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Journal : Science and Technology Indonesia

ZnAl LDH-based Derivative Materials as Photocatalysts: Synthesis, Characterization, and Catalytic Performance in Tetracycline Degradation Rohmatullaili; Ahmad, Nur; Erviana, Desti; Zultriana; Savira, Dila; Mohadi, Risfidian; Lesbani, Aldes
Science and Technology Indonesia Vol. 9 No. 2 (2024): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2024.9.2.457-469

Abstract

Layered Double Hydroxide (LDH)-derived materials exhibited different characteristics from LDH precursors. The conversion of ZnAl LDH into its derivative material has been carried out to find the best catalyst for TC degradation. ZnAl (LDH)-based catalysts in this study have been effectively synthesized using coprecipitation, calcination, and restacking procedures. ZnAl Layered Double Oxide (LDO) is derived from the calcination of ZnAl LDH at 500°C. ZnAl LDH was also modified by adding Garcinia mangostana pericarp extract (GME). XRD, FT-IR, UV-DRS, and SEM-EDX were used to investigate the synthesized catalyst. ZnAl LDH exhibited the typical LDH FT-IR spectra, whereas ZnAl LDO showed metal oxide-like spectra, and the ZnAl-GME composite displayed the combination spectra of precursor material. The ZnAl LDH XRD diffraction pattern exhibited the attributes of a layered material, whereas the other three catalysts did not. Calcination destroyed the layered structure of ZnAl LDH, whereas the addition of GME to LDH and LDO generated a single-layered composite. The modified ZnAl-GME composite showed a decrease in both particle size and bandgap energy. At an ideal pH of 5, the synthesized catalyst was used in a batch system photodegradation of 5 mg/L Tetracycline (TC), employing solar light irradiation. ZnAl LDO holds the most significant catalytic activity and structural stability through the fifth regeneration cycle, degraded TC up to 100% in 90 minutes.
Polyoxometalate-Assisted Layered Double Hydroxide for Facile Photocatalytic Methylene Blue and Malachite Green Hanifah, Yulizah; Ahmad, Nur
Science and Technology Indonesia Vol. 10 No. 4 (2025): October
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2025.10.4.1312-1321

Abstract

To increase the photodegradation activities of polyoxometalate, the co-precipitation approach has been used to prepare intercalated polyoxometalate compounds with ZnAl-LDH on methylene blue and malachite green dye. It is strongly advised to use the preparation catalyst LDH with polyoxometalate to create a successful method for anionic dye reduction. This study demonstrated the effectiveness environmentally method for intercalating ZnAl_LDH with polyoxometalate compound by employing methylene blu and malachite green dye as an organic pollutant. Additionally, the results showed that for pH = 7 for ZnAl- SiW12O40 on degraded malachite green, and the highest researching 94% on degradation methylene blue on ZnAl-PW12O40. Due to the rapid dissociation of the procion red reduction from the polyoxometalate photocatalytic activities, it was thought to have significant co-catalyst effects.
Co-Authors Adi Mansah Adiba, Thoriq Ahmad, Aunillah Ainy, Hanik Qurratul Aldes Lesbani Amri Amri Amri Amrullah, Jadnika Dwi Rakhmawan Anasom, Anasom Aprilia, Kartini Arsyad, Fitri Suryani Azizah, Nabilah Nur Didik Hermawan, Didik Dila, Anisa Ratna Dwi Yuliati, Yuli Erviana, Desti Fakhrurazi, Fakhrurazi Farhan Zulfikar, Ahmad Fathimah, Zuni Maulida Febriani, Eke Windiar Firdha Yusmar Fithrianto, Novan Fortuna, Teeusa Febby Fuadina, Zakiya Nur Hadi Kusuma, Hamdan Hanifah, Yulizah Hasja Paluta Utami, Hasja Paluta Hidayat, Aprilia Lulita Nadya I Ketut Mahardika Idha Royani Indrawati Indrawati Indrawati Jailani, Muhammad Taufiq Bin Mohd Jumaniar, Jamiatul Kholis, Moh. Nur Khumairoh, Nurista Yuliatul Kussudyarsana Kussudyarsana Laela, Rizka Amalia Mahbubah, Isna Nikmatul Mardiyanto Mardiyanto Marhestian, Sherin Marlan, Abd Rahman MIFTAKHUL JANNAH Mufid Andrianata Muliana, Siti Mulkan Habibi Muna, Fitria Nada, Rafa Nafis, Umi Zakiatun Negara, Satria Putra Jaya Niam, Muhammad Yusrun Nurcahyati, Ai Nurkhasanah Nurkhasanah Nusaibah Nusaibah Pertiwi, Salsabiela Pramudya Dwi Aristya Putra Pratama, Farandika Nanda Putri, Bunga Indah Putri, Dewi Ramandani Rahmadani, Vivi Rahmadhoni, Novita Kusuma Rahmani, Tara Puri Ducha Rhischa Assabet Shilla, Rhischa Assabet Ridlo, Zainur Rasyid Rini, Norma Puspa Risfidian Mohadi Rizkika, Maulidiya Rizky, Dyah Astiari Rofiq Faudy Akbar Rohmatullaili Rohmatullaili, Rohmatullaili Roikhan Mochamad Aziz, Roikhan Mochamad Rusdianto Rusdianto Rusdianto, Rusdianto Safitri, Erica Meilia Saputri, Ginanjar Zukhruf Sari, Devi Nur Indah Sari, Rika Sumita Wimanda Savira, Dila Sholahudin, M. Soedewo, Ery Sri Rejeki Dwi Astuti Sri Wahyuni Sugihartoko, Sugihartoko Suharsono, Judi Supeno Supeno Suroiyya, Serin Himatus Sutarto Sutarto Tiastutik, Fuji ULIN NUHA ULIN NUHA Ulin Nuha, Ulin Watson, Lee James Wibiyan, Sahrul Wibowo, Satrio Bayu Widayanto, Mutinda Wijaya, Alfan Yuniarti, Elmi Zultriana