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Journal : Journal of Science Innovare

SYNTHESIS OF SCHIFF BASE VERDANTIOL BY SIMPLE CONDENSATION Niken Oktaviani; Leny Heliawati; Yudhie Suchyadi
Journal of Science Innovare Vol 2, No 2 (2019): Journal of Science Innovare, September 2019
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (109.144 KB) | DOI: 10.33751/jsi.v2i2.1533

Abstract

Schiff base is a chemical compound that is formed from the reaction between aldehydes and primary amines by condensation and produces by-products in the form of water. Schiff base is the raw material that is added in making Fragrance. The purpose of this study was to determine the method of synthesis of Schiff base verdantiol with simple condensation. The research method was carried out with four stages: preparation, synthesis, testing and measurement of parameters, and calculations. Preparation includes weighing the raw material Schiff base verdantiol. Schiff base synthesis is carried out by stirring at a temperature of about 90°C ± 5° C (Arctender, 1969) with a modification time of 15 minutes, 30 minutes, 1 hour, 2 hours and 3 hours. Testing and measurement parameters include organoleptic, density and specific gravity tests in pycnometer and compound confirmation using Gas Chromatography Mass Spectrometry. The results showed that the optimum synthesis of Schiff base verdantiol compounds was carried out at a heating time of 2 hours. The results of odor, color, density and gravity specifications heating time 2 hours according to specifications with the standard. GCMS confirmation results at 2 hours percent similarity are above 94%.
DEVELOPMENT OF COD (CHEMICAL OXYGEN DEMAND) ANALYSIS METHOD IN WASTE WATER USING SPECTRODIRECT Ade Heri Mulyati; Leny Heliawati; Sutanto .; Uswatun Hasanah; Diana Widiastuti; Siti Warnasih; Yulian Syahputri
Journal of Science Innovare Vol 3, No 2 (2020): Journal of Science Innovare
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33751/jsi.v3i2.3006

Abstract

Increased human activities will cause various problems, one of which is water pollution in water sources because it receives a pollution load that exceeds its carrying capacity. In the context of environmental conservation, the government has set quality standards for liquid waste produced by various industries and other activities in a Decree of the State Minister for the Environment. COD (Chemical Oxygen Demand) is one of the most important parameters in wastewater quality standards. This study aims to validate the COD analysis method which refers to COD Thermoreactor System (LOVIBOND brand) at Pakuan University Service Laboratory, to ensure the validity of COD analysis results at Pakuan University Service Laboratory. Spectrodirect COD analysis method provides results that meet the requirements of accuracy, precision, LOD, and LOQ which is quite good. The results of the Coefficient of Variation give good results with a value of 1.8841% indicating the accuracy of the analysis method is good. The accuracy parameter also gives good results and meets the requirements with a% recovery value of 98.70351%. Overall, it can be stated that the spectrodirect analysis method tested is an accurate, precise, simple, and economical method for determining COD levels
SYNTHESIS OF SCHIFF BASE VERDANTIOL BY SIMPLE CONDENSATION Niken Oktaviani; Leny Heliawati; Yudhie Suchyadi
Journal of Science Innovare Vol 2, No 2 (2019): Journal of Science Innovare, Volume 02 Number 02 2019
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33751/jsi.v2i2.1533

Abstract

Schiff base is a chemical compound that is formed from the reaction between aldehydes and primary amines by condensation and produces by-products in the form of water. Schiff base is the raw material that is added in making Fragrance. The purpose of this study was to determine the method of synthesis of Schiff base verdantiol with simple condensation. The research method was carried out with four stages: preparation, synthesis, testing and measurement of parameters, and calculations. Preparation includes weighing the raw material Schiff base verdantiol. Schiff base synthesis is carried out by stirring at a temperature of about 90°C ± 5° C (Arctender, 1969) with a modification time of 15 minutes, 30 minutes, 1 hour, 2 hours and 3 hours. Testing and measurement parameters include organoleptic, density and specific gravity tests in pycnometer and compound confirmation using Gas Chromatography Mass Spectrometry. The results showed that the optimum synthesis of Schiff base verdantiol compounds was carried out at a heating time of 2 hours. The results of odor, color, density and gravity specifications heating time 2 hours according to specifications with the standard. GCMS confirmation results at 2 hours percent similarity are above 94%.
DEVELOPMENT OF COD (CHEMICAL OXYGEN DEMAND) ANALYSIS METHOD IN WASTE WATER USING SPECTRODIRECT Ade Heri Mulyati; Leny Heliawati; Sutanto .; Uswatun Hasanah; Diana Widiastuti; Siti Warnasih; Yulian Syahputri
Journal of Science Innovare Vol 3, No 2 (2020): Journal of Science Innovare, Volume 03 Number 02 2020
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33751/jsi.v3i2.3006

Abstract

Increased human activities will cause various problems, one of which is water pollution in water sources because it receives a pollution load that exceeds its carrying capacity. In the context of environmental conservation, the government has set quality standards for liquid waste produced by various industries and other activities in a Decree of the State Minister for the Environment. COD (Chemical Oxygen Demand) is one of the most important parameters in wastewater quality standards. This study aims to validate the COD analysis method which refers to COD Thermoreactor System (LOVIBOND brand) at Pakuan University Service Laboratory, to ensure the validity of COD analysis results at Pakuan University Service Laboratory. Spectrodirect COD analysis method provides results that meet the requirements of accuracy, precision, LOD, and LOQ which is quite good. The results of the Coefficient of Variation give good results with a value of 1.8841% indicating the accuracy of the analysis method is good. The accuracy parameter also gives good results and meets the requirements with a% recovery value of 98.70351%. Overall, it can be stated that the spectrodirect analysis method tested is an accurate, precise, simple, and economical method for determining COD levels
Co-Authors Ade Gunawan Ade Gunawan Ade Heri Mulyati Ade Heri Mulyati, Ade Heri Adinda Adriansyah, Putri Nabila Adriansyah, Putri Nabila Adinda Afakillah, I.Ibnu Agus Ismangil Anna Muthia Soliha Anna Permanasari Asep Kadarohman Asep Saepulrohman Bibin Rubini Bibit Harianto Bustanussalam Bustanussalam Carlina Anggraeni Carsono, Adi Dadang Jaenudin Diana Widiastuti Didit Ardianto Didit Ardianto Dwi Pursitasari, Indarini Eka Herlina Elvi Kurniasih Elvi Kurniasih Eris Septiana Farida Nuraeni Fauzia Nurul Izzati Fauziah, Zahra Nur Fauzy Rachman Fenny Pebriani Fenny Pebriani Firmayanto, Rudi Giyanto Giyanto Henrikus Suparjono Herlina Herlina I. Dwi Pursitasari I.Ibnu Afakillah Indang Dwi Rahayu Indarini Dwi Pursitasari Irvan Permana Juliatriyani Juliatriyani Kabir, Abyan Jausan Karimah, Fani Ulya kerans, geterudis Khoiriyah, Ainun Kurniasih, Septi Kurniasih, Surti Layung Paramesti Martha Lidiawati, Linda Linda Jati Kusumawardani Linda lidiawati Linda Lidiawati Linda Lidiawati M Zainal Arifin, M Zainal Mahrun Mahrun Mahrun Mahrun, Mahrun Makmuri Makmuri Melani Nurastuti Misbah Misbah Momo Rosbiono Mr Sjaeful Anwar Muhammad Fathurrahman Muhammad Fathurrahman Mulyani, Pangastuti Sri Nabila Adinda Adriansyah, Putri Nanang Winarno Niken Oktaviani Nulhakim, Lukman Parlindungan Sinaga Partomuan Simanjuntak Pebriani, Fenny Prasetyorini Prasetyorini Pursitasari, I. Dwi Rahmawati, Siti Irma Ramadhan, Muhamad Farhan Rd. Nia Elisa Yulianti Rienoviar, - Rita Retnowati Rudi Firmayanto Salam, Abduh Semuel Unwakoly Siti Fatimah Siti Warnasih Sundari, Tri Surti Kurniasih Sutanto . Syamsiah Syamsiah Taufik, Annisa Novianti Tri Aminingsih Tri Aminingsih Tri Sundari Uswatun Hasanah Utami, Indri Sari Uun Sundari Uun Sundari Uun Sundari Warliyah, Heli Wien Kusharyoto Yatri Hapsari Yudhie Suchyadi Yulian Syahputri Yuliani, Galuh Zulnaidi, Hutkemri