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Chemical Engineering Department, Faculty Of Sain And Technology, Universitas Jambi, Jambi Department Of Agriculture Product Technology, Faculty Of Agriculture, University Of Jambi Centre Of Excellent In Bio-Geo Material, University Of Jambi
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Journal : Bulletin of Chemical Reaction Engineering

 1 
Oxidation of Styrene to Benzaldehyde Using Environmentally Friendly Calcium Sulfate Hemihydrate-Supported Titania Catalysts Koesnarpadi, Soerja; Wirawan, Teguh; Nurhadi, Mukhamad; Wirhanuddin, Wirhanuddin; Prananto, Yuniar Ponco; Nazarudin, Nazarudin; Degirmenci, Volkan; Lai, Sin Yuan; Nur, Hadi
Bulletin of Chemical Reaction Engineering & Catalysis 2024: BCREC Volume 19 Issue 4 Year 2024 (December 2024)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20224

Abstract

This paper presents the synthesis and characterization of calcium sulfate hemihydrate (CSH)-supported titania (TiO2) catalysts and their application in the environmentally friendly oxidation of styrene to benzaldehyde using hydrogen peroxide (H2O2) as the oxidant. The study explores the catalyst's structure-activity relationship, emphasizing the importance of mesoporous materials for enhanced catalytic performance. The CSH-Titania catalysts were synthesized using fish bone-derived CSH as a support, which aligns with green chemistry principles. Characterization techniques such as Fourier Transform Infra Red (FTIR), X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), and Brunauer-Emmett-Teller (BET) surface area analysis confirmed the successful impregnation of titania and its catalytic efficiency. The catalysts exhibited high selectivity for benzaldehyde, achieving up to 49.45% conversion of styrene, with benzaldehyde as being the main product. The research highlights that the catalyst’s performance decreased after calcination due to a reduced surface area and pore volume, yet it maintained recyclability across three cycles with minimal  lose  in selectivity loss. Overall, this study introduces a cost-effective and sustainable approach to styrene oxidation, demonstrating the potential for industrial application in producing high-value chemicals with minimal environmental impact. Copyright © 2024 by Authors, Published by BCREC Publishing Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Co-Authors -, Maison AA Sudharmawan, AA Abu Bakar Abu Bakar Achmad, E Adang, Ferry Ade Yulia Afreni Hamidah Afrida Afrida Agus Ari Setiawansyah Agus Salim Agus Salim Agustini, Yetty Ahmad Syadzali Amalia, Rahma Andi Aderus Andrilolo, Andrilolo Arafi Satria Nugraha Ardina, V Aris Doyan Aris Doyan Asep Bambang Susanto asih, yekti purwo Asni Johari Asrial Asyhar, R Balqis Rahmatullah Putri Bilady, Royhan Darmiyati Dedi Gusriadi Degirmenci, Volkan Deni Irawan Dewantara, Dede Dian Wulansari Dian Wulansari Dwina, Dila Oktarise Dyah Kumalasari E. Maryana Edy Panda Erawaty, Lela Ervan Johan Wicaksana Evita Anggereini Firdaus Muhammad FITRY TAFZI Friani, Desi Gusriadi, Dedi Hadi Nur Hadistya Suryadri Hesti Megawati Hutwan Syarifuddin I. Rahmayani Ibnatun Rif'ah Ilham Falani Indra Agung Pratama Indra Indra Indriyani Indriyani, I Iqbal Ridho Juliandri Ira Galih Ira Galih Prabasari Irma Rahmayani Irma Rahmayani Ismail, Gurawan Dayona Juanda, Adrisma Jumardi Budiman Junri anton Situmorang Kanto, Rizky Khusnelia, Jeni Kurniaty, Dwi Lai, Sin Yuan Lavlinesia Lavlinesia Lavlinesia, lavlinesia Leny Marlinda Lisani Lisani, Lisani M. Rizki Mahardini, Angger Putri Mahmuddin Mahmuddin Marlinda, Leny Muhammad Agus Muljanto Mukhamad Nurhadi, Mukhamad Mundarti, Sri Murdia, Agus Miranda Mursalin, M Mursyid . Mursyid Mursyid N Panjaitan Nawahdani, Ahmad Mansur Ninada Ninada Nova Andriani Nova Kafrita Nur Wulandari Nursela, S Oki Alfernando Pamungkas, Putra Panda, Edy Pratami, Tesy Putri Sakinah Harahap Putri, Niken Tasya Clara Ra'ida Raudhatussya'rifah Rahayu Suseno Rahmawati, Medina Alia Rahmayani, I Ramadani, Suci Putri Rara Ayu Lestary Recky, Recky Ria Amelia Yolanda Rifqi Oktarianda Rizky Kanto Rosmawati Sipayung Rosyani Rulaini, Melati S.P. Amalia Said Sanimubarak Al'qudusi Salsabila Setyaningsih Seftiananda Pratama Septikasari, Anisa Nur Septina Yuri Cahyati Silvi Leila Rahmi Siregar, Nurainun Siti Nursela Soerja Koesnarpadi Sri Widiyawati Sulistiana, Ika Putri Sunarno Sunarno Surhaini Surhaini, Surhaini Suripto Dwi Yuwono SUSENO, JOKO Susilawati - Teguh Wirawan, Teguh Tezar, Muhammad Tomara, Anggel Ulyarti Wahyu Ningrum, Wulan Wahyudi Zahar Widyaningsih, Atria Tiffany Widyastuti, Nita Winda Ananda Wirhanuddin, Wirhanuddin Y. G. Armando Yani, Zunarta YG Armando Yogie Yogendra Hans Yuana yuana, Yuana Yuniar Ponco Prananto Yusfi, Liza Aulia Zunarta Yani