'atullah Achmad Roesyadi Aditama, Narendra Yudha Agi Iqbal Velayas Ahmad Muklason Aisyah Triana Chintiyah Dewi Aldri Frinaldi Ali Altway Amalia Putri, Fauziah Annas Wiguno Aparamarta, Hakun Wirawasista Aswie, Viqhi Awaludin Rauf Firmansyah Awaludin Rauf Firmansyah Ayu Paramita Firdaus Darmawan, Raden Daru Satria Prayanto Delita Kunhermanti Dhaniar Rulandri Widoretno Dhiya Dini Azmi Donny Satria Bhuana Dwi Aris Setiawan Dwi Utari, Wahyuni Eric Nurandriea Eskalalita, Eskalalita Fabroyir, Hadziq Fachrudin Fachrudin Fachry Abda El Rahman Fahmi Muhammad Izzuddin Fatih Ridho Muhammad Fenni Suryanti Fikaputri Rohmatul Maula Fitria Fatmawati Fitria Romadhoni Fitrony Fitrony Gita Shintavia Hakun Wirawasista Hakun Wirawasista Harmami Harmami Hasanah, Yuliana Hidayatul Imro’atus Nur Mufidah Dimyati Putri Ina Nurfia Indraswari, Rarasmaya Indriana Purwaningsih Indriana Purwaningsih Istianah, Nur Ita Ulfin Ja'far As Shodiq Jamiliya Susantin Juwari Juwari Karim, Busro Khairudin, Nur KHOIRUL ANAM Kristianto, Teguh Kusuma, Heri Septya Kuswandi, Kuswandi M. Yogi Riyantama Isjoni Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud Mahfud mahfud mahfud Mashuri Mashuri Maula, Fikaputri Rohmatul Mochammad Ainun Hikam Mochammad Ainun Hikam Mohamad Iman Rachmadi Mohammad Fandy Ardhilla Mohammad Fandy Ardhilla Muhammad Salahudin Ni Luh Putu Hariastuti Niniek Fajar Puspita, Niniek Fajar Nuniek Hendrianie Nur Aini Rakhmawati Nur Jannah Nur Syofa Lira Dalimunthe Nur wahidah Nurkhamidah, Siti Permana, Dhiam Permata, Arif Rachman Eka Putri, Malfa Liya Raden Darmawan Raden Darmawan Rahadiantino, Lienggar Raka Selaksa Raka Selaksa Charisma Muchammad Renita Nurul Fitria Ridha Agustina Kholifatun Nisa Rizky Nurrochmad Ismail Rizky, Ratna Oktavina Rizqy Fauzi Rozi, Iqbal Fakhrur Ryvalda, Dhea Septyanonie Safetyllah Jatranti Sahiba Sahila Sarkawi Sarkawi, Sarkawi Selfina Gala Setiyo Gunawan Siti Machmudah Siti Nurhasanah Siti Zullaikah Sri Rachmania Juliastuti Subhan, Moh Suffahurrohman, M Nur Suhaimi Suhaimi Sumarno . Syafa’atullah, Achmad Qodim Syamsul Rijal Tantular Nurtono Tri Nugraha Ibnu Abdillah tri wahyuni Umar Faruq Viqhi Aswie Viqhi Aswie Wahyono, Sapto Widiyastuti Winardi, Sugeng Yeni Rahmawati, Yeni Yuyun Yuniati Zahid , Moh