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All Journal International Journal of Renewable Energy Development Jurnal Al Bayan: Jurnal Jurusan Pendidikan Bahasa Arab Jurnal Al-Maqayis ARABIYAT Seminar Nasional Teknik Kimia Kejuangan Jurnal Akuatika Indonesia Arabi : Journal of Arabic Studies Ijaz Arabi Journal of Arabic Learning ASALIBUNA Al Mi’yar: Jurnal Ilmiah Pembelajaran Bahasa Arab dan Kebahasaaraban Studi Arab Thaqafiyyat : Jurnal Bahasa, Peradaban dan Informasi Islam El-Tsaqafah: Jurnal Jurusan PBA EDUKATIF : JURNAL ILMU PENDIDIKAN J-KESMAS: Jurnal Kesehatan Masyarakat Jurnal Akuntansi Kompetif PREPOTIF : Jurnal Kesehatan Masyarakat ENTITA: Jurnal Pendidikan Ilmu Pengetahuan Sosial dan Ilmu-Ilmu Sosial Management Studies and Entrepreneurship Journal (MSEJ) Jurnal ABDINUS : Jurnal Pengabdian Nusantara Legal Spirit At-Thullab : Jurnal Pendidikan Guru Madrasah Ibtidaiyah Edu Masda Journal Moluccas Health Journal Kontribusi: Jurnal Penelitian dan Pengabdian Kepada Masyarakat Jurnal Kesehatan dan Pengelolaan Lingkungan Asalibuna Sewagati Journal of Educational Management Research Jurnal Al-Ihda Journal of Educational Management and Learning International Journal of Renewable Energy Development Menara Tebuireng : Jurnal Ilmu-Ilmu Keislaman Jurnal KALANDRA NGARSA: Journal of Dedication Based on Local Wisdom Jurnal Manajemen Strategis Qismul Arab: Journal of Arabic Education Bayan lin-Naas : Jurnal Dakwah Islam Hudan Linnaas: Jurnal Ilmu Sosial dan Humaniora Proceeding Of International Conference On Education, Society And Humanity Al-Tadris: Jurnal Pendidikan Bahasa Arab EL-FUSHA Al-Irfan: Journal Of Arabic Literature and Islamic Studies AL TADIB : Jurnal Ilmu Pendidikan
Lailatul Qomariyah, Lailatul
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Journal : International Journal of Renewable Energy Development

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Optimization of ultrasonication time on the production of ZnO-SiO2 nanocomposite as photocatalytic material Qomariyah, Lailatul; Faizah, Nurul; Karisma, Achmad Dwitama; Rabbani, Sulthan; Kalloka, Sultan Hendra Mahardi; Putra, Nicky Rahmana
International Journal of Renewable Energy Development Vol 14, No 5 (2025): September 2025
Publisher : Center of Biomass & Renewable Energy (CBIORE)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.61435/ijred.2025.61248

Abstract

Nanocomposite ZnO-SiO2 is widely known for its efficacy as a semiconductor photocatalyst. Current nanocomposite production methods face challenges like particle agglomeration and inconsistent particle size control. To overcome this problem, the ultrasonication method was used to prevent agglomeration and produce composites in nanoscale, where this study synthesized ZnO-SiO2 for photocatalytic degradation of dye color. To prepare this nanocomposite, the ultrasonication time was varied from 0 to 45 minutes to understand the particle properties and the effectivity on the photocatalytic activity. Silica was prepared from water glass via sol-gel method to produce colloidal SiO2 nanoparticles and then mixed with ZnO with the ratio of 3% wt and subjected to ultrasonication method. Under various ultrasonication time, the FTIR analysis shows the Si-O peak at 895 cm-1 indicates the presence of SiO2 particles. The XRD validate the formation of ZnO-SiO2 nanoparticles, supporting the FTIR analysis. The best nanoparticle properties were achieved with 45 minutes of ultrasonication. The SEM analysis confirms the present of SiO2 and ZnO. From BET analysis, ZnO-SiO2 has a high surface area (117.64 m2/g), moderate pore volume (0.46 cm3/g), and small particle pore size (11.59 nm). The photocatalytic activity of ZnO-SiO₂ nanocomposites was evaluated by the degradation of methylene blue (MB) under sunlight and the best performance reached by the nanocomposite prepared under 45 minutes ultrasonication. The results show that the ultrasonication technique efficiently reduces agglomeration, as indicated by a reduction in particle diameter from 35.04 nm (pure ZnO) to 11.59 nm (ZnO-SiO₂), and significantly enhances photocatalytic activity, achieving 97% degradation of MB under sunlight after 180 minutes. The aforementioned technique demonstrates significant potential for industrial use, providing higher efficiency and expandability in manufacturing superior photocatalytic substances.
Co-Authors A.Fatikhul Amin Abdullah, A.Fatikhul Amin Aang Kunaifi Abda Abda Abdul Qodir Abdul Qodir Achmad Dwitama Karisma Adam Ibrahim, Faishol Mahmud Adi Soeprijanto adminojs, adminojs Afan Hamzah, Afan Agustin, Dayriqoh Ahmad Zulfikar Ali Ahya', Akhmad Sauqi Ahya, Ahmad Sauqi Ahya, Akhmad Sauqi Ahya’, Akhmad Sauqi Ahya’, Akhmad Sauqi Akhmad Farid Al Hayaza, M. Iqbal Alamsyah, Wisnu Tansya Trisna Alrasid Alfarisi, Achmad Hasan AlGhifari, Husain Ali Altway Ali Mahsun Ali Maskur, Muhammad Aljauhari, Ahmad Khusnul Umam Alkamalia, Andini Nabila Andesra, Zel Anggraini Karditiawati Anisa, Lia Rizqi Nur Apri Arisandi Arifin, Rizal Ariga Bahrodin Asriana kibtiyah Aulia, Anisa Fatma Cahyani, Budiato Dahlina, Dahlina Danawati Hari Prajitno Dewi Indah Sari, Dewi Indah Dian Pratiwi Erna Sulistyowati Fadhilah, Lailatul Fadli Hidayat, M. Noer Faisal Mubarak Faizal, Doddy Fariza, Dita Sari Rofi’u Fatah, Muhammad Ghoni Abdillah Fauziyah, Naily Hanif, Nafis Fauzul Hidayatullah, Wasil Humaira Fadhilah Ibrahim, Faishol Mahmud Adam Ika Suswanti Ilahiyah, Iva Inayatul Ilahiyah, Iva Inyatul Inayah Inayah Inayah Inayah Indana Lazulfa, Indana Indra Kurniawan Inggri Dwi Rahesi Ismahayati, Dewi Iva inayatul Ilahiyah Jepri Nugrawiyati Jojok Dwiridotjahjono Kalloka, Sultan Hendra Mahardi Kurniawati, Novia Indah Laily Masruroh, Laily Lily Pudjiastuti, Lily Luthfi Hakim Luthfiyatul Mustafidah Ma'muroh, Ma'muroh Maharani, Karlina Dewi Mahbubah, Surotul Mahmoud, Mustafa Farouq Abdul-Aaleem Maimon Sumo Mamluatul Hasanah Maskanah, Siti Naharul Masruroh, Sayidah Afyatul Ma’suq, Ahmad Tarajjil Melady, Dian Muhammad Ahsanul Husna Muhammad Ridho Muhammad Zulfikar Adha Mulkis, Ismi Malika Mustafidag, Luthfiya Musyarrofah, Musyarrofah Mu’at Mu’at, Mu’at MZ, Isniyatun Niswah Najahah, Umdatun Ni'mah, Mamluatun Niniek Fajar Puspita, Niniek Fajar Niswah MZ, Isniyatun Niswah, Isniyatun Nur Kuswanti Nuritasari, Fetty Nurlaili Humaidah, Nurlaili NURUL FAIZAH Patriolika, Erika Putra, Nicky Rahmana Rabbani, Sulthan Rafiudin, Asep Ratnawati, Mamik Ririn Probowati, Ririn Rohanah, Rohanah Romlah, St RR. Ella Evrita Hestiandari Salim, Sulaiman Salsabila, Fina Fathiya Satriani Satriani Sa’adah, Khofifatus Setyabudi, Mohammad Arif Siti Rofiah Sucipto Sulfa, Indana Suprapto Suprapto SYAIFUL BAHRI Syarif Hidayatullah Tamim Mulloh Taufiqurrahman Taufiqurrahman Tien Fitriyah, Mas Anienda Tri Nur Fauziyah, Tri Nur Trisanti, Warlinda Eka Umam, Muhammad Khairul Wazis, Kun Widiyati, Evita Wildan Nafi'i Yulia Yulia Zabrina, Diva Zainul Hidayah Zayyadi, Moh Zenyta, Zenyta Zuchrillah, Daril Ridho