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Journal : Science and Technology Indonesia

The Synthesis of CuO/Polystyrene Nanocomposite Superhydrophobic Layer using The Spin Coating Method Ratnawulan Ratnawulan; Ahmad Fauzi; Sarimai Sarimai
Science and Technology Indonesia Vol. 7 No. 2 (2022): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3067.897 KB) | DOI: 10.26554/sti.2022.7.2.158-163

Abstract

This paper shows the synthesis of CuO/Polystyrene(PS) nanocomposite superhydrophobic layer using the spin coating method. The objective of this study was to determine the effect of calcination temperature on the contact angle, morphology, and energy gap of the CuO/PS nanocomposite thin layer. Preparation of copper powder into copper oxide (CuO) nanoparticles using the method of High Energy 3 Dimensional Milling (HEM-3D) for 20 hours. The calcination temperature variations used were 100◦C , 150◦C, 180◦C, 200◦C, and 300◦C. In this study, sample analysis was performed using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), and Ultraviolet-Visible (UV-Vis) Spectrophotometry. The contact angle was determined using the sessile drop method. The findings indicate that the calcination temperature affects the contact angle of the nanocomposite thin films the highest contact angle was obtained at 162◦ at a temperature of 200◦C. The results of SEM analysis obtained that at a temperature of 200◦C, the particle size was 62.91 nm and the particles were evenly distributed in the composite layer. The energy gap at 200◦C is 2.03 eV. We found that CuO/PS synthesized at a temperature of 200◦C was superhydrophobic.
The Characterization of the Hydrophobic Surface of Nanocomposites Aloe vera/PS for Antimicrobial Pathogens Lathifa Zonesya Putri; Ratnawulan Ratnawulan; Ramli Ramli; Hamdi Rifai; Faridah Lisa Supian; Irna Humairah
Science and Technology Indonesia Vol. 8 No. 2 (2023): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2023.8.2.212-218

Abstract

The spread of pathogenic microorganisms on a large scale creates a health disaster for the world. Modifying the surface of the fabric so that it is antimicrobial pathogens with hydrophobic properties is one solution to inhibit the spread of microorganisms. Surface modification was carried out using Aloe vera powder as filler and polystyrene matrix with Aloe vera:PS composition variations of 1:5, 2:5, and 3:5 using the dip coating method and drying temperatures of 10◦C, 50◦C, and 90◦C. The characterization results that have been carried out with the best composition variations are 3:5 and 50◦C with a layered morphology using Scanning Electron Microscopy (SEM), resulting in a surface particle size of 21.243 nm, large contact angle/WCA using a Canon D350 camera with a size of 150.23◦, Fourier Transmission Infrared Analysis (FTIR) with the dominant functional group in the vibration band 2629 cm−1 indicates the presence of a long hydroxyl chain, the vibration band 1500 cm−1 with C-H stretching of the aromatic ring is caused by the characteristics of the polystyrene polymer and the wave number is 1700 cm−1 with stretching C=O which shows the characteristics of the carbonyl group in the Aloe vera sample is a flavonoid compound. The resistance of Aloe vera/PS solution to Klebsiella pneumonia resulted in a 20.18 mm diameter barrier showing strong resistance against bacteria and X-Ray Diffraction analysis showed that the AV powder was amorphous. Thus, the AV/PS 3:5 composition with a calcination temperature of 50◦C represents the greatest variation in the synthesis and characterization of hydrophobic thin films for pathogenic antimicrobial organisms.
Co-Authors - Hamdi AA Sudharmawan, AA Abdul Aziz Adilla, Rika Afrilla, Sonya Ahmad Fauzi Ahmad Fauzi aisyah fadillah Akmam Akmam Al Naim, A. F. Almunazar, Fauziyah Amelia Roza Haqu Amirullah, Fajar Fikri Anisa Janna Anisa Surya Annisa Kurniawati Aprianti, Rika Aria Ulfa Aris Alfikri Arni Sopianti Asri Devialita Asrizal - Betty Mizarwan Bizar al furqan Dafri Zaldi Dani Gustaman Syarif Delianis Pringgenis Desnita Desti Yuspita Sari Deswita, Pipi Devana Dhiya Purnama Sari, Salsabila Dian Septiana Dila Juliawati Djusmaini Djamas Doni, Rahma Dwi Putri Ramadhani Elvira Diana. S Emiliannur Emiliannur Ernita Susanti Ernmaniati Ramli Fadhila Ulfa Jhora Fadli M Fanny Rahmatina Rahim Faridah Lisa Supian Fatni Mufit Fauzi Ahmad Muda Fauziyah, Faadhilah Febriona, Fhica Febriya, Dhea Fitri, Hidayatul Forni, Francesca Fran Surya Andi Fuad Sofaturahman Gusnedi Gusnedi Gusnedi Gusnedi Gusnedi Gusnedi Gusnedi, - Gusriandi, Dedi Gustaman Syarif Gusti, Dian Arima Gustika Yonanda Hamdi Rifai Hardina, Yuli Harman Amir Hayyu Yumna Hidayat, Zaitul Hidayati Hidayati Hidayati Hidayati Hidayatul Lisma, Rahmi Hosman, N. J. Hufri Hufri I Made Arnawa Idam Arif Ilahi, Fitratul Intan Purnama Yani Ipal Ipal Irna Humairah Ismira, Ismira Izzati Salsabilla Madina Jasmine, Alifa Jhora, Fadhila Jhora, Fadhila Ulfa Kharisma Marta Judenta Korry Nilyani Lailatul Rahmi Lathifa Zonesya Putri Letmi Dwiridal Letmi Dwiridal Lia Rifka Septiana M. Bayu Ihsan Maharani Erika Putri Maharani, M Maritza Syalsabilla Masril Masril Mayasari, Tantri Mira Syuriyani Mohd Azmi, M. S. Muhammad Ridwan Azizi Mutiara Kusuma Febriwanti nabila aulia rahma Nadia Raisa Aryani Nadiyyah, Khoirotun Najmiatul Fajri Naspin, Desi Ariyanti Nessa Aqila Novella Febriana Nur Azizah Nurhabibah Nasution Nurhayati Nurhayati PAT, Anggi Angelina PAT Angelina Putri Dwi Sundari Putri, Sri Fany Mulya Rahima Syabrina Sarmi Rahmad Efendi Rahmat Hidayat Rahmat Hidayat Rahmat Hidayat Raisa, Nadia Ramadhani, Dinda Ramli Ramli Renol Afrizon Renold Fernanda Retna Junia Rifka, Lia Riri Camara Putri Riri Jonuarti Riri Jonuarti Riri Yandari Rita Iranie Riyasni, Selma rizka fauziah Rizki Fernanda Rosa Ayuni Utami Rosi Selfia Putri Santika, Viera Alvio Saputri, Ririn Hustia Sarimai Sarimai Sarmi, Rahima Syabrina Septia, Zahwa Silvi Yulia Sari Sinthia Dwi Jayanti Sisi Gusti Putri Sofaturrohman, Fuad Suherman, Dea Stivani Sumanti, Syahputri Supian, F. L. Syafri Syafri Syafriani Syafriani Syafriani Syafriani, - Syahputra , Ilham Syakbaniah Syakbaniah Syalsabilla, Maritza Syuriyani, Mira Tho, S. W. Triana Dwi Restika Trisia Meidini, Ella Ulfa Jhora, Fadhila Ulfa Jhora, Fadhilla Ulfa Jhora, Fadila Urwatil Wuskha Usmeldi Usmeldi Vauzia, Vauzia Veni Wahyuni Vonny Tinedi Wardatul Ullya Widiasih, Widiasih Witriani Marvinatur Ihsan Wong, Y. Y. Yanna, Fitri Yedho Syahadha Yenni Darvina Yola sri Wahyuni Yuliani, Kurnia Dwi Yulianti, Lastri Yuliza Noerman, Kiki Yulkifli Yulkifli Yurnetti Yurnetti Zaitul Hidayat Zakirman Zaturrahmi Zaturrahmi Zoni, Muhammad Ari Zulhendra Zulhendra Zulhendri Kamus