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All Journal IAES International Journal of Artificial Intelligence (IJ-AI) VALENSI JURNAL ILMU SOSIAL Agrikultura Jurnal Natur Indonesia Journal of Tropical Soils Widya Wacana : Jurnal Ilmiah Alchemy : Journal of Chemistry Bulletin of Electrical Engineering and Informatics Journal on Mathematics Education (JME) Teosofi: Jurnal Tasawuf dan Pemikiran Islam Jurnal Ilmu Kimia Universitas Brawijaya Indonesian Green Technology Journal Jurnal Pembangunan dan Alam Lestari The Journal of Pure and Applied Chemistry Research AGRIVITA, Journal of Agricultural Science SEMIRATA 2015 Prosiding Semnastek JURNAL ILMIAH PENDIDIKAN FISIKA AL BIRUNI Majalah Obat Tradisional Proceeding SENDI_U Wahana Akademika: Jurnal Studi Islam dan Sosial Profetika JOIV : International Journal on Informatics Visualization Jurnal Akta Union: Jurnal Ilmiah Pendidikan Matematika Jurnal Penelitian Pendidikan IPA (JPPIPA) Jurnal Matematika Sains dan Teknologi JURNAL SINEKTIK Mesin Martabe : Jurnal Pengabdian Kepada Masyarakat Jurnal Surya Masyarakat Walisongo Journal of Chemistry Prima: Jurnal Pendidikan Matematika MUHARRIK: JURNAL DAKWAH DAN SOSIAL Seminar Nasional Lahan Suboptimal International Journal of Active Learning Journal of Authentic Research on Mathematics Eduacation (JARME) M A T H L I N E : Jurnal Matematika dan Pendidikan Matematika Jurnal Komunikasi Pendidikan Indonesian Journal of Electrical Engineering and Computer Science Southeast Asian Mathematics Education Journal Al-Manhaj: Jurnal Hukum dan Pranata Sosial Islam Jurnal Penelitian Pendidikan Matematika Interdisciplinary Social Studies Indo-MathEdu Intellectuals Journal Educenter: Jurnal Ilmiah Pendidikan Jurnal Penelitian Ilmu Sosial dan Eksakta Jurnal Pengabdian Masyarakat Bestari (JPMB) Jurnal Ilmiah Pendidikan Dasar (JIPDAS) Makara Journal of Technology JAPI: Jurnal Akses Pengabdian Indonesia Community Services and Social Work Bulletin Indonesian journal of teaching and learning Proceeding of International Conference on Science, Education, and Technology Jurnal Konseling Pendidikan Islam Jurnal Komprehenshif International Journal of Renewable Energy Development The Sociology of Islam EDUCENTER JURNAL PENDIDIKAN Journal of Tropical Pharmacy and Chemistry Help: Journal of Community Service Jurnal Sosialita: Jurnal Kajian Sosial dan Pendidikan Jurnal Studi Islam dan Sosial
Warsito Warsito
Jurusan Fisika, FMIPA, Universitas Lampung
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Journal : Alchemy : Journal of Chemistry

 1 
ISOLASI ASAM-9Z,12Z,15Z-OKTADEKATRIENOAT DARI BIJI SELASIH (Ocimum basilicum) Fasya, Ahmad Ghanaim; Retnowati, Rurini; Rahman, M.; Duengo, Suleman; Warsito, Warsito
ALCHEMY ALCHEMY (Vol.2 No.1
Publisher : Department of Chemistry, Faculty of Science and Technology UIN Maulana Malik Ibrahim Malan

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (783.743 KB) | DOI: 10.18860/al.v0i0.2300

Abstract

The α-linolenic acid (9,12,15-octadecatrieonic acid) is omega-3 fatty acid that more active than other fatty acids to inhibit cell membrane damages, formation and growth of brain functions, antiinflamatory and prevent several cronic deseases like lung desease and arthrytis. Some research explain that geometri of omega-3 fatty acids had effect on its bioactivity. This research purpose was to isolate α-linolenic acid with geometry Z,Z,Z (9Z,12Z,15Z-oktadekatrienoat).O. basilicum seeds oil was isolated from O. basilicum seeds using Soxhlet extraction with n-hexane, then hidrolized by 12 % solution of KOH in aquadest. The α-linolenic acid was separated from other fatty acids by urea inclusion methods. The optimum condition of urea inclusion was determined in various temperature     (+ 5, + 3, + 1, + (-1), + (-3), + (-5))0C and ratio of fatty acid : urea 1:1; 1:1,5; 1:2; 1:2,5; 1:3; 1:3,5; 1:4.From this research, extraction of O. basilicum seeds oil with n-hexane as solvent resulted clear yellow-brown oil with refractive indeks 1,466 and density 0,855 g/mL. Gas Chromatography (GC) analysis of fatty acids hidrolyzed from   O. basilicum oil showed peak at tR= 19,949 minutes with relative percentage 70,72 %. Base on Mass Spectrum (MS), the fragmentation of this compound, with  tR= 19,949 minutes, was identic with 9Z,12Z,15Z-oktadecatrienoic acid.Isolation of α-linolenic acid from other fatty acids using urea inclusion at temperature 0-2 0C dan rasio fatty acid: urea 1:1,5 showed nonadduct fraction contains compound with tR= 19,980 minutes and relative percentage 88,51 %. Base on Mass Spectrum (MS), the fragmentation of this compound, with tR= 19,980 minutes, was identic with 9Z,12Z,15Z-oktadecatrienoic acid.
Co-Authors A. Ghanaim Fasya Abd. Rasyid Syamsuri Abdul Madjid Adhaini, Finna Adi Hermansyah, Adi Admi Syarif Adryanto, Edwin Aewaditha, Randha Kentama Agus Hermawan Agus Hidayat Agus Riyanto Agus Wantoro Ahmad Ahmad Ahmad Amarullah, Ahmad Akhmad Dzakwan, Akhmad Akhmad Sabarudin Alfiansyah, Irfan Alief, M. Fadel Amartiya Sari, Shabilla Angraini, Lili Anis Artiyani Apriyanto, Donni Kis Arie Srihardyastutie Arif Fadilah, Ahmad Armanto, Mustika Edi Asrowi Asrowi Ayu Sangging, Putu Ristyaning Azhar, Asyfariatus Zulfa Aziz, Mohamad Fathoni Azzahra, Vina Octavia Bakri Bakri Bayu Indrayanto Berliana, Adilatunnisa Nur Indah Chabiburrochman, M. Mas'ud Citra, Dewi Sriani D Budianta, D Damiana Nofita Birhi Darmanto, Prihadi Setyo Dedi Muhtadi, Dedi Denanda Putri, Lisa Destyarini, Normalita Dewi, S. K. Dewi, S. K. Diah Mardiana Dian Wahyuningsih Dodi Iskandar, Dodi Dwi Hartantri, Saktian Dwi Paserena, Karinda Dwi Setyawan Dyan Isworo Edi Priyo Utomo Elvina Dhiaul Iftitah Endah Setiani Astuti Erwanto Evi Elisanti, Evi Fahmi, Jam’an Farhana, Nida Fuady, Anies Ghea Salsabila, Nadhira Ghifari, Muhammad Al Gumilar, Aris Guntoro, Muhammad Yogi Gurum A P Gurum A P, Gurum A P Gusrianto, Anindira Aiska Haikal, Umair Hamdani Hamdani Hardati, Ratna Nikin Haswati, Desty Heni Sulistiani Hepsi Nindiasari Husnul Muttaqin I Made Astina Ichsan Ichsan Ilham Mundzir Iskandar, Ratu Sarah Fauziah Junaidi Junaidi Kalpataru I Kalpataru I, Kalpataru I Kamilatun, Nur Ahya Kautsari, Alya Paradisa Khairun Nisa Kuncara, Fatihah Nanda Kurnia Muludi M. Farid Rahman M. Rahman Mardiansa, Edwin Maren, A Marjunus, Roniyus Markoni Markoni Marlina Marlina Marsi Marsi Masruri Masruri Masruri Meilasari, Nabilla Melan, Firdania Desfani Miranda, Fitri Ariadna Sodi Moch Sasmito Djati Momon Sodik Imanuddin Muhammad Ikhsanudin, Muhammad Muhammad Wildan Muhammad Yasir Mulyoto mulyoto Mustaufir, Mustaufir Nashi Widodo Nisa Berawi, Khairun Nisa’us Sholikah Noer Aini Nugraha, Fadylah Akbar NUNI GOFAR Nur Choiro Siregar, Nur Choiro Nur Hidayat Nuriyanti, Ika Nur’aini, Dhiva Maulida Rizqi Pangestu, Ilham Aji Pauzi, Gurum Ahmad Pradja, Bara P. Prahesti Tirta Safitri, Prahesti Tirta Pratomo, Sigit Adhi Priatna, S J Purwo Haryono Putri Nur, Tri Ramadhan, Dwi Sapri Redy Susanto, Erliyan Renih Hayati Rina Arum Prastyanti, Rina Arum Rini Rahayu Kurniati Rizqi Alima Fabri, Ahmad Rodiyah, Roirotul Rohaya, Nizla Rollando, Rollando Rosli, Roslinda Rukmono Budi Utomo, Rukmono Budi Rully Charitas Indra Prahmana Rurini Retnowati Sabaruddin Sabaruddin Sabilah, Sahla Safitri, Wulan Dwi Sahil, Mawardi Abi Saleh, Hairul Satria Jaya Priatna, Satria Jaya Seta, Fadhlih Arya Setyawan, Dodi Yudo Shofiatul Jannah Siti Mariyah Ulfa SITI MUSLIKAH Sri Anitah Sri Budiyono, Sri Sri Suciyati, Sri Sri Wahyu Suciyati Sudiyo Widodo, Sudiyo Suharti, Eni Suhud Eko Yuwono Sukirwan Sukirwan Sulaiman, Abdulah Suleman Duengo Sumaryo Gitosaputro Sumaryo Sumaryo sunhaji sunhaji Supriyanto, Amir Surtono, Arif Susi Harnani, Susi Sutiman B. Sumitro Teguh Achadi Upik Mutiara Vientje Ratna Multiwijaya Wardana, Dian Widoretno, W. Widoretno, W. Wisnu Nugroho Aji, Wisnu Nugroho Wulan, Indah Indar Yakup Parto Yanti Yulianti Yeni Nuraeni, Yeni Yeni Prasetyo, Yeni Yodhi Yuniarthe Zatira, Dhea