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Andri Prasetiyo
Fakultas Farmasi Universitas Pancasila
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The transformation of titrimetric methods in pharmaceutical, herbal and food analysis: a literature review (2013–2026s) Faridah Faridah; Diva Dwi Putri Permatasari; Andri Prasetiyo; Intan Permata Sari
JURNAL ILMU KEFARMASIAN INDONESIA Vol. 24 No. 2 (2026): JIFI In Press
Publisher : Faculty of Pharmacy, Universitas Pancasila

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35814/jifi.v24i2.2183

Abstract

The development of analytical methods in the fields of pharmaceuticals, plant/herbal ingredients, and food shows a significant transformation from classical titrimetry toward more selective and efficient instrumental and digital techniques This study aims to evaluate method transformation, comparative validity, and the application of green analytical chemistry (GAC) principles in pharmaceutical, herbal, and food analysis based on a literature review. A non-systematic narrative literature review was conducted on 28 Scopus-indexed journal articles covering titrimetry, UV-Vis spectrophotometry, chromatography (HPLC and RP-HPLC), Karl Fischer, atomic spectrometry, as well as μPAD-based innovations, conductometry, and digital analysis. The synthesis showed that classical methods remain relevant because of their simplicity, low cost, and accessibility, but their selectivity may be limited in complex matrices. Instrumental methods generally provide improved precision, accuracy, and selectivity, particularly for multicomponent samples, whereas miniaturization and digitization enhance analytical efficiency and reduce resource requirements. However, explicit integration of GAC principles remained limited, with only 7 of the 28 reviewed studies demonstrating identifiable green analytical strategies. These findings indicate that analytical modernization does not necessarily result in greener methods. Overall, analytical method development is increasingly integrative, combining classical and instrumental approaches according to analytical requirements, matrix complexity, and sustainability considerations. This review therefore provides a structured evaluative framework for selecting and transforming analytical methods across pharmaceutical, herbal, and food matrices.
Co-Authors Ade Yeni Aprilia Aey Fadilah, Yasin Agustia, Rini Agustin, VIna Ahmad Nuruhidin Alwie, Rakhmat Ramdhani Ariansyah, Edward Armanjaya, Satria Audrey, Cresentia Bambang Pontjo Priosoeryanto Bella Rofi Desi Nadya Aulena Dhani, Muhammad Diva Dwi Putri Permatasari Esti Ambar Widyaningrum Esti Mumpuni Esti Mumpuni Esti Mumpuni, Esti Evi Kurniawati Evi Susanti Fadlu Rachman Fajar Ramadhan, Ziko Faridah Faridah Fitry Angger Pangestu Gayatri Indah Pramesti Gumay, Jovana Renaldy Hakim, Zainur Rahman Hutagaol, Lungguk Indriani, Aqilah Idelia Inggrid Tania Intan Permata Sari Julian Rahmat Lalu Sanik Wahyu Fadil Amrulloh Lidya Luziana Lilik Sulastri Lilik Sulastri LUNGGUK HUTAGAOL Lungguk Hutagaol Luziana, Lidya Maratu Soleha Marlien Bokko Martati, Titiek Maulida Mazaya Maulinda, Elvi Sahri Mawijaya, Agus Megawati - Muhamad Yamin Muhammad Yamin Muhammad Zulfadhli, Muhammad Mukh Fajar Nasrulloh Mulatsari, Esti Nabila Prihantini Khairunnisa Nana Nawasiah Natthawani, Amitta Novi Yantih Noviyantih, Noviyantih NURAINI HARMASTUTI Nuraini Harmastuti Nurmala Ahmar Nuruhidin, Ahmad Nurul Laily Fadhillah Panca Bayu Chandra, Pra Pratamaa, Yuga Rachman, Fadlu Rachmi Ridho Rafrini Amyulianthy Rahmat, Ayi Ramadhan, Islami Al-Kaffah Ramadhani, Karina Natasya Ramani, Sofyan Ratna Surya Alwi Raymond R. Tjandrawinata Renaldy Gumay, Jovana Reza Alrayan Rhahmadini, Yahdi Thia Rina Herowati Risna Rosmiyati Saeful Amin Saeful Amin Salsabila Adlina Saputra, Putri Windari Sarah Annisaa Nurwan Sari Dewi, Rika Sari, Felinda Sekar Harsti Rahmadhani Shaquille, Haikal Shirly Kumala Simanjuntak, Josua Donrio Simanjuntak, Vino Soaduon Siswahyudianto Siswandono, Siswandono Sodik, Alfan Nur Syamsudin Abdillah Syifa Aulia Taqwa, Iqbal Ananda Taurhesia, Shelly Utami, Santi Yanuarti Winana Kartika Dewi Wiwi Winarti Yogaswara, Amira Thufailla Zahra, Nurulita Az Ziko Fajar Ramadhan, Ziko Fajar