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All Journal Journal of Agromedicine and Medical Sciences Window of Health : Jurnal Kesehatan JOPS (Journal Of Pharmacy and Science) Journal Syifa Sciences and Clinical Research (JSSCR) AMALIAH: JURNAL PENGABDIAN KEPADA MASYARAKAT Jurnal Dunia Farmasi Jurnal Ilmiah Manusia dan Kesehatan ad-Dawaa : Journal of Pharmaceutical Sciences Indonesian Journal of Pharmaceutical and Clinical Research Jurnal Aisyah : Jurnal Ilmu Kesehatan Community Development Journal: Jurnal Pengabdian Masyarakat Journal of Pharmaceutical and Health Research International Journal Of Science, Technology & Management (IJSTM) Indonesian Journal of Chemical Science and Technology Jurnal Kesehatan Tambusai JUKESHUM: Jurnal Pengabdian Masyarakat Jurnal EduHealth FORTE JOURNAL Jurnal Altifani Penelitian dan Pengabdian kepada Masyarakat Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan Jurnal Sains dan Teknologi International Journal of Health and Pharmaceutical (IJHP) SENTRI: Jurnal Riset Ilmiah Sciences of Pharmacy FARMASAINKES PCJN Pharmaceutical and Clinical Journal of Nusantara Herbal Medicine Journal Journal of Pharmaceutical and Sciences. Media Farmasi Indonesian Journal of Science and Pharmacy Jurnal Bakti Nusantara Jurnal Akademika Kimia Jurnal Sains dan Kesehatan
Zulmai Rani
Universitas Muslim Nusantara Al-Washliyah, Medan, Indonesia
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Journal : Media Farmasi

 1 
Isolasi Dan Identifikasi Kitosan Dari Cangkang Kerang Bulu (Anadara antiquata) Dewi Rizki; Ridwanto; Zulmai Rani
Media Farmasi Vol 19 No 2 (2023): Media Farmasi
Publisher : Jurusan Farmasi Poltekkes kemenkes Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32382/mf.v19i2.174

Abstract

Chitosan is a polysaccharide formed via deacetylation of chitin. In general, chitosan is made from waste products from the fishing industry, such as shrimp, crabs, shells of feather clams, snails, and so on. The chitosan comes from the head, skin, and carapace. The development of chitosan applications has great potential because the production of shrimp, crab, and feather clam shells continues to increase. Chitosan is a bioactive substance with use in the fishing industry. This research aims to isolate and characterize chitosan from feather clam shells (Anadara antiquata) to convert feather clam shells into chitin and deacetylate it into chitosan then to determine the functional groups and characteristics of chitosan using Fourier infrared (FTIR). The isolation methods used were deproteination using 4% NaOH solvent, demineralization with a 1:5 ratio of 2N HCl solvent, depigmentation with a 1:10 ratio of 4% NaOCl solvent and deacetylation with a 1:20 ratio of 50% NaOH solvent. and chitosan characterization. According to the study's findings, the degree of deacetylation obtained in the form of a white powder was 75%, odorless fine powder. Chitosan dissolves in acetic acid, according to the solubility test. The obtained water content was 3.81% and the ash content obtained was 0.7%. Feather clam shell waste is declared to be well isolated and meets the requirements by SNI with a degree of deacetylation value of 75%. Kitosan merupakan polisakarida dari deasetilasi kitin; biasanya dibuat dari limbah produk industri perikanan seperti bekicot, kepiting, udang, bulu kerang, dan cangkang kerang. Kitosan berasal dari kulit, karapas, dan bagian kepala. Karena produksi udang, kepiting, dan cangkang kerang bulu yang terus meningkat, pengembangan aplikasi kitosan sangat potensial. Kitosan merupakan bahan bioaktif memiliki manfaat untuk industri perikanan. Tujuan studi ini adalah untuk mengidentifikasi, menggambarkan kitosan yang ditemukan dalam cangkang kerang bulu (Anadara antiquata) agar merubah cangkang kerang bulu menjadi kitin dan di deasetilasi menjadi kitosan kemudian untuk mengetahui gugus fungsi dan karakteristik kitosan menggunakan fourier infrared (FTIR). Metode isolasi yang dilakukan yaitu  deproteinasi menggunakan pelarut NaOH 4%, demineralisasi menggunakan pelarut HCl 2N dengan perbandingan 1:5, depigmentasi menggunakan pelarut NaOCl 4% (1:10), deasetilasi dengan pelarut NaOH 50% (1:20) dan karakterisasi kitosan. Hasil penelitian menunjukkan derajat deasetilasi yang di peroleh yaitu 75% berbentuk serbuk halus berwarna putih dan  tidak berbau. Menurut uji kelarutan, kitosan larut dalam asam asetat. Kadar air yang diperoleh 3,81% dan kadar abu yang diperoleh 0,7%. Limbah cangkang kerang bulu dinyatakan terisolasi dengan baik dan telah memenuhi syarat sesuai dengan SNI dengan nilai derajat deasetilasi sebesar 75%.
Isolasi Dan Identifikasi Kitosan Dari Cangkang Kerang Bulu (Anadara antiquata) Rizki, Dewi; Ridwanto; Rani, Zulmai
Media Farmasi Vol 19 No 2 (2023): Media Farmasi Edisi Oktober 2023
Publisher : Jurusan Farmasi Poltekkes kemenkes Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32382/mf.v19i2.174

Abstract

Chitosan is a polysaccharide formed via deacetylation of chitin. In general, chitosan is made from waste products from the fishing industry, such as shrimp, crabs, shells of feather clams, snails, and so on. The chitosan comes from the head, skin, and carapace. The development of chitosan applications has great potential because the production of shrimp, crab, and feather clam shells continues to increase. Chitosan is a bioactive substance with use in the fishing industry. This research aims to isolate and characterize chitosan from feather clam shells (Anadara antiquata) to convert feather clam shells into chitin and deacetylate it into chitosan then to determine the functional groups and characteristics of chitosan using Fourier infrared (FTIR). The isolation methods used were deproteination using 4% NaOH solvent, demineralization with a 1:5 ratio of 2N HCl solvent, depigmentation with a 1:10 ratio of 4% NaOCl solvent and deacetylation with a 1:20 ratio of 50% NaOH solvent. and chitosan characterization. According to the study's findings, the degree of deacetylation obtained in the form of a white powder was 75%, odorless fine powder. Chitosan dissolves in acetic acid, according to the solubility test. The obtained water content was 3.81% and the ash content obtained was 0.7%. Feather clam shell waste is declared to be well isolated and meets the requirements by SNI with a degree of deacetylation value of 75%. Kitosan merupakan polisakarida dari deasetilasi kitin; biasanya dibuat dari limbah produk industri perikanan seperti bekicot, kepiting, udang, bulu kerang, dan cangkang kerang. Kitosan berasal dari kulit, karapas, dan bagian kepala. Karena produksi udang, kepiting, dan cangkang kerang bulu yang terus meningkat, pengembangan aplikasi kitosan sangat potensial. Kitosan merupakan bahan bioaktif memiliki manfaat untuk industri perikanan. Tujuan studi ini adalah untuk mengidentifikasi, menggambarkan kitosan yang ditemukan dalam cangkang kerang bulu (Anadara antiquata) agar merubah cangkang kerang bulu menjadi kitin dan di deasetilasi menjadi kitosan kemudian untuk mengetahui gugus fungsi dan karakteristik kitosan menggunakan fourier infrared (FTIR). Metode isolasi yang dilakukan yaitu  deproteinasi menggunakan pelarut NaOH 4%, demineralisasi menggunakan pelarut HCl 2N dengan perbandingan 1:5, depigmentasi menggunakan pelarut NaOCl 4% (1:10), deasetilasi dengan pelarut NaOH 50% (1:20) dan karakterisasi kitosan. Hasil penelitian menunjukkan derajat deasetilasi yang di peroleh yaitu 75% berbentuk serbuk halus berwarna putih dan  tidak berbau. Menurut uji kelarutan, kitosan larut dalam asam asetat. Kadar air yang diperoleh 3,81% dan kadar abu yang diperoleh 0,7%. Limbah cangkang kerang bulu dinyatakan terisolasi dengan baik dan telah memenuhi syarat sesuai dengan SNI dengan nilai derajat deasetilasi sebesar 75%.
Co-Authors A'dilah, Nur Abadi, Hafizhatul Adjelie, Tiara Adli Nuzula Rahmah Adyani Maulinda Afriati, Nelsi Afridah, Nurul Ilmi Ahmad Rasyid Ridho Alviana, Liya Amelia Kudadiri Andi Syahputra, Ricky Andjelie, Tiara Ani Sutiani Ani Sutiani Anny Sartika Daulay Anny Sartika Daulay Anny Sartika Daulay Aprilia, Hijjatun Arifin, Khairil Fikri Arrosty, Muflizah Athaillah, Athaillah Audry Pratiwi Aulia Fitri Aulia Fitri, Aulia Auza , Maharani Azhar, Gustika Bambang Hermanto Bambang Hermanto Beby Noplya Wulandari BJ Sutrisna Chandra, Putra Dama Yanti, Fradilla Daulay, Anny S. Dea Anggreini Denny Satria Dewi, Sri Harti Dikki Miswanda Dinda Sari Utami Dwi Jati, Fatma Emma Susanti Erma Susanti Evi Depiana Gultom Evi Depiana Gultom Fadhlah Al-Uyun Nasution Fahmi Fahmi Fajri, Fajrilda Aqilah Fauziah Erna Witular Panggabean Ferendina, Imelda Fithri Pulungan, Ainil Fitri, Nurul Fitri, Raissa Gabena Indrayani Dalimunthe Ginting, Grace Anastasia br Ginting, Ovalina Sylvia Br Ginting, Ovalina Sylvia Br. Gultom, Evi Depiana Hanafis Sastra Winata Harahap, Sumiyarni Haris Munandar Nasution Hariyadi Dharmawan Syahputra Hariyadi Dharmawan Syahputra Hariyadi Dharmawan Syahputra Hasibuan , Fika Miah Sasmitha Hasibuan , Nabila Hasim Hasibuan, Zulfiana Ramadhani Hindri Syahputri Humaira, Annisa Husna, Miftahul Hutagalung, Victor H Indrayani, Gabena Inna Myesha Julia Reveny Karo Sekali, Elva Swandi Kasta Gurning Khairunnisa , Ardina Khan, Sahrani Nazwa Kiki Rawitri Kiki Rawitri Lestari, Amanda Putri Lestari, Kurnia Dwi Lilik Septiana Lilik Septiana Linda, Rosa Lubis, Asira Lubis, Minda Sari lubis, muhammad fauzan Lubis, Nurazizah M. Alfaruqi Maghfirah, Dini Mainal Furqan Malahayati Malahayati Maryanti Yuza Matondang , Fikriyah Hafni Maulana Putri, Yasinta Mira Febrina, Mira Monica Suryani Moondra Zubir Muhammad Agus Muljanto Muhammad Amin Nasution Muhammad Fauzan Lubis Muhammad Yunus Muhammad Yunus Mukti, Ridho Munandar, Verissa Nadila Indra Sepvina Nasri Nasri Nasri Nasri Nasri Nasri, Nasri Nasution, Wardah Nazuhra, Oca Nia Novranda Pertiwi Nindya Indah Damayanti Ningtias, Anggita Ningtias, Anggitha Nomi Noviani Nur Ain Thomas Nur, Hijrotun Nurdalilah, Nurdalilah Nurhayati Nurhayati Nurmazela, Virda Nursyafira, Arini Ovalina Sylvia Br. Ginting Ovalina Sylvia Br. Ginting Ovalina Sylvia Br. Ginting Paramitha, Ratih Parapat , Anjarlit Romiyuliana Br Pasar Maulim Silitonga Pertiwi, Rahma Pitaloka, Syifa Amilia Puteri, Cut Intan Annisa Putra, Andhika Dharma Putri Khairani Rahma Dona, Rahma Raissa Fitri Rambe, Robiatun Rawitri, Kiki Reza Irma Ricky Andi Syahputra Ridho, Ahmad Rasyid Ridwanto Ridwanto Ridwanto Rinda Sari, Syilvi Rinda Sari, Sylvi Ritonga , Nur Sakina Rizki, Dewi Rizki, Vitri Dea Robiatun Rambe Robiatun, Robiatun Rambe Rukmana, Siti Sagala, Hasel Untung Bersinar Samran, Samran Sari Lubis, Winda Sari, Farida Sari, Syilvi Rinda Sari, Sylvi Rinda Sartika Daulay, Anny Savitri, Novia Herma Septiana, Lilik silalahi, zahra salsabila Sindi, Sindi Sipahutar, Rizki Anjani Siregar , Misbah Siti Anisa Siti Rahmah Siti Rahmi Ningrum Sony , Suyefri Sri Wahyuni Sri Wahyuni Suci, Nurul Sulwiyatul K Sani Supiyani, Supiyani SURBAKTI, CHRISTICA ILSANNA Syafa Nadira Ashiilah Syahputra, Ricky Andi Syarifah Nadia Syilfia Hasti Tania, Chyntia Glori Tarigan, Eni Surabini Trizaldi, Asep Urip Harahap Uswatun Nisa, Uswatun Vera Estefania Kaban Widya, Rizka Yayuk Putri Rahayu Yayuk Putri Rahayu Yuli Haryani Yuliatil Adawiyah Harahap Yuniarti , Rafita Yuniarti, Rafita Zahira Ahmad, Madani Ziza Putri Aisyia Fauzi Zulfikri Zulfikri Zulhij, Fizrya