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Journal : Journal of Science Innovare

SYNTHESIS OF SCHIFF BASE VERDANTIOL BY SIMPLE CONDENSATION Niken Oktaviani; Leny Heliawati; Yudhie Suchyadi
Journal of Science Innovare Vol 2, No 2 (2019): Journal of Science Innovare, September 2019
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (109.144 KB) | DOI: 10.33751/jsi.v2i2.1533

Abstract

Schiff base is a chemical compound that is formed from the reaction between aldehydes and primary amines by condensation and produces by-products in the form of water. Schiff base is the raw material that is added in making Fragrance. The purpose of this study was to determine the method of synthesis of Schiff base verdantiol with simple condensation. The research method was carried out with four stages: preparation, synthesis, testing and measurement of parameters, and calculations. Preparation includes weighing the raw material Schiff base verdantiol. Schiff base synthesis is carried out by stirring at a temperature of about 90°C ± 5° C (Arctender, 1969) with a modification time of 15 minutes, 30 minutes, 1 hour, 2 hours and 3 hours. Testing and measurement parameters include organoleptic, density and specific gravity tests in pycnometer and compound confirmation using Gas Chromatography Mass Spectrometry. The results showed that the optimum synthesis of Schiff base verdantiol compounds was carried out at a heating time of 2 hours. The results of odor, color, density and gravity specifications heating time 2 hours according to specifications with the standard. GCMS confirmation results at 2 hours percent similarity are above 94%.
SYNTHESIS OF SCHIFF BASE VERDANTIOL BY SIMPLE CONDENSATION Niken Oktaviani; Leny Heliawati; Yudhie Suchyadi
Journal of Science Innovare Vol 2, No 2 (2019): Journal of Science Innovare, Volume 02 Number 02 2019
Publisher : Universitas Pakuan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33751/jsi.v2i2.1533

Abstract

Schiff base is a chemical compound that is formed from the reaction between aldehydes and primary amines by condensation and produces by-products in the form of water. Schiff base is the raw material that is added in making Fragrance. The purpose of this study was to determine the method of synthesis of Schiff base verdantiol with simple condensation. The research method was carried out with four stages: preparation, synthesis, testing and measurement of parameters, and calculations. Preparation includes weighing the raw material Schiff base verdantiol. Schiff base synthesis is carried out by stirring at a temperature of about 90°C ± 5° C (Arctender, 1969) with a modification time of 15 minutes, 30 minutes, 1 hour, 2 hours and 3 hours. Testing and measurement parameters include organoleptic, density and specific gravity tests in pycnometer and compound confirmation using Gas Chromatography Mass Spectrometry. The results showed that the optimum synthesis of Schiff base verdantiol compounds was carried out at a heating time of 2 hours. The results of odor, color, density and gravity specifications heating time 2 hours according to specifications with the standard. GCMS confirmation results at 2 hours percent similarity are above 94%.
Co-Authors Afiff, Sofia Muhammad Amalia Suryani Amani, Gita Salwa Nisrina Anis Khoerunisa Annisa Salsabila Billa, Salsa Budiana, Sandi Chairunisa Dadang Kurnia Dian Wulandari Dian Wulandari Dita Destiana Eka Suhardi Elly Sukamanasa Elly Sukmanasa Endah Tri Wahyuningsih Erinda Amalia Akmal Fenty Tiara Junika Fitri Anjaswuri Fitri Siti Sundari Ganeswara, M Ginanjar Haria Wiryangga Hidayat, Nada Syifa Hilda Sovia Marwah Indriani, Rini Sri Iskandar, Bunga Jaja Sudarjat Karmila, Nita Layung Paramesti Martha Leny Heliawati Lina Novita Martha , Layung Paramesti Mira Mirawati Mirawati, Mira muhajang, tatang N. Nurjanah Nadhifah, Tsaltsa Rizky Nadisa Dwi Gunawan Nanda Nurohmah Nasution, Yan Noviar Niken Oktaviani Nintin Nurlela Nurfauziyyah, Sifa Nurjanah . Nurjanah . Nurjanah Nurjanah Nurlinda Safitri Oding Sunardi Pertiwi, Ravhi Putri, Novi Nurlaela Rahma Alfiani Rany Nuraningsih Ratih Purnamasari Ratih Purnamasari, Ratih Ravhi Pertiwi Rita Istiana Roshella Sylviana Sulaeman Rukmini Handayani, Rukmini Safitri, Destriani Safitri, Nurlinda Safitri, Nurlinda Salma Khoerotu Syarifah Sandi Budiana Santa . Santa, Santa Setyaningsih, Sri Shafa Nabila Sulistio Putri Sheren Eriska Priscilia Listy Silvia Hamzari Siti Hanifah Awalliah, Siti Hanifah Awalliah Soewarto Hardhienata Soiman, Agus Sonnia Neng Bagus Sri Rini Indriyani Sri Setyaningsih Suci Setiarani Sucita Nurafrilian Sudarmin Sudarmin Suhendra Sumardi . Sumardi . Sumardi Sumardi Sunardi, Oding Suryani, Amalia Tatang Muhajang Tri Mahajani Tustiyana Windiyani Wahyuningsih, Endah Tri Wawan S. Anwar Wawan Syahiril Anwar Yuli Mulyawati Yulia Ambarsari Yusup, Muthia Khairunnisa P. Yusup, Muthia Khairunnisa Putri YUYUN ELIZABETH PATRAS, YUYUN ELIZABETH