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Uji Aktivitas Antioksidan Ekstrak Daun dan Kulit Labu Air (Lagenaria siceraria (Molina) Standl.) Masrifah, Masrifah; Rahman, Nurdin; Abram, Paulus H.
Jurnal Akademika Kimia Vol 6, No 2 (2017)
Publisher : Universitas Tadulako

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The aim of the study was to determine the inhibitory concentration (IC50) of free radicals on an extract of calabash’s leaves and skins. The sample used in this study was the extract of calabash’s leaves and skins that made of 100 mg/L concentration. Determination inhibitory concentration of free radicals after adding DPPH (2,2-diphenyl-1-picrylhydrazyl) on the samples was determined using UV-Vis spectrophotometry. Concentration variations in leaves and skins extract of calabash used was 5, 10, 15 and 20 mg/L. The positive control used a vitamin C solution with a concentration that identical to the concentration of sample 5, 10, 15 and 20 mg/L. In the other hand, the negative control used a DPPH solution that was dissolved in ethanol p.a. The results showed that the leaves and skins extract of calabash with control of vitamin C have a concentration inhibition of free radicals (IC50) respectively was 9.268 mg/L (leaf extract), 9.332 mg/L (skin extract) and 6.839 mg/L (Vitamin C). The matter it was indicated that leaves and skins extract of calabash was a powerfully natural antioxidant.
Analisis Kadar Vitamin C Mangga Gadung (Mangifera sp) Dan Mangga Golek (Mangifera indica L) Berdasarkan Tingkat Kematangan Dengan Menggunakan Metode Iodimetri Rahman, Nurdin; Ofika, Mairet; Said, Irwan
Jurnal Akademika Kimia Vol 4, No 1 (2015)
Publisher : Universitas Tadulako

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Mango fruits contain several nutrients which are beneficial for the improvement of people’s nutrition. Vitamin C is one of which highly needed by the body and can be used as a source of antioxidants. Vitamin C level of mangoes is strongly influenced by their varieties, environments, places, fertilizers, maturity levels, and so on. Levels of vitamin C will increase until the fruit is ripe, and will decrease when the maturity level has been exceeded. This research determined the vitamin C level of gadung and golek mangoes based on the maturity levels. gadung and golek mangoes used as the samples were half-ripe, ripe, and overripe fruits. Analysis of vitamin C levels in the samples was done by iodimetry method. The results showed that the vitamin C levels of Gadung were 83.66 mg/100 g on the half-ripe fruits, 101.82 mg/100 g on the ripe fruits, and 92.85 mg/100 g on the overripe fruits. Whereas the vitamin c levels of golek were 57.72 mg/100 g on the half-ripe fruits, 79.30 mg/100 g on the ripe fruits, and 61,14 mg/100 g on the overripe fruits. The data indicate that the ripe fruits of mangoes contain the optimum level of vitamin C.
Meningkatkan Aktivitas Dan Hasil Belajar Siswa Pada Pembelajaran Kimia Penyetaraan Reaksi Redoks Melalui Lesson Study Di Kelas XII IPA SMA Negeri 2 Palu Chairunnisa, Chairunnisa; Supriadi, Supriadi; Rahman, Nurdin
Jurnal Akademika Kimia Vol 6, No 1 (2017)
Publisher : Universitas Tadulako

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The research about the balancing of redox reaction on chemistry subject has been done. This research was conducted on class XII IPA8 SMA Negeri 2 Palu with 28 of the student, in the first semester of the academic year 2014-2015. The research method used is a descriptive qualitative in which data processing use percentages and rating scale. The data is collected by observation sheets, questionnaires, and documentation. Implementation of lesson study on class XII IPA8 SMA Negeri 2 Palu is conducted in three meetings time (open class) with 3 phases; plan, do and see, respectively. Based on the results obtained every meeting by the researcher, the data activity of students is rising by 54.93, 59.86, and 74.30%. Furthermore, at the third meeting, the data obtained is an excellent category which means the student’s activity in the lesson study was increased. These prove that through the lesson study can increase the activity of the learning process of students. In addition, based on the data analysis of the student’s learning outcomes during three meeting times is increased. Average of completeness of student’s learning outcomes of every meeting is 67.85, 85.71, and 100%, respectively. Again, these prove that the student’s learning outcomes by classical can be increased through the lesson study.
KANDUNGAN MERKURI (Hg) DALAM AIR LAUT, SEDIMEN, DAN JARINGAN IKAN BELANAK (Liza melinoptera) DI PERAIRAN TELUK PALU Yusuf, Moh.; Hamzah, Baharuddin; Rahman, Nurdin
Jurnal Akademika Kimia Vol 2, No 3 (2013)
Publisher : Universitas Tadulako

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Mercury (Hg) is one type of a dangerous heavy metals. As one of contaminants, mercury enter the aquatic ecosystem through atmospheric decomposition or sourced from the industrial waste externalisation and bilogical and chemical converted in methyl mercury. This research aims to find out and determine the mercury concentrate which contained in sea water, sediment and belanak (Liza melinoptera) network in Palu bay water. The analysis of mercuri content on the tested sample using Automatic Mercury Analyzer. The working principle of the device is gold amalgamation method by heating and separation. The research result showed that the mercury content in belanak network is 0.143 - 0.188 ppm, sediment is 2.453 - 2.800 ppm and the sea water is 0.030 – 0.040 ppm. Based on the decision of the state minister of environmental regarding the guidelines for determination of Hg standard quality for sea water is 0.002 ppm and 0.001 ppm for marine biota. It shows that the Palu bay water condition has been polluted and the belanak is not worth to be consumed.
Pembuatan Etanol dari Buah Salak (Salacca zalacca) Melalui Proses Fermentasi Wartini, Ni Ketut; Abram, Paulus Hengky; Rahman, Nurdin
Jurnal Akademika Kimia Vol 6, No 4 (2017)
Publisher : Universitas Tadulako

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The study aimed to determine the level of ethanol that produced by the flesh of salak fruits with the fermentation process. The method used was an experimental method. The technical is fermentation, with tape yeast starter, determination of ethanol and purification. Ethanol level in the flesh of fresh fruits without handling was 11.3%, the highest levels of ethanol in the fruit flesh of 4 days after the plucking was 7.6%, and the fruit flesh of 7 days after the plucking was 3.4%. 
Efek Ekstrak Daun Alpukat (Persea americana Mill.) dalam Menurunkan Kadar Kolesterol Darah pada Mencit (Mus Musculus) Mufida, Mufida; Rahman, Nurdin; Supriadi, Supriadi
Jurnal Akademika Kimia Vol 7, No 1 (2018)
Publisher : Universitas Tadulako

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This study aimed to determine the effective concentration of avocado leaves extract in lowering cholesterol blood levels in mice (Mus musculus). The animals test were 15 male mice and were induced with propylthiouracil and high-fat dietary food. Mice were divided randomly into 5 groups with different treatments. Treatments I, II and III were given avocado leaves extracts each with a concentration of 10, 20, and 40%, respectively. Treatment IV was given simvastatin suspension as a positive control, and treatment V was given (Na-CMC) 1% as a negative control. Data were analyzed statistically with analysis of variance (ANOVA) test followed by Duncan test. The results showed that avocado leaves extract contained positively of alkaloids, flavonoids, saponins, tannins, and triterpenoid or steroids. Avocado leaves extract lowered cholesterol blood levels in mice with the most effective concentration was 10% (w/v).
Analisis Kadar Mineral Natrium dan Kalium Pada Daging Buah Nanas (Ananas comosus (L) Merr) di Kota Palu Sada, Nurjayanti Abdullah; Rahman, Nurdin; Supriadi, Supriadi
Jurnal Akademika Kimia Vol 3, No 2 (2014)
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Mineral is inorganic component which is in the human body. The needs of mineral for the body can be obtained by consuming fruits. Pineapple (Ananas comosus (L) Merr) is one of fruits contains mineral such as potassium (K) and sodium (Na). the objective of the research was to analysis the mineral level (Na and K) contained in pineapple flesh that spread out in Palu City. The analysis of Na and K mineral level used flame photometry analysis. The research result show that pineapple Cayenne varieties (common pineapple) contains sodium mineral as much 3.71 mg/kg and potassium as much at 376 mg/kg. The pineapple Queen varieties (Bogor pineapple) contains mineral sodium as much as 2.41 mg/kg and potassium as much as 198 mg/kg.
Uji Aktivitas Antioksidan Ekstrak Buah Kluwih (Artocarpus Communis) Arif, Mohammad; Rahman, Nurdin; Supriadi, Supriadi
Jurnal Akademika Kimia Vol 7, No 2 (2018)
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This study aimed to determine antioxidant activity of artocarpus camansi fruit extracts from Sigi, Central Sulawesi. This study was conducted by maceration extraction technique, and 2,2-diphenyl-1-picrylhydrazyl (DPPH) as the source of free radicals, and vitamin C as a positive control. UV-Vis spectrophotometer was used for measuring the absorbance of artocarpus camansi fruit extracts. artocarpus camansi fruit powder was extracted by maceration using ethanol. Various concentrations of artocarpus camansi fruit extracts used were 20, 40, 60, and 80 mg/L. The results showed that the IC50 value for artocarpus camansi (artocarpus communis) fruit extract was 88.715 mg/L, whereas the IC50 value for vitamin C was 37.153 mg/L. Artocarpus camansi (artocarpus communis) fruit extracts are powerful antioxidants category based on IC50 value. The optimum percentage antioxidant activity of artocarpus camansi fruit extracts to inhibit free radical amounted to by 50.65%
Uji Aktivitas Antioksidan Ekstrak Buah Semangka (Citrullus lanatus) Mariani, Sri; Rahman, Nurdin; Supriadi, Supriadi
Jurnal Akademika Kimia Vol 7, No 2 (2018)
Publisher : Universitas Tadulako

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The aim of this study is determine the IC50 extracts values of white peel and flesh of red watermelon, white peel and flesh of yellow watermelon as antioxidants. To determine antioxidant activities DPPH reagent was used as well as UV-Vis Spectrophotometry was used to measure vitamin C as a positive control measurement. The samples mixed with ethanol in various concentration of 5, 15, 25 and 35 mg/L. The results showed that the IC50 values for each extract of red watermelon flesh, yellow watermelon flesh, white peel of red watermelon, and white peel of yellow watermelon were 16.619 mg/L, 16.575 mg/L, 14.729 mg/L, and 16.782 mg/L, respectively. Vitamin C as the positive control has IC50 value of 9.526 mg/L. These IC50 values showed that vitamin C had higher antioxidant activity than watermelon extracts, but the extracts of watermelon still categorized in strong natural antioxidants. This study concluded that watermelon is good to be consumed because it is a very strong antioxidant.
ANALISIS LOGAM TEMBAGA (Cu) PADA BUANGAN LIMBAH TROMOL (TAILING) PERTAMBANGAN POBOYA Nuriadi, Nuriadi; Napitupulu, Mery; Rahman, Nurdin
Jurnal Akademika Kimia Vol 2, No 2 (2013)
Publisher : Universitas Tadulako

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Abstract

The analyses of Copper (Cu) has been performed in the sample of drum waste (tailings) gold mining in Poboya by using Atomic Absorption Spectrophotometry (AAS) method.The alkaline destruction by the addition of HNO3 and HClO4 has been done by heating then distilled. The absorbance was measured at a wavelength (λ) = 324.7 nm on copper metal analysis. From the analysis,it was obtained copper metal in each drum consist of as follows drum A. 204.92 mg/kg, drum B 151.85 mg/kg, drum C 79.51 mg/kg, drum D 167.78 mg/kg, drum E 190.68 mg/kg, with the overall average value of 158.94 mg/kg. The data shown that the area gold mining at Poboya contain copper metal ion in high quantity.
Co-Authors A Fahira Nur A, Madinah Abd Rahman Abd. Rahman Abram, Paulus H. Achmad, Rahim Adhar Arifuddin Afni, Nur' Agustin Tiwow Ahmad Yani ahmad yani Aldiza Intan Randani Amyadin, Amyadin Anang Wahid M.Diah Andi Mascunra Ami Andi Saifah Andriani Andriani Ariani Ariani Ariani Ariani Ariani Ariani Ariani Arie Wibowo Arie Wibowo Asmawati Asmawati Aulia Rakhman Aulia Rakhman Baharuddin Hamzah Bahriul, Putrawan Bohari Bohari Bohari Bohari Chaeriah, Siti Chairunnisa Chairunnisa Darmayanti Darmayanti Daud Karel Walanda Devi Nadila Diah Ayu Hartini Fadjriah, Rasyika Nurul Fajaryanti, Desi Eka Fajriah, Rasyika Nurul Fatma Hamid, Fatma Fendi Pradana Fitra Armawaty, Fitra Frini, Merlinda Gusman Arsyad Hasanah Hasanah Hayati Hayati Herman Herman Herman Herman Herman Hermiyanti Hermiyanti, Hermiyanti Hermiyanty Hermiyanty Hermiyanty Hermiyanty, Hermiyanty Hijra Hijra I Made Tangkas Imelda Imelda Indriany, Indriany Irawati, Dwi Ardi Irwan Irwan Laba, Stefiani Bengan Laida, Marsia Lilis Fauziah, Lilis Linda Ayu Rizka Putri Madinah A Mahfudz Mangundap, Selvi A Mardia Hi Rahman, Mardia Hi Marsia Laida Masrifah, Masrifah Ma’rifat Ma’rifat Mercy Joice Kaparang Mery Napitupulu Meylan Ratnawati Miftahul Haerati Sulaiman Minarni Rama Jura Moh. Yusuf, Moh. Mohammad Arif Mufida, Mufida Muhammad Agus Muljanto Muhammad Nur Ali Muhammad Ryman Napirah Muhammad Ryman Napirah Muhammad, Nurlaela Munir, Muh Ardi Munir, Muhammad Ardi Ni Luh Cicik Fitriani Nikmah Utami Dewi Ningrum, Arum Sekar Nur Ali, Muhammad Nur, Makmur Jaya Nurfadilah Nurfadilah Nurhanifah Muthmainnah Nurdin Nuriadi, Nuriadi NURLIANA NURLIANA Nurulfuadi Nurulfuadi Ofika, Mairet Oksandi Oksandi Pangaribuan, Helena Parmin - Paulus Hengky Abram Pitriya, Ida Ayu Putri, Eska Perdanawati Kahar Radiansah, Roy Ramlan Ratman Ratman Ratman Ratman Resti Agustia Riska Safitri, Riska Rosa Dwi Wahyuni Rosdia Rosdia Rosmala Nur Sada, Nurjayanti Abdullah Salsabila, Unik Hanifah Saprudin Saprudin, Saprudin Siang Tandi Gonggo Siang Tandi Gonggo Siti Ika Fitrasyah Siti Nuryanti Sri Mariani Sri Mulyani Sabang Sri Nurbaeti Stefiani Bengan Laba Sudirman Sudirman Sulaeha, Siti Sulaiman, Miftahul Haerati Sumarni Sahjat, Sumarni Sunarto, Sunarto Supirno, Supirno Suriati Suryaningsih Suryaningsih Tri Setyawati Try Nur Ekawati Lukman Tutri Aprilia Mellyni Ummu Aiman Veruswati, Meita Vidyanto, Vidyanto Vina Febriyani Vivi Putri Damayanti Wardatul Jannah, Wardatul Wartini, Ni Ketut Yulfiana Yulfiana Yulfiana, Yulfiana Yulfiana, Yulfiana Yundari, Yundari Yusdin Gagaramusu Zulaikha, Nurratri Zulaikha, Nurratri Zulviana, Eva