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Heru Susanto
Department Of Chemical Engineering, Faculty Of Engineering, Universitas Diponegoro, Jl. Prof. Soedharto SH, Tembalang, Semarang 50275, Indonesia
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Journal : JURNAL KIMIA SAINS DAN APLIKASI

 1 
Silica-rich Sodalite Synthesis: The Effect of Variations in Ultrasound Treatment and Hydrothermal Temperature Sriatun Sriatun; Marta Chandra Anikke Putri; Hanifa Zakiyatul Urbach; Adi Darmawan; Widayat Widayat; Heru Susanto
Jurnal Kimia Sains dan Aplikasi Vol 25, No 4 (2022): Volume 25 Issue 4 Year 2022
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3852.166 KB) | DOI: 10.14710/jksa.25.4.137-145

Abstract

Silica-rich sodalite zeolite has been synthesized by ultrasound treatment and hydrothermal temperature variation. This study aimed to determine the effect of ultrasound treatment and hydrothermal temperature variations on the crystallinity, hydrophobicity, and structural properties of silica-rich sodalite zeolite. The synthesis was conducted by reacting a sodium aluminate and sodium silicate solution by varying Si/Al ratios of 20, 30, 40, 60, 80, and 90. The next step was to characterize the product. The product with the best crystallinity was used as a reference to determine the effect of ultrasound and hydrothermal temperature. The reaction gel was treated with and without ultrasound and hydrothermal using autoclave at 100, 150, and 200°C for 24 hours. The last step was the product characterization using XRD, FTIR, and GSA. The XRD showed similarity peaks at 2θ = 14.058°; 24.41°; 31.73°; 34.75°; 42.88°. The best crystallinity was silica-rich sodalite zeolite with a Si/Al ratio of 30. Meanwhile, silica-rich sodalite zeolite peaks were obtained at 2θ = 14.16°, 24.66°, 31.99°, 35.13°, and 43.39° by ultrasound treatment and hydrothermal temperature variation (100, 150, and 200°C). Ultrasound treatment revealed the presence of other peaks besides sodalite at 2θ = 19.05° and 27°, where these peaks were referred to as SAPO-56. In conclusion, the degree of crystallinity increased with increasing temperature, decreasing Si-OH/Si-O-Si showed increased hydrophobic properties. Increasing the hydrothermal temperature of 150 and 200°C with and without ultrasound treatment increased the surface area significantly to 114.137 m2/g and 160.717 m2/g, and the pore volume of sodalite with a Si/Al ratio of 30 to 0.318 cc/g and 0.274 cc/g.
Co-Authors . Widayat Abdul Ghofur Abu Rokhmad Addina Nur Adi Darmawan Adjie, Firman Tri Afdal Makkuraga Putra Agus Nur Cahyo Agus Nurawan Agustina Kumala Dewi Agustina Kumala Dewi Sholihah Andayani Andayani Anny Sulaswatty, Anny Apriliana, Pamella Aprilina Purbasari Ariestya Meta Devi Ariestya Meta Devi Arsita, Tiara Seno Asteria Apriliani Susanto Atikah Anindyarini Audityo, Muhammad Shelviano Aulia Ainis Lisa Aurum Azzahra Ayuningrum, Denandha Putri B Budiyono Bakti Jos Bambang Cahyono Bambang Pramudono Basituasi Baene Belia Alfiko Berkah Fajar Burhanudin Burhanudin Desiriani, Ria Dian Histifarina Dini Karunia Sari Dudi Hidayat Dwi Titik Apriyanti Dyah Hesti Wardhani Erdi Guna Utama Eti Sunarsih Eva Purwanti, Eva Fajar Wulandari Fajar Wulandari Faleh Setia Budi Fauzi Ahmad Bogas Fekri Pratama Filardli, Abdullah Malik Islam Firda, Nur Firdausi Husrin Fitri Fitri Gonzales, Ralph Rolly Gricela, Sara Gunawan Gunawan Gunta Wirawan Hamdani, Kiki Kusyaeri Handaja, Suka Hanifa Zakiyatul Urbach Heny Kusumayanti Hermawan Hermawan Hermawan Hesti Rahayu I G. Wenten I Nyoman Widiasa I Nyoman Widiasa Insan Suwanto Insan Suwanto irul, Khairullah irul Joddy Arya Laksmono khabibi Khabibi Khairurrijal Khairurrijal Khairurrijal Khairurrijal Kiki Kusyaeri Hamdani Kuwat Triyana Leonel Adrian Triskanto lois_denissa, Lois Denissa Lulluil Mahsunnah Lulluil Mahsunnah Luqman Buchori Maharani, Nesti Dwi Mamlukhah Mansyur Marga Dharma Prayoga Marta Chandra Anikke Putri Meindy Catur Risqiputra Muhammad Cholid Djunaidi Muhammad Luqman Bukhori Muhammad Rafly Pramudya Nagoro, Ignatius Henry Adi Ngadiwiyana M.Si. S.Si. Nisrina Nita Aryanti Nor Basid Adiwibawa Prasetya Novery Lysbetti Novi Syafa’atun Novintan Elistya Nur Firdausi Husrin Nur Mufarokhah Nur Rokhati Nurcahyo, Agus Nurcahyo, Agus Nurhafifah, Meilina Nursyamsu Nursyamsu Nursyamsu Nursyamsu Olivedia Justin Wijaya Oppie, Oppie Pardoyo Pardoyo Pertiwi Andarani Prasetiya, Hafiizh Qomariah Qomariah Rahmania, Yusi Luluk Ratnadewi, Dwijani Rika Wahyuni Rika Wahyuni Risa Suryana Rosmaiyadi Satrio Kuntolaksono Serlina Adelia Setiawan, Arief Ameir Rahman Siahaan, Samuel Ezra Sima, Sima Siswo Sumardiono Sri Mulyani Sriatun Sriatun Susan Neni Triani Tamara Cindy Samsita Rani Titik Istirokhatun Tri Martini Tutuk Djoko Kusworo Umi Baroroh Lili Utami Utama, Erdi Guna Wawan Wahyudin Wibowo, F Mukti Widianti, Nurhannah Widiyanto, Edhi Wiloso, Edi Iswanto Wishnu Wijaya Yanuar Ariyanto Yanuardi Raharjo, Yanuardi Yoga Prasetya ZAMAN, Badrus Zetli, Sri Zulfahita, Zulfahita