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NURUL FAIZAH
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Journal : International Journal of Renewable Energy Development

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Optimization of ultrasonication time on the production of ZnO-SiO2 nanocomposite as photocatalytic material Qomariyah, Lailatul; Faizah, Nurul; Karisma, Achmad Dwitama; Rabbani, Sulthan; Kalloka, Sultan Hendra Mahardi; Putra, Nicky Rahmana
International Journal of Renewable Energy Development Vol 14, No 5 (2025): September 2025
Publisher : Center of Biomass & Renewable Energy (CBIORE)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.61435/ijred.2025.61248

Abstract

Nanocomposite ZnO-SiO2 is widely known for its efficacy as a semiconductor photocatalyst. Current nanocomposite production methods face challenges like particle agglomeration and inconsistent particle size control. To overcome this problem, the ultrasonication method was used to prevent agglomeration and produce composites in nanoscale, where this study synthesized ZnO-SiO2 for photocatalytic degradation of dye color. To prepare this nanocomposite, the ultrasonication time was varied from 0 to 45 minutes to understand the particle properties and the effectivity on the photocatalytic activity. Silica was prepared from water glass via sol-gel method to produce colloidal SiO2 nanoparticles and then mixed with ZnO with the ratio of 3% wt and subjected to ultrasonication method. Under various ultrasonication time, the FTIR analysis shows the Si-O peak at 895 cm-1 indicates the presence of SiO2 particles. The XRD validate the formation of ZnO-SiO2 nanoparticles, supporting the FTIR analysis. The best nanoparticle properties were achieved with 45 minutes of ultrasonication. The SEM analysis confirms the present of SiO2 and ZnO. From BET analysis, ZnO-SiO2 has a high surface area (117.64 m2/g), moderate pore volume (0.46 cm3/g), and small particle pore size (11.59 nm). The photocatalytic activity of ZnO-SiO₂ nanocomposites was evaluated by the degradation of methylene blue (MB) under sunlight and the best performance reached by the nanocomposite prepared under 45 minutes ultrasonication. The results show that the ultrasonication technique efficiently reduces agglomeration, as indicated by a reduction in particle diameter from 35.04 nm (pure ZnO) to 11.59 nm (ZnO-SiO₂), and significantly enhances photocatalytic activity, achieving 97% degradation of MB under sunlight after 180 minutes. The aforementioned technique demonstrates significant potential for industrial use, providing higher efficiency and expandability in manufacturing superior photocatalytic substances.
Co-Authors 'Alam, Ghasa Faraasyatul ., Abbas A. Mustika Abidin Abror Achmad Dwitama Karisma Adha, Munirah Fatimah Agustina, Melinda Ahmad Nashir Ahmad Zuhdi Ahmad Zuhdi Andari, Fadhilah Nur Antari, Gladeva Yugi Ardiana Aribaat, Salma Khoirotunnisa Arifin, Rizal Arin Ika Puspitaningsih Armenia, Ivan Gustra Manca Aulia, Anisa Fatma Aulia, Kunni Rofiqotul Ayu , Sadriana AYU LESTARI Badriyah, Nur Lailatul Badrud Tamam BAMBANG SURATMAN Basuki, Edi Pujo Br.Tarigan, Dinda Florentina Rania Burhanuddin Burhanuddin Cahyani , Anggun Cita Diah Ratna Widiarti Eti Setiawati, Eti Fairuzia Khaidaroh, Hilda faizah, Nurl Faradila, Nindy Faridah, Mutiah Fatahillah, Fatahillah Febriani, Putri Indah Febriyani, Rani Diah Febry Kodoatie, Maria Stela Firdiansyah, Firdiansyah Fitri Andriani Fatimah Fitri, Wahyu Nurul Fitria Wahyuni Fuadi, Rifki Hardianti, Laily Harun Al-Rasyid Hasna, Oktavia Hikmah, Harisna I Ketut Suatha I Wayan Batan Indrawadi, Junaidi Irawan , Hisba Cahyani Isa Anshori Ismah, Nurul Ismiati Joang Ipmawati Kalloka, Sultan Hendra Mahardi Kaloka, Ardista Izdhihar Kartini Kartini Kartini, Dyan Nurwita Khasanah, Indayati Kirana, Khalida - Lailatul Qomariyah, Lailatul Lasiama, Nabila Lestari, Ida Puji Listiana Hidayati M. Imamuddin M. Yusuf Amin Nugroho Maria Montessori Maulida, Aisyah Putri Mernawati, Mernawati Moch Sasmito Djati MOCHAMMAD YASIR Mohamad, Nursa'adat Afifah binti Muali, Chusnul Muammar, Amri Mufsiroh, Istijabah Ifti Muhammad Alfian Muhammad Nurul Hasanudin Mukhlisa, Dian Murtadlo Murtadlo Mustofa Mustofa Ngulum, Mochamad Bahrul Noprianti, Yuni Noviyanti Watman, Ika Nugroho, Muhammad Yusuf Amin Nur Aisyah Nurul Hidayat Pramesti, Novita Ayu Pratiwi , Ika Ari Prayadi, Icha Nur Putra, Muhammad Benaldo Anugrah Putra, Nicky Rahmana Qomaria, Nur Rabbani, Sulthan Raden Bambang Sumarsono Rafika Rahman, K.A Rahmat Aryandi Ramlah Ratna Yunita Retnoningrum, Sri Murti Rivani, Sinta romdhoni, muhammad wildan S. Latinapa, Moh. Hidayat Şaban, Ömer Safutri, Lhutfia Wahyu Saijun, Saijun Saputri, Nadia Elga Saputro, Rafly Restu Dwi Setiyadi, Bradley Setyaningrum, Eka Wahyu Shabrina, Amalina Shafina, Shafina Siti Ummi Masruroh Slamet Suyanto Sri Aju Indrowaty Suryanef Suryanef Syamsiarna Nappu, Syamsiarna Syukur, Muhammad Adnan Thufailah, Gladys Sukma Tsaqifah, Ainun Wati, Ni’mah Wawan Shokib Rondli Widayanti, Agnisa Wifaq Kholidiyah, Ananda Wijaya, Nur Widad Wiwin Puspita Hadi Wulandari, Elis Dwi Yahya Nur Ifriza Yenita Roza Yhustien, Dhea Yogananda, Amrina Amalia Yulianti, Selvia Zakiyyah, Rifqatun Zulfatun Ruscitasari Zulkipli Lessy