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Journal : ASEAN Journal of Chemical Engineering

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Optimization of Lithium Separation from NCA Leachate Solution: Investigating the Impact of Feed Concentration, Pressure, and Complexing Agent Concentration Mustika, Pra Cipta Buana Wahyu; Suryanaga, Edward Chandra; Perdana, Indra; Sutijan, Sutijan; Astuti, Widi; Petrus, Himawan Tri Bayu Murti; Prasetya, Agus
ASEAN Journal of Chemical Engineering Vol 23, No 3 (2023)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ajche.83096

Abstract

Recycling lithium batteries (LIB) has emerged as an attractive solution in the global pursuit of environmentally friendly practices. The aim of achieving zero–waste hydrometallurgical technology is within reach. This research focuses on utilizing the low-pressure nanofiltration process to address this challenge by separating lithium ions from other ions and achieving a desirable permeate flux. The NCA battery leachate concentrate was obtained through a hydrometallurgical process involving sulfuric acid–peroxide. To ensure the prevention of potential nanofiltration membrane (TS80) fouling, the concentrate is initially filtered using an ultrafiltration membrane (UH004) to remove any particles. The research investigates the impact of pressure (4, 6, and 7 bar), solution concentration (concentrate, 10x, and 50x dilution), and the concentration of the complexing agent (EDTA) on the desired separation performance. The investigation reveals that pressure variations exhibit consistent rejection rates, remaining stable above 80%. A similar trend is observed with the addition of EDTA, which consistently yields rejection rates above 80%. However, when examining different feed concentrations, the rejection of lithium falls below 80% for leachate concentrates. In summary, satisfactory results are obtained by employing nanofiltration with a TS80 membrane at a pressure of 7 bar, a dilution factor of 10x, and using a 0.02M EDTA complexing agent. Meanwhile, it was found that the separation factors (Li⁺/Ni²⁺ = ~8.6, Li⁺/ Co²⁺ = ~7.3, Li⁺/Al³⁺ = ~4.9) and permeate flux ±46.58 L m⁻² h⁻¹. The findings demonstrate good selectivity along with relatively high flux.
Co-Authors Afdalia, Tiara Agus Prasetya Agus Syahrani Andi Fitriani Djollong Angrum, Alna Triskaya Aprilianto, Doni Riski Aqmarin, Ifni Arifin, Ardian Asfar, Dedy Ari Azmi, Chairanda Al Bernadetha Nadeak Bina, Risa Masdania Kartika Cakranegara, Pandu Adi Chandra Wahyu Purnomo Dany Try Hutama Hutabarat Darnita, Darnita Debora Demitra Devi, Kharisma Diman, Paul Dwisetyo, Vici Erisyerico, Mimo Lalito Fadillah, Farika Asna Fajar Fajar Gazali Salim Hary Sulistyo Hasanah, Nunur Hasby, Nazar Hery Widijanto Himawan Tri Bayu Murti Petrus Hinode, Hirofumi Holten Sion, Holten Ilham Ilham Ilham Ilham Islamiah, Neneng Iswandi, Rizky Joni Bungai, Joni Juwita, Nadilla Rahma Kaharap, Mongga Karani, Elannari Karani, Elanneri Kathryn, Morse Kinanti, Divita Hayyu Kristanoval, Kristanoval Kriswantara, Glory Lazarus Linarto Linarto, Lazarus Linggua Sanjaya Usop Lubis, Lili Kahirina Azhari Lubis, Rafly Aulia Manurung, Mangaraja Marhaban, Saiful Maria Arina Luardini Maria Arina Luardini Mas'ud Muhammadiah Maulina, Evaf Misrita Misrita, Misrita Muh. Wahyu Syabani Mustika, Pra Cipta Buana Wahyu Nadila, Indriani Najmiah, Lailatun Nasution, Adenisya Natalina Asi, Natalina Natasya Nita, Lisa Afria Noviasi Nur Muttaqien Zuhri Nurhasanah Nurhasanah Nurwidyaningrum, Kristanti Nuryoto Oscar, Scherschligt Panut Mulyono Pasaribu, Liza Umami Pattiasina, Petrus Jacob Paulina, Novely Esterika Petrus Jacob Pattiasina Petrus Poerwadi Pradnya Paramitha, Putu Elvira Pratiwi, Irda purwaka, albertus Putri, Julia Rahma Putri, Nelliza Rahman, Muhammad Irfan Rahmat Winata Ramadani, Fitra Ratna Pancawati Ristati, Ristati Rizaldi, Muhammad Rochmadi Rumondang, Rumondang Salam, Agus Sanjaya Usop, Linggua Sari, M. Alpian Sasmithae, Lia Sedyatama, Deska Anggrait Silalahi, Juniar Tiurma Uli Silvianti, Annisa Sinuraya, Jusak Kencana Siregar, Fazriana Siti Arnisyah Siti Nurul Aisyiyah Jenie, Siti Nurul Aisyiyah Sitompul, Theresia Friska Damayanti Sitorus, Akmal Satria Alfin Sitorus, Muhammad Aldi Prayuda Slamet Sumardi, Slamet Sriwahyuni, Riza Sujoto, Vincent Sutresno Hadi Supriyadi Supriyadi Suryanaga, Edward Chandra Sutijan Syahrunsyah, Syahrunsyah Syapiq, Mirza Theasy, Yoan Thesaloga, Rino Tri Susilowati Umar, Vebrianti Vandan Wiliyanti Veniaty, Syarah Verawati Verawati Wahyu Imam Santoso Wahyudi Budi Sediawan Wardani Dwi Wihastyanang, Wardani Dwi Warmita, Helena Karunia Weliyadi, Encik Widi Astuti Wijaya, Chandra Ridho Wildan Habibi Yupita, Yupita Zuwandana, Ahmad