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Optimization of Red Ginger (Zingiber officinale var. Rubrum) Extraction Using Microwave Assisted Hydrodistillation Method Nurjanah, Sarifah; Rosalinda, Sari; Andina, Dwita Putri
Jurnal Teknik Pertanian Lampung (Journal of Agricultural Engineering) Vol. 13 No. 2 (2024): June 2024
Publisher : The University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jtep-l.v13i2.369-380

Abstract

Red ginger is a spice plant that has high economic and social value. One of the uses of red ginger is to process it into a product, namely essential oil. This study aims to determine the optimization of the extraction process conditions on solvent volume, time, and extraction power that can produce optimum yield and residual content of red ginger essential oil solvent. The extraction was carried out with the help of microwaves. The research method is experimental design and optimization process with Response Surface Methodology (RSM) type Box-Behnken Design (BBD). The results showed that the optimum yield was at 700 mL solvent volume, 1 min extraction time, and 10% power (69.9 watts) with the equation Y = 0.2076 + 0.0262A – 0.0300B – 0.0013C and the concentration conditions the optimum remaining solvent with the equation Y = 4.98 – 1.0000A + 4.56B + 5.44C. The optimal yield of red ginger essential oil was 0.205%, with a residual solvent content of 3.8%, specific gravity 0.885, acid number 1.399, refractive index 1.485. The results of the optimum residual solvent content of -6.023%. Based on the results obtained, the yield value with the help of microwaves is higher than that without the help of microwaves. Keywords: Essential oil, Microwave, Residual solvent content, Response surface methodology (RSM), Yield.
KARAKTERISASI BIODIESEL DARI MINYAK KEMIRI SUNAN DENGAN KATALIS HETEROGEN SILIKA TERIMPREGNASI KALSIUM OKSIDA (CaO/SiO2 ) Haryono; Yati B. Yuliyati; Atiek Rostika Noviyanti; Mochammad Rizal; Sarifah Nurjanah
Jurnal Penelitian Hasil Hutan Vol. 38 No. 1 (2020): Jurnal Penelitian Hasil Hutan
Publisher : BRIN Publishing

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20886/jphh.2020.38.1.10-20

Abstract

Commercial biodiesel of oil palm is controversial as the palm oil is classified as food oil and palm plantation utilizesfertile land. One potential type of vegetable oil as biodiesel raw material is kemiri sunan (Reutealis trisperma(Blanco) Airy Shaw) oil. This research aimed to prepare a heterogeneous solid catalyst in the form of an impregnatedSiO2by CaO catalyst (CaO/SiO2), to study the effect of the esterification stage on free fatty acid (FFA) content ofoil, and to test the activity of the CaO/SiO2catalyst during the trans-esterification stage for biodiesel formation. CaO/SiO2catalysts were prepared by sol-gel method made from natural materials (egg shells and rice husk). The FFAcontent of kemiri sunan oil was determined through various esterification stages namely 1; 1.5; and 2 hours in thepresence of H2SO4catalyst. While the trans-esterification stage was carried out under reaction temperature of 60°C,oil to methanol ratio of 1:9, reaction time of 2 hours and CaO/SiO2catalyst content of 3%. The results showed thatthe esterification stage for 1; 1.5; and 2 hours reduced the FFA content from 12.5% (without esterification) to 0.65%;0.58%; and 0.54% respectivaly. Biodiesel made from kemiri sunan oil which was synthesized with the addition ofCaO/SiO2catalyst at optimal conditions of trans-esterification stage fulfilled SNI 7182-2015: Biodiesel based ondensity, viscocity, moisture content, iodine number, and cetane number.
Rekayasa Waktu Dan Temperatur Penyulingan Untuk Peningkatan Rendemen Minyak Atsiri Kulit Jeruk Lemon (Citrus Limon. L) Fadila, Abil; Nurjanah, Sarifah; Rosalinda, Rosalinda
JURNAL REKAYASA DAN MANAJEMEN AGROINDUSTRI Vol 14 No 1 (2026): Maret
Publisher : Department of Agroindustrial Technology, Faculty of Agricultural Technology, Udayana University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24843/JRMA.2026.v14.i01.p08

Abstract

Lemon processing generates a substantial amount of peel waste, accounting for approximately 40-50% of the total fruit weight. The lemon peel, particularly the flavedo layer, contains essential oil compounds with the potential to be developed into value-added products through distillation. This study evaluates the influence of distillation duration and temperature parameters on the yield and physicochemical quality of essential oil derived from lemon peel waste. The experiment employed a Factorial Completely Randomized Design (CRD) with two factors: distillation time (P = 4, 5, 6, 7, and 8 hours) and distillation temperature (T = 83, 90, 100, 110, and 117°C). The observed parameters included oil yield, specific gravity, refractive index, acid value, and solubility in 70% alcohol. Data were processed using Analysis of Variance (ANOVA) followed by Duncan's Multiple Range Test (DMRT) at a 95% confidence level. The findings indicate that distillation time significantly affects the essential oil yield, whereas temperature variations within the tested range do not show a significant impact. The highest yield of 0.84% was achieved at a distillation time of 8 hours at 100°C. The resulting essential oil exhibited a specific gravity of 0.851 g/mL, a refractive index of 1.473, an acid value of 5.60 mg KOH/g, and a 1:10 solubility in 70% alcohol, all of which meet quality standards. These results demonstrate that optimizing distillation conditions can enhance yield while maintaining the quality of lemon peel essential oil.
Model Sorpsi Isotermis sebagai Dasar Pendugaan Masa Simpan Biji Pala (Myristica fragrans) Jamalludin, Jamalludin; Nurjanah, Sarifah; Rialita, Tita; Rienoviar, Rienoviar; Rosalinda, Sarinarulita
Teknotan: Jurnal Industri Teknologi Pertanian Vol 20, No 1 (2026): TEKNOTAN, April 2026
Publisher : Fakultas Teknologi Industri Pertanian

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Pala (Myristica fragrans) merupakan salah satu komoditas perkebunan unggulan Indonesia dengan nilai ekspor yang cukup tinggi dan prospek pasar yang terus meningkat. Biji pala banyak dimanfaatkan pada berbagai bidang, mulai dari industri pangan sebagai bahan penyedap dan flavoring, industri farmasi sebagai komponen obat tradisional, hingga industri kosmetik. Meskipun demikian, dalam beberapa tahun terakhir sejumlah negara tujuan ekspor menolak pengiriman pala Indonesia karena kadar aflatoksin yang terdeteksi melebihi ambang batas maksimum yang diizinkan. Aflatoksin umumnya terbentuk akibat kontaminasi jamur selama proses panen maupun pascapanen, terutama ketika kondisi kadar air tidak terkendali. Proses pengeringan yang kurang optimal dan penyimpanan yang tidak sesuai seringkali meningkatkan kadar air biji pala sehingga menciptakan lingkungan yang mendukung pertumbuhan kapang penghasil aflatoksin. Oleh karena itu, penentuan kadar air kesetimbangan dan kondisi penyimpanan yang tepat melalui pendekatan sorpsi isotermis sangat penting untuk meminimalkan risiko kontaminasi. Penelitian bertujuan mengidentifikasi kondisi penyimpanan optimal yang mampu mencegah pertumbuhan mikroorganisme penghasil aflatoksin pada biji pala. Metode yang digunakan adalah eksperimen dengan menentukan Kurva Sorpsi Isotermis menggunakan larutan garam jenuh NaOH, CH3COOK, MgCl2, Kl, NaCl, KCl, BaCl2, pada berbagai tingkat aktivitas air. Data hasil pengukuran kemudian dianalisis menggunakan model sorpsi Halsey, Henderson, Caurie, Oswin, Chen-Clayton, GAB, dengan mengevaluasi akurasi melalui perhitungan nilai Mean Relative Deviation (MRD). Hasil penelitian menunjukkan bahwa model Oswin  y=0.0851x+0.0333 menghasilkan nilai MRD terendah yaitu 1,6497, sehingga model yang paling sesuai dalam memprediksi kadar air kesetimbangan bubuk pala. Dengan demikian, model Oswin dapat dijadikan acuan dalam merancang strategi pengeringan dan penyimpanan pala untuk menjaga mutu serta meningkatkan ekspor
Optimization of Microwave-Assisted Hydrodistillation from Indonesian White Pepper (Piper nigrum L.) Essential Oils Sekar Widyaningrum; Sarifah Nurjanah; Bambang Nurhadi; S. Rosalinda; Rienoviar Rienoviar
Jurnal Teknik Pertanian Lampung (Journal of Agricultural Engineering) Vol. 14 No. 2 (2025): April 2025
Publisher : The University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jtep-l.v14i2.362-371

Abstract

Pepper is one of the agricultural commodities that Indonesia widely exports. Pepper can be processed into various products, including essential oils. Pepper essential oil can be extracted using several methods, including the microwave. This method can speed up the essential oil extraction process. Optimization was carried out using the Box-Behnken design using the three independent parameters: solution ratio, time, and microwave power. The upper and lower limits used for the independent variables are solvent amount of 1,350 mL and 750 mL, time of 90 minutes and 60 minutes, and microwave power of 440 watts and 136 watts. The optimal data generated is treatment with a solvent amount of 1,050 mL, 90 minutes, and 440 watts of power, resulting in validation data of 99.046%. The optimal essential oil treatment gives a specific gravity of 0.8281, a refractive index of 1.4824, solubility in ethanol 1:2, acid number 0.739 mg KOH/g, ester number 19.599 mg KOH/g, and a hue value of 186,38 (green). Oil with optimum treatment also has an IC50 antioxidant activity of 32,919.9 ppm. Keywords: Antioxidant; Extraction; Microwave; Pepper; RSM.
Enhancing Sustainability in Packaging: Response Surface Optimized Sago Pith Waste Biocomposites with PBAT and MDI Maya Irmayanti; Sarifah Nurjanah; Akbar Hanif Dawam Abdullah; Rossy Choerun Nissa; Yeyen Nurhamiyah
Jurnal Teknik Pertanian Lampung (Journal of Agricultural Engineering) Vol. 14 No. 3 (2025): June 2025
Publisher : The University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jtep-l.v14i3.979-990

Abstract

This study aims to optimize the biocomposites of sago pith waste (SPW) for sustainable packaging applications. The biocomposite was prepared using the biodegradable polymer polybutylene adipate-co-terephthalate (PBAT) as a matrix and methylendifenyl diisocyanate (MDI) as a chain extender. RSM-CCD was used to assess the impact of the incorporation of SPW (5-20% p/p) and MDI (1–5%) into the PBAT matrix on the tensile strength and elongation of biocomposites by melt mixing. The optimal formula shown by RSM was 5% SPW and 5% MDI, which resulted in a 5.14 MPa tensile strength and 8.14% elongation. The barrier properties of all treatments, including moisture content, contact angle, and water absorption, were checked. The optimal formula showed good barrier properties compared to other treatments: water content of 3.12%, contact angle of 42.84°, and water absorption of 0.82%. Other characterizations of SEM, FTIR, DSC, TGA, and biodegradability tests showed an increase in SPW-PBAT compatibility due to the use of MDI. MDI as a chain extender had a positive impact on the material's strength, and the addition of SPW accelerated the degradation process, thus improving biodegradability. Keywords: Biocomposite, Chain extender, Melt-mixing, Response Surface Methodology, Sago pith waste.
Optimasi kondisi proses pengeringan ampas wortel menggunakan RSM dan pemanfaatannya sebagai masker gel peel off Asri Widyasanti; Tiara Namira; Sarifah Nurjanah
AGROINTEK Vol 19, No 3 (2025)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v19i3.20431

Abstract

Carrot pulp is a by-product of juice production with a source of pectin and carotene precursors of vitamin A. One way to use carrot pulp is through a drying process, such as convection drying, to produce carrot pulp flour. The purpose of this study was to determine the optimal conditions for drying carrot pulp using a food dehydrator, to determine the characteristics of carrot pulp powder under optimal conditions, and to determine the potential of carrot pulp powder in preparing peel off gel masks. The parameters in this study were moisture content, ash content, and drying yield. In addition, the parameters observed in the optimum carrot pulp flour were color and antioxidant activity. The dryer used was a food dehydrator operating at a temperature range of 45°C to 65°C for a duration of 20 to 26 hours. This research method was an experimental method with optimization using the Response Surface Methodology (RSM) type Central Composite Design (CCD) in the Design Expert 13 application. RSM determined the optimal drying process condition to be 65°C for 26 hours. This condition resulted in a product with a moisture content of 3.033%, an ash content of 5.326% and a drying yield of 11.062%. Carrot pulp flour produced under optimal drying conditions, when formulated into a peel off gel mask preparation, exhibited a drying time of 15-21 minutes.
Pemodelan kondisi hidrodistilasi minyak atsiri jahe merah (Zingiber officinale var. Roscoe) dengan menggunakan Response Surface Methodology Annissa Ramadhanti; Sarifah Nurjanah; Asri Widyasanti; Nurul Ainina
AGROINTEK Vol 18, No 2 (2024)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v18i2.18904

Abstract

Red ginger contains volatile components that are essential oils. Essential oils can be obtained through the distillation method. Hydrodistillation is a method of distillation that involves providing direct contact between the materials and water at a high temperature, which is influenced by several factors, including time and the solvent feed ratio (SF ratio). This study aimed to determine the best conditions for high yields and essential oil quality using SNI No. 06-1312-1998 as a reference. The research method used was experimental research, and optimization was carried out using Response Surface Methodology (RSM) with CCD design. The treatments for distillation were time (2 hours, 4 hours, and 6 hours) and solvent feed (SF) ratio (8:1, 10:1, and 12:1). The parameters observed were yield, residual solvent content, specific gravity, refractive index, and acid number. The results showed that the time and SF ratio variables had no significant effect on the yield but had a significant effect on the residual solvent content. The optimization process resulted in a time of 6 hours and a solvent volume of 720 ml (ratio 1:12), yielding 0.14 with a residual solvent content of 3,557%. The characteristics of the essential oils produced were 0.8794 for the specific gravity, 1.473 for the refractive index, and 2.13  for the acid number. Red ginger essential oil met the requirements of SNI ginger oil on the parameters of specific gravity and refractive index.
Exploration of Antifungal Tests Based on Δ-Guaiene From Subang Patchouli Oil Rahmi Rahmawati; Sarifah Nurjanah; Tita Rialita; Efri Mardawati; Fitry Filianty
International Journal of Science and Environment (IJSE) Vol. 5 No. 3 (2025): August 2025
Publisher : CV. Inara in Colaboration with www.stie-sampit.ac.id

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51601/ijse.v5i3.194

Abstract

Guaiene is a derivative compound produced as a byproduct in the production of patchouli alcohol from patchouli oil (Pogostemon cablin Benth.). This study aims to evaluate the antifungal activity of δ-guaiene extracted from patchouli oil originating from Subang against four types of skin pathogenic fungi: Aspergillus niger, Candida albicans, Microsporum gypseum, and Trichophyton mentagrophytes. The method used was a laboratory experiment, with the main parameters observed including Inhibition Zone Diameter (IZD), Minimum Inhibitory Concentration (MIC), and Minimum Fungicidal Concentration (MFC). The results showed that δ-guaiene inhibited the growth of C. albicans at a concentration of 40%, with an IZD of 0.15 mm. Against A. niger, the compound demonstrated an inhibition zone of 1.4 mm at a 20% concentration and had an MFC of 20%. For T. mentagrophytes, an IZD of 0.4 mm was observed, with both MIC and MFC at 20%. Activity against gypseum showed an IZD of 0.25 mm, with MIC and MFC also at 20%. These findings suggest that δ-guaiene from patchouli oil has potential as a candidate antifungal agent derived from local resources, supporting the development of natural bioactive compounds and sustainability.
Genetic gain and relationship of yield and yield attributes of mutant and cross-bred stevia (Stevia rebaudiana) genotypes Suseno Amien; Haris Maulana; Dedi Ruswandi; Sarifah Nurjanah
Biodiversitas Journal of Biological Diversity Vol. 22 No. 8 (2021)
Publisher : Society for Indonesian Biodiversity

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13057/biodiv/d220805

Abstract

Abstract. Amien S, Maulana H, Ruswandi D, Nurjanah S. 2021. Genetic gain and relationship of yield and yield attributes of mutant and cross-bred stevia (Stevia rebaudiana) genotypes. Biodiversitas 22: 3119-3126. Plant breeding programs involved many traits and genetic parameters in the selection process. The information on genetic parameters on yield and other related traits provided an overview for breeders and farmers in selecting new superior genotypes. The purpose of this study was to estimate genetic parameters including heritability and genetic gains in yield and other traits, to determine the relationship between various traits, and to select superior stevia (Stevia rebaudiana Bertoni) genotypes for each trait. Field experiments were carried out in two planting environments, namely, the highlands and the medium plains employing a randomized completed block design and each genotype was three replicates. The results showed that the yield had high heritability and genetic gains  ??in mutant populations, whereas cross-bred populations had moderate heritability and low genetic gains. Stem weight (SW) and number of leaves (NoL) traits were identified as having high heritability and genetic gains in both populations. The GT biplot measurement showed that the yield was identified to have a significant and positive correlation with SW (p<0.05). H4 was correlated with Number of branches (NoB), Yield, SW, and chlorophyll content (Chl) traits in the cross-bred populations. H9 excelled on and was correlated with NoL and plant height (PH). M11 was identified to be highly correlated with NoL, PH, NoB, and Chl traits in the mutant populations, while M15 excelled on and was correlated with yield and SW. The results of this study revealed that there was a potential for improvement in the traits tested of stevia through cross-bred and mutant populations in different environmental conditions. The selected genotypes can be developed in a suitable environment and used for further stevia plant breeding programs.  
Co-Authors Abdullah Md Zain Abil Fadila Ade Moetangad Kramadibrata Agil Firhan Iskandar Agnes Klarasitadewi Ahmad Thoriq Ainina, Nurul Akbar Hanif Dawam Abdullah Anas Bunyamin Andina, Dwita Putri Andri Permana Annissa Ramadhanti Arinda Nur Ariva Asri Widyasant Asri Widyasanti Atiek Rostika Noviyanti Azizah, Ise Wafiq Bambang Nurhadi Boy Macklin Pareira Prawiranegara Budhi Indrawan David S. Marpaung Dedi Ruswandi Dedy Prijatna Dina Aprilia Dwi Merita Rosi Dwita Putri Andina E Gumbira-Sa’id - Efri Mardawati Efri Mardawati Eki Dwiyan Saputra Elazmanawati Lembong Ema Komalasari Etty Riani Fadila, Abil Fakhira, Qonita Raihani Fany Trihapsoro Farah Nuranjani Farah Nuranjani Fathia Salsabila Emmaputri Fawaiz, Husni Syamil Fitry Filianty Galih Adhi Respati Gumbira-Sa'id, E Handarto Haris Maulana HARYONO Haryono Haryono Haryono Haryono Hilman Syaeful Alam Huda Nurul Quddus Ibrahim A. I. Ifmalinda Ilham Fajri Imas Siti Setiasih Indira Lanti Kayaputri Intan Aprilia Irene June Sidabutar Isti Sulistiani Jamalludin, Jamalludin Jeremia Kristian Khaswar Syamsu Khaswar Syamsu - Kurnia, Ina Laily Rizki Safira Lita Fitriyani Khairunisa M. Ade Moetangad Kramadibrata Maya Damayanti Maya Irmayanti Mimin Muhaemin Mochammad Rizal Mochammad Rizal Muhammad Gilang Ramadhan Muhammad Rizky Ramanda Muhammad Saukat Nadyah Rachma Dewi Namira, Tiara Nedia Cahyati Muchtarina Nedia Cahyati Muchtarina Novia Dwi Anggraeni Nur Oktavia Benedicta Nuranjani, Farah Nurfauziah, Isni Nurpilihan Bafdal Nurul Ainina Nurul Ainina Pirdani Nur Fitri Prisilia Ratna Setyaningrum Puji Lestari Pusponegoro, Annisa Putri, Farinissa Deliana Qurratu’ain, Yona Rahmawati, Rahmi Rahmi Rahmawati Reza Permana Aji Rienoviar Rienoviar Rienoviar, Rienoviar Rifki Amrullah Rizika Wulandari Rizky Mulya Sampurno Rizqi Putri Fathoni Rosalinda Rosalinda Rosalinda, Sari Rosalinda, Sarinarulita Roshita Ibrahim Rossy Choerun Nissa Rudi Adi Saputra Ruth Anggia Assyera S Rosalinda S. Rosalinda S. Rosalinda S. Rosalinda, S. Salman Hafidz Sarinarulita Rosalinda Sekar Widyaningrum Selly Harnesa Putri Septianti, Nur Alifa Shayana Junita Sudaryanto Zain Sudaryanto Zain Sudaryanto Zain Sudaryanto Zain Suprihatin - Suprihatin Suprihatin Suseno Amien Thoriq, Ahmad Tiara Namira Tio Febriananda Tita Rialita Tita Rialita Totok Herwanto Totok Pujianto Totok Pujiyanto Wahyu Daradjat Wahyu Kristian Sugandi Yati B Yuliyati Yati B. Yuliyati Yeyen Nurhamiyah Yona Qurratu’ain Zahrah Eza Arpima Zhaqqu Ilham Alhafidz Zulfaa Irbah Zain ‪Irna Dwi Destiana